IP Library Granted Patent US 11,579,060
Granted Patent B2
US 11,579,060 · App. 16/956,940 · Granted Feb 14, 2023

Method and device for measuring fat in milk

Inventors: Stefan Pflüger (Munich, DE); Wolfgang Drahm (Erding, DE); Hao Zhu (Freising, DE)
Assignee: Endress+Hauser Flowtec AG
G01N9/002G01F1/74G01F1/8436G01F1/8468G01K13/02G01L19/00G01N22/00G01N33/06G01K13/026
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Quick Facts
Patent No.
US 11,579,060
App. No.
16/956,940
Granted
Feb 14, 2023
Kind
B2
Abstract

Disclosed is a method for determining of fat content of milk having variable solids fractions and flowing with variable gas content in a pipeline. The method includes ascertaining a velocity of sound and an average density value for the milk based on eigenfrequencies of at least two bending oscillation wanted modes of measuring tubes of a densimeter arranged in the pipeline. The method further includes ascertaining a static pressure in the pipeline; a gas volume fraction based on the velocity of sound; the average density; the pressure; a density of the milk without gas content based on the average density and the gas volume fraction; and a permittivity of the milk based on a propagation velocity and/or an absorption of microwaves in the milk. The fat fraction is calculated based on the density of the milk without gas content and on the effective permittivity.

Claims (36)

1. A method for determining a fat content of milk, wherein the milk has variable solids fractions and flows with a variable gas content in a pipeline, the method comprising:

arranging a densimeter in the pipeline and flowing the milk through the densimeter;

determining a first eigenfrequency of a first bending oscillation mode of the densimeter and a second eigenfrequency of a second bending oscillation mode of the densimeter;

calculating a velocity of sound in the milk and calculating an average density for the milk based on the first and second eigenfrequencies;

measuring a static pressure in the pipeline using a pressure sensor connected to the pipeline;

calculating a gas volume fraction of the milk based on the velocity of sound in the milk, the average density, and the static pressure;

calculating a density of the milk without gas content based on the average density and based on the gas volume fraction;

measuring a propagation velocity and/or an absorption of microwaves in the milk using a microwave sensor arranged in the pipeline and calculating an effective permittivity of the milk from the propagation velocity and/or the absorption; and

calculating a fat fraction of the milk based on the density of the milk without gas content and on the effective permittivity of the milk.

2. The method as claimed in claim 1 , further comprising:

modeling the milk as a three component system of fat, water, and fat-free solids.

3. The method as claimed in claim 2 , wherein the fat-free solids include proteins and carbohydrates.

4. The method as claimed in claim 3 , further comprising:

calculating a concentration of each of the three components of fat, water, and fat-free solids:

modeling the density of the milk without gas content as a function of the concentration of each of the components of fat, water, and fat-free solids using density values of the respective component as weighting factors;

modeling the effective permittivity of the milk using the gas volume fraction of the milk, the concentration of each of the components of fat, water, and fat-free solids, and permittivity values of the respective components.

5. The method as claimed in claim 4 , further comprising:

measuring a temperature of the milk; and

calculating temperature dependent values for density and/or permittivity of the components contained in the milk.

6. The method as claimed in claim 4 , wherein the densimeter includes a Coriolis mass flowmeter, the method further comprising:

calculating at least one of the following: a mass flow of the milk, a volume flow of the milk, a fat flow of the milk, a fat-free solids flow of the milk, and a water flow of the milk in the pipeline.

7. The method as claimed in claim 1 , wherein the microwaves include at least one frequency above 1 GHz.

8. A measuring arrangement for determining a fat content of milk in a pipeline, comprising:

a densimeter having at least one oscillatable measuring tube and configured to determine a first eigenfrequency of a first bending oscillation mode and a second eigenfrequency of a second bending oscillation mode;

a pressure sensor for measuring a static pressure in the pipeline;

a microwave sensor for ascertaining a propagation velocity and/or an absorption of microwave signals in the milk; and

a computer unit for calculating the fat content of the milk, wherein the computer unit is configured to:

calculate a velocity of sound in the milk and calculate an average density for the milk based on the first and second eigenfrequencies;

read the static pressure in the pipeline using the pressure sensor;

calculate a gas volume fraction of the milk based on the velocity of sound in the milk, the average density, and the static pressure;

calculate a density of the milk without gas content based on the average density and based on the gas volume fraction;

measure the propagation velocity and/or the absorption of microwaves in the milk using the microwave sensor;

calculate an effective permittivity of the milk from the propagation velocity and/or absorption; and

calculate a fat fraction of the milk based on the density of the milk without gas content and on the effective permittivity.

9. The measuring arrangement as claimed in claim 8 , wherein the densimeter, the pressure sensor, and the microwave sensor are installed in the pipeline.

10. The measuring arrangement as claimed in claim 8 , wherein the densimeter includes a Coriolis mass flowmeter.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 22, 2020
From: PFLÜGER, STEFAN; DRAHM, WOLFGANG; ZHU, HAO
To: ENDRESS+HAUSER FLOWTEC AG
Reel/Frame 053003/0640 →
Priority Claims (1)
DE 10 2017 131 269.2 · Dec 22, 2017 · national
Continuity (1)
Related Publication 20210003491A1 · Jan 7, 2021