IP Library › Granted Patent US 11,519,071
Granted Patent B2
US 11,519,071 · App. 16/778,642 · Granted Dec 6, 2022

Method for fabricating chamber parts

Inventors: Gang Grant Peng (Fremont, CA); David W. Groechel (Los Altos Hills, CA); Han Wang (Palo Alto, CA)
Assignee: Applied Materials, Inc.
C23C16/56C23C16/405H01J37/32495H01J37/3426
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Quick Facts
Patent No.
US 11,519,071
App. No.
16/778,642
Granted
Dec 6, 2022
Kind
B2
Abstract

One example of the disclosure provides a method of fabricating a chamber component with a coating comprising a yttrium containing material with desired film properties. In one example, the method of fabricating a coating material includes providing a base structure comprising an aluminum containing material. The method further includes forming a coating layer that includes a yttrium containing material on the base structure. The method also includes thermal treating the coating layer to form a treated coating layer.

Claims (38)

1. A method of fabricating a coating material, comprising:

providing a base structure comprising an aluminum containing material;

forming a coating layer comprising a yttrium containing material on the base structure; and

thermal treating the coating layer with a thermal source to form a treated coating layer, wherein the thermal source has an energy density between about 1 μJ/cm 2 and about 2 μJ/cm 2 , and a frequency between about 1 kHz and about 20 MHz.

2. The method of claim 1 , wherein the yttrium containing material is at least one of yttrium oxide or fluorine yttrium oxide, or fluorine yttrium oxide with metal dopants.

3. The method of claim 1 , wherein thermal treating the coating layer comprises:

performing a laser treatment process on the coating layer.

4. The method of claim 3 , wherein performing the laser treatment process comprises:

directing a light radiation from a laser module to a surface of the coating layer.

5. The method of claim 4 , wherein the laser module provides the light radiation having a wavelength between about 187 nm and about 10000 nm.

6. The method of claim 4 , wherein the laser module provides the light radiation having a wavelength between 248 nm and about 2100 nm.

7. The method of claim 1 , wherein thermal treating the coating layer further comprises:

maintaining a base structure temperature at between about 15 degrees Celsius and about 75 degrees Celsius.

8. The method of claim 1 , wherein the yttrium containing material is yttrium oxide.

9. The method of claim 1 , wherein the treated coating layer has a film density greater than 4 g/cm 3 .

10. The method of claim 1 , wherein the treated coating layer has a thickness between about 0.5 μm and about 50 μm.

11. The method of claim 1 , wherein the base structure is a gas distribution plate or a substrate support assembly in a processing chamber.

12. The method of claim 1 , wherein the base structure is a chamber component utilized in a plasma processing chamber.

13. The method of claim 1 , wherein the treated coating layer has a surface roughness greater than Ra 5 micrometer.

14. The method of claim 1 , wherein the aluminum containing material of the base structure is Al 2 O 3 , AlN or a ceramic material.

15. The method of claim 1 , wherein thermal treating the coating layer further comprises:

removing surface particles from the base structure.

16. A method of fabricating a coating material, comprising:

providing a base structure comprising an aluminum containing material;

forming a coating layer comprising a yttrium containing material on the base structure; and

laser treating the coating layer to form a treated coating layer, wherein the laser has an energy density between about 1 μJ/cm 2 and about 2 μJ/cm 2 , and a frequency between about 1 kHz and about 20 MHz.

17. The method of claim 16 , wherein the yttrium containing material is at least one of yttrium oxide, fluorine yttrium oxide, or fluorine yttrium oxide with metal dopants.

18. The method of claim 16 , wherein the base structure is a gas distribution plate disposed in a plasma processing chamber.

19. A method of fabricating a coating material, comprising:

forming a coating layer comprising a yttrium containing material on a base structure, the base structure comprising an aluminum containing material; and

laser treating the coating layer to form a treated coating layer, the laser treating comprising:

applying a series of laser pulses to the coating layer, wherein each laser pulse of the series of laser pulses has an energy density within a range of about 1 μJ/cm 2 to about 2 μJ/cm 2 , a frequency within a range of about 1 kHz to about 20 MHz, a wavelength within a range of about 248 nm to about 2100 nm, and a duration within a range of about 10 femto-seconds to about 10 micro-seconds, and

reacting a gas with the coating layer, the gas containing one or more of oxygen or nitrogen.

20. The method of claim 19 , wherein the gas reacts with the coating layer while the series of laser pulses are applied to alter a bonding energy of the coating layer, and the treated coating layer has:

a density within a range of about 4.0 g/cm 3 to about 5.2 g/cm 3 ;

a yttrium to oxide (Y:O) ratio within a range of about 1:1 to about 2:1;

a thickness within a range of about 0.5 μm to about 50 μm; and

a pore density less than 2%.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 5, 2020
From: PENG, GANG GRANT; GROECHEL, DAVID W.; WANG, HAN
To: APPLIED MATERIALS, INC.
Reel/Frame 051730/0152 →
Continuity (2)
Provisional Application 62804545 · Feb 12, 2019
Related Publication 20200255946A1 · Aug 13, 2020
Cited By (1)
US 12,637,761