IP Library › Granted Patent US 11,542,214
Granted Patent B2
US 11,542,214 · App. 17/060,506 · Granted Jan 3, 2023

Oxidative coupling of methane methods and systems

Inventors: Guido Radaelli (South San Francisco, CA); Robert Bridges (Friendswood, TX); Humera A. Rafique (Dublin, CA); Suchia Duggal (San Rafael, CA); Srinivas Vuddagiri (Davis, CA); Joel Cizeron (Redwood City, CA); Jarod McCormick (San Carlos, CA); Bipinkumar Patel (Richmond, TX); Satish Lakhapatri (Mountain View, CA)
Assignee: Lummus Technology LLC
C07C2/84C01B3/38C07C4/02C07C5/48C07C29/1518C07C29/48C25B1/04C25B1/26C25B15/08C01B2203/0233C01B2203/0283C01B2203/043C01B2203/0445C01B2203/0465C01B2203/0475C01B2203/061C01B2203/068C01B2203/0811C01B2203/0827C01B2203/0833C01B2203/0872C01B2203/1241C01B2203/84
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Quick Facts
Patent No.
US 11,542,214
App. No.
17/060,506
Granted
Jan 3, 2023
Kind
B2
Abstract

The present disclosure provides natural gas and petrochemical processing systems including oxidative coupling of methane reactor systems that integrate process inputs and outputs to cooperatively utilize different inputs and outputs of the various systems in the production of higher hydrocarbons from natural gas and other hydrocarbon feedstocks.

Claims (29)

1. An oxidative coupling of methane (OCM) method to generate hydrocarbon compounds containing at least two carbon atoms (C 2+ compounds), the method comprising:

(a) injecting oxygen (O 2 ), methane (CH 4 ), and ethane (C 2 H 6 ) into an adiabatic OCM reactor, wherein the adiabatic OCM reactor comprises an adiabatic OCM reaction section comprising an OCM catalyst bed for facilitating an OCM reaction and an adiabatic post-bed cracking (PBC) section for facilitating conversion of C 2 H 6 to ethylene (C 2 H 4 ) with the aid of heat liberated by the OCM reaction, and wherein the C 2 H 6 has a concentration of at least 3 mol % at an inlet of the adiabatic OCM reactor and wherein the concentration of C 2 H 6 at the inlet of the adiabatic OCM reactor is maintained within +/−0.2 mol %;

(b) with the aid of the OCM catalyst in the adiabatic OCM reaction section, performing an OCM reaction to convert the CH 4 into C 2+ compounds as part of a product stream;

(c) in the adiabatic PBC section of the adiabatic OCM reactor and with the aid of heat liberated by the OCM reaction, converting C 2 H 6 in the product stream into C 2 H 4 as part of an OCM effluent;

(d) separating the OCM effluent to produce at least an ethane stream and a stream enriched in C 2 H 4 ;

(e) recycling a portion of the ethane stream to an inlet of the adiabatic OCM reaction section; and

(f) recycling a portion of the ethane stream to the adiabatic PBC section, wherein the method has a carbon efficiency of at least 60%.

2. The method of claim 1 , wherein the concentration of C 2 H 6 at an inlet of the OCM catalyst bed is at least 3.5 mol %.

3. The method of claim 1 , wherein at least a portion of the C 2 H 6 is injected into the adiabatic OCM reactor separately from the CH 4 .

4. The method of claim 1 , further comprising increasing or decreasing an amount of CH 4 injected in (a) to maintain the concentration of C 2 H 6 during the injecting.

5. The method of claim 1 , wherein the concentration of C 2 H 6 at the inlet of the OCM reactor is from 3 mol % to 6 mol %.

6. The method of claim 1 , wherein the carbon efficiency is from 60% to 85%.

7. The method of claim 1 , wherein at least a portion of the C 2 H 6 injected into the adiabatic OCM reactor is injected into a sulfur removal unit prior to being injected into the adiabatic OCM reactor.

8. The method of claim 1 , wherein the methane injected into the adiabatic OCM reactor is provided by a methanated stream comprising methane produced by a methanation reactor.

