IP Library › Granted Patent US 11,660,574
Granted Patent B2
US 11,660,574 · App. 16/885,369 · Granted May 30, 2023

Devices and methods for removing perfluorinated compounds from contaminated water

Inventors: Dibakar Bhattacharyya (Lexington, KY); Anthony Saad (Lexington, KY); Rollie Mills (Lexington, KY); Lindell Ormsbee (Lexington, KY); M. Abdul Mottaleb (Lexington, KY)
Assignee: University of Kentucky Research Foundation
B01D69/147B01D69/125B01D71/34B01J20/267B01J20/2805B01J20/28047B01J20/321B01J20/3483C02F1/285C02F1/288B01D2323/28B01D2323/30B01D2323/40B01D2323/46B01D2325/12C02F2101/36
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Quick Facts
Patent No.
US 11,660,574
App. No.
16/885,369
Granted
May 30, 2023
Kind
B2
Abstract

Purification devices and methods remove perfluorinated compounds (PFCs) from PFC-contaminated water using temperature swing adsorption and desorption.

Claims (11)

1. A purification device for removing perfluorinated compounds (PFCs) from PFC-contaminated water, comprising:

a membrane including a PFC-adsorbing temperature responsive polymer hydrogel in pores of the membrane;

a contactor in which the membrane is contacted with the PFC-contaminated water and a temperature of the PFC-adsorbing temperature responsive polymer hydrogel is raised above a predetermined temperature at which PFCs are adsorbed from the PFC-contaminated water by the PFC-adsorbing temperature responsive polymer hydrogel;

a heating device heating at least one of the PFC-contaminated water and the PFC-adsorbing temperature responsive polymer hydrogel in the contactor;

a cooling device for cooling at least one of a cooling fluid and the PFC-adsorbing temperature responsive polymer hydrogel in the contactor to release PFCs from the PFC-adsorbing temperature responsive polymer hydrogel, regenerate the PFC-adsorbing temperature responsive polymer hydrogel and collect the PFCs in the cooling fluid; and

a cooling fluid source, a PFC-contaminated water source and an inlet valve selectively connecting the cooling fluid source and the PFC-contaminated water source with the contactor.

2. The purification device of claim 1 , including a discharge valve downstream from the membrane having a first outlet for treated water and a second outlet for cooling fluid with the PFCs in the cooling fluid.

3. The purification device of claim 2 , including a drain valve downstream from the discharge valve, the drain valve having a PFC recovery outlet and a cooling fluid recycling outlet connected to the cooling fluid source.

4. The purification device of claim 1 , wherein the PFC-adsorbing temperature responsive polymer hydrogel is selected from a group of polymers consisting of poly-N-i sopropylacrylamide (PNIPAm), substituted poly-N-isopropylacrylamide, poly(vinyl ether), poly(N-vinyl caprolactam), poly(N-vinyl isobutyramide) and combinations thereof.

5. The purification device of claim 4 , wherein the membrane is selected from a group of membranes consisting of polysulfone, polyethersulfone, cellulose acetate, polypropylene, polyester, polyacrylonitrile, polyamide, polyimide, polyvinylidene fluoride (PVDF) and combinations thereof.

6. The purification device of claim 1 , wherein the membrane is selected from a group of membranes consisting of polysulfone, polyethersulfone, cellulose acetate, polypropylene, polyester, polyacrylonitrile, polyamide, polyimide, polyvinylidene fluoride (PVDF) and combinations thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 18, 2020
From: BHATTACHARYYA, DIBAKAR, DR.; SAAD, ANTHONY; MILLS, ROLLIE; ORMSBEE, LINDELL, DