Method of manufacturing semiconductor device
According to one aspect of the technique, there is provided a method of manufacturing a semiconductor device, including: (a) heating a substrate to a first temperature while supporting the substrate on a substrate support, and supplying a process gas into a process vessel accommodating the substrate support; (b) lowering a temperature of a low temperature structure provided in the process vessel to a second temperature lower than the first temperature by supplying an inert gas or air to a coolant flow path provided in the process vessel after (a) for a predetermined time, wherein defects occur when a cleaning gas is supplied to the low temperature structure at the first temperature; and (c) cleaning the low temperature structure by supplying the cleaning gas into the process vessel after (b).
1. A method of manufacturing a semiconductor device, comprising:
(a) heating a substrate to a first temperature while supporting the substrate on a substrate support, and supplying a process gas into a process vessel accommodating the substrate support;
(b) lowering a temperature of a low temperature structure provided in the process vessel to a second temperature lower than the first temperature by supplying an inert gas or air to a coolant flow path provided in the process vessel and connected to a vacuum pump after (a) for a predetermined time, wherein corrosion or peel-off of a coating occurs when a cleaning gas is supplied to the low temperature structure at the first temperature; and
(c) cleaning the low temperature structure by supplying the cleaning gas into the process vessel after (b),
wherein the coolant flow path is vacuum-exhausted while the vacuum pump is in operation during at least one of (a) or (c).
2. The method of claim 1 , wherein the inert gas supplied to the coolant flow path comprises a gas capable of maintaining a cooling effect at the first temperature.
3. The method of claim 1 , wherein a valve is provided at the coolant flow path, and is closed when the second temperature is reached in (b).
4. The method of claim 1 , further comprising
(d) elevating an inner temperature of the process vessel after (c) without supporting the substrate on the substrate support.
5. The method of claim 4 , wherein the vacuum pump vacuum-exhausts the coolant flow path in (d).
6. The method of claim 4 , wherein a heater located radially more inward than the coolant flow path is controlled in (d).
7. The method of claim 4 , wherein a heater is embedded in the substrate support, and a distance between the substrate support and the low temperature structure is set to be greater in (d) than in (a).
8. The method of claim 1 , wherein the low temperature structure is made of a material susceptible to corrosion by the process gas and a corrosion prevention coating is formed on a region of the low temperature structure in contact with the process gas, and
wherein the process gas is supplied in (a) in a state in which the low temperature structure is coated by the corrosion prevention coating, and
the temperature of the low temperature structure is lowered in (b) to a temperature capable of preventing a deterioration of the corrosion prevention coating.
9. The method of claim 1 , wherein the low temperature structure comprises a shower head, and the coolant flow path is provided around the shower head.
10. The method of claim 1 , wherein the low temperature structure comprises a shower head made of a material susceptible to corrosion by the process gas and a corrosion prevention coating is formed on a surface of the shower head parallel to the substrate, and
wherein the process gas is supplied in (a) in a state in which the low temperature structure is coated by the corrosion prevention coating, and
the temperature of the low temperature structure is lowered in (b) to a temperature capable of preventing a deterioration of the corrosion prevention coating.
11. The method of claim 1 , wherein the low temperature structure comprises a shower head made of a material susceptible to corrosion by the process gas and a corrosion prevention coating is formed on a through-hole of the shower head, and
wherein the process gas is supplied in (a) in a state in which the low temperature structure is coated by the corrosion prevention coating, and
the temperature of the low temperature structure is lowered in (b) to a temperature capable of preventing a deterioration of the corrosion prevention coating.
12. The method of claim 1 , wherein the low temperature structure comprises a shaft supporting the substrate support, and the coolant flow path is provided inside the shaft.
13. The method of claim 1 , wherein a substrate loading/unloading port is provided at the process vessel,
a gate valve constituted by a valve body and a shaft is provided adjacent to the substrate loading/unloading port, and
the low temperature structure is located in vicinity of the substrate loading/unloading port.
14. The method of claim 1 , wherein a viewport is provided at the process vessel such that an inside of the process vessel is visually recognizable from an outside of the process vessel through the viewport, and
the low temperature structure is located in vicinity of the viewport.
15. The method of claim 1 , wherein the low temperature structure comprises an O-ring, and the coolant flow path is provided around the O-ring.
16. The method of claim 15 , wherein the coolant flow path is provided between the O-ring and a heater.
17. The method of claim 1 , wherein a heater is embedded in the substrate support, and a distance between the substrate support and the low temperature structure is set to be greater in (b) than in (a).
18. A substrate processing apparatus configured to be capable of performing the method of claim 1 .
19. A method of manufacturing a semiconductor device, comprising:
(a) heating a substrate to a first temperature while supporting the substrate on a substrate support, and supplying a process gas into a process vessel accommodating the substrate support;
(b) lowering a temperature of a low temperature structure provided in the process vessel to a second temperature lower than the first temperature by supplying an inert gas or air to a coolant flow path provided in the process vessel and connected to a vacuum pump after (a) for a predetermined time, wherein corrosion or peel-off of a coating occurs when a cleaning gas is supplied to the low temperature structure at the first temperature; and
(c) cleaning the low temperature structure by supplying the cleaning gas into the process vessel after (b),
wherein the coolant flow path is vacuum-exhausted while the vacuum pump is in operation during at least one of (a) or (c), and
wherein the low temperature structure comprises one selected from the group consisting of:
a material susceptible to corrosion by the process gas;
a structure located in vicinity of a viewport wherethrough an inside of the process vessel is visually recognizable from an outside of the process vessel; and
an O-ring provided around the coolant flow path.
20. A substrate processing apparatus configured to be capable of performing the method of claim 19 .