9. The method of claim 8 , wherein a natural gas stream comprising methane is combined with the OCM effluent prior to separating the OCM effluent.

10. An oxidative coupling of methane (OCM) method to generate hydrocarbon compounds containing at least two carbon atoms (C 2+ compounds), the method comprising:

(a) injecting oxygen (O 2 ), methane (CH 4 ), and ethane (C 2 H 6 ) into an adiabatic OCM reactor, wherein the adiabatic OCM reactor comprises an OCM reaction section comprising an OCM catalyst bed for facilitating an OCM reaction and an adiabatic post-bed cracking (PBC) section for facilitating conversion of C 2 H 6 to ethylene with the aid of heat liberated by the OCM reaction, and wherein the C 2 H 6 has a concentration of at least 3 mol % within the OCM catalyst bed and wherein a concentration of C 2 H 6 at an inlet of the adiabatic OCM reactor is maintained within +/−0.2 mol %; and

(b) with the aid of the OCM catalyst bed in the OCM reaction section, performing an OCM reaction to convert CH 4 into C 2 + compounds as part of a product stream;

(c) in the adiabatic PBC section of the adiabatic OCM reactor and with the aid of heat liberated by the OCM reaction, converting C 2 H 6 in the product stream into ethylene (C 2 H 4 ) as part of an OCM effluent;

(d) separating the OCM effluent to produce at least an ethane stream and a stream enriched in C 2 H 4 ;

(e) recycling a portion of the ethane stream to the OCM reaction section; and

(f) recycling a portion of the ethane stream to the adiabatic PBC section, wherein the method has a carbon efficiency of at least 60%.

11. The method of claim 10 , wherein at least a portion of the C 2 H 6 is injected into the adiabatic OCM reactor separately from the CH 4 .

12. The method of claim 10 , further comprising increasing or decreasing an amount of CH 4 injected in (a) to maintain the concentration of C 2 H 6 at the inlet of the adiabatic OCM reactor.

13. The method of claim 10 , wherein the concentration of C 2 H 6 at the inlet of the adiabatic OCM reactor is from 3 mol % to 6 mol %.

14. The method of claim 10 , wherein the carbon efficiency is from 60% to 85%.

15. The method of claim 10 , wherein at least a portion of the C 2 H 6 injected into the adiabatic OCM reactor is injected into a sulfur removal unit prior to being injected into the adiabatic OCM reactor.

16. The method of claim 10 , wherein at least a portion of the methane injected into the adiabatic OCM reactor is provided by a methanated stream comprising methane produced by a methanation reactor.

17. The method of claim 16 , wherein a natural gas stream comprising methane is combined with the OCM effluent prior to separating the OCM effluent.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 7, 2020
From: RADAELLI, GUIDO; BRIDGES, ROBERT; RAFIQUE, HUMERA A.; DUGGAL, SUCHIA; VUDDAGIRI, SRINIVAS; CIZERON, JOEL; MCCORMICK, JAROD; PATEL, BIPINKUMAR; LAKHAPATRI, SATISH
To: SILURIA TECHNOLOGIES, INC.
Reel/Frame 053998/0412 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 7, 2020
From: SILURIA TECHNOLOGIES, INC.
To: SILURIA (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
Reel/Frame 053998/0486 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 7, 2020
From: SILURIA (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
To: LUMMUS TECHNOLOGY LLC
Reel/Frame 053998/0508 →
Continuity (10)
Continuation 15690090 · Aug 29, 2017
Continuation PCTUS2016022891 · Mar 17, 2016
Continuation In Part 14789953 · Jul 1, 2015
Provisional Application 62195237 · Jul 21, 2015
Provisional Application 62190182 · Jul 8, 2015
Provisional Application 62141177 · Mar 31, 2015
Provisional Application 62152706 · Apr 24, 2015
Provisional Application 62134508 · Mar 17, 2015
Provisional Application 62300287 · Feb 26, 2016
Related Publication 20210024439A1 · Jan 28, 2021
Cited By (1)
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