IP Library › Granted Patent US 11,643,612
Granted Patent B2
US 11,643,612 · App. 16/472,254 · Granted May 9, 2023

Fluorinated polyacrylate antifoam components for lubricating compositions

Inventors: Donald J. Knobloch (Mentor, OH); Kevin J. Hughes (Sammamish, WA); Michael E. Huston (Painesville, OH); William R. S. Barton (Belper, GB); Dennis M. Dishong (Willoughby Hills, OH); David M. Nickerson (Concord Township, OH)
Assignee: The Lubrizol Corporation
C10M147/04C10M101/00C10M169/041C10M2203/003C10M2213/04C10N2020/069C10N2020/071C10N2030/18C10N2040/04C10N2040/046C10N2040/08C10N2040/135C10N2040/25C10N2040/30
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Quick Facts
Patent No.
US 11,643,612
App. No.
16/472,254
Granted
May 9, 2023
Kind
B2
Abstract

There is disclosed an antifoam component for a mechanical device which includes a fluorinated poly(acrylate) copolymer. The antifoam component has improved foam performance and thermal stability in finished fluids, such as driveline fluids.

Claims (20)

1. A method of improving the foam reduction performance of a lubricating composition in the presence of silicone-based form-in-place gasket material, said method comprising:

adding an antifoam component to a form a lubricating composition, wherein said lubricating composition comprises:

a) an oil of lubricating viscosity selected from the group consisting of a Group II oil, a group II+ oil having a viscosity index greater than or equal to 110 and less than 120, Group III oil, a Group IV oil, a Group V, or mixtures thereof; and

b) said antifoam component comprising a poly(acrylate) copolymer including:

(i) from about 50 wt % up to about 72 wt % of an acrylate monomer having C 4 to C 8 alkyl esters of acrylic acid;

(ii) from about 10 wt % up to about 31 wt % of an acrylate comonomer having C 2 to C 3 alkyl esters of acrylic acid; and

(iii) from about 7.0 wt % up to 20 wt % of a fluorinated (meth)acrylate monomer selected from the group consisting of 2,2,2-trifluoroethyl (meth)acrylate, 1,1,1,3,3,-hexafluoroisopropyl (meth)acrylate, octafluoropentyl (meth)acrylate, heptadecafluoroundecyl (meth)acrylate, tridecafluorooctyl (meth)acrylate, or 2,2,3,4,4,4-hexaflurobutyl (meth)acrylate;

the antifoam component having a M w of at least 45,000 Daltons.

2. The lubricating composition of claim 1 , wherein the acrylate monomer (i) is present in an amount of about 54 wt % to about 72 wt %, and the acrylate comonomer (ii) is present in an amount of about 31 wt % to about 23 wt %.

3. The lubricating composition of claim 1 , wherein the acrylate monomer (i) comprises 2-ethylhexyl acrylate.

4. The lubricating composition of claim 1 , wherein the comonomer (ii) comprises ethyl acrylate or propyl acrylate.

5. The lubricating composition of claim 1 , wherein the acrylate monomer (i) is 2-ethylhexyl acrylate and the acrylate comonomer (ii) is ethyl acrylate.

6. The lubricating composition of claim 1 , wherein the antifoam component has a M w of from about 45,000 Da to about 80,000 Da.

7. The lubricating composition of claim 1 , wherein the antifoam component is present in the lubricating composition in an amount of at least 10 ppm.

8. The lubricating composition of claim 1 further comprising at least one further additive selected from the group consisting of dispersants, viscosity modifiers, supplemental friction modifiers, detergents, antioxidants, seal swell agents, and anti-wear agents.

9. A method of lubricating a mechanical device comprising supplying to the mechanical device the lubricating composition of claim 1 .

10. The method of claim 9 wherein the mechanical device comprises a driveline device.

11. The method of claim 10 wherein the driveline device comprises an axle, a gear, a gearbox or a transmission.

12. The method of claim 9 wherein the mechanical device comprises an internal combustion engine.

13. The method of claim 9 , wherein the mechanical device comprises a hydraulic system, a turbine system, a circulating oil system, a refrigeration lubricant system, or an industrial gear.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 17, 2019
From: KNOBLOCH, DONALD J.; HUGHES, KEVIN J.; HUSTON, MICHAEL E.; BARTON, WILLIAM R.S.; DISHONG, DENNIS M.; NICKERSON, DAVID M.
To: THE LUBRIZOL CORPORATION
Reel/Frame 050747/0024 →
Continuity (2)
Provisional Application 62437871 · Dec 22, 2016
Related Publication 20190322959A1 · Oct 24, 2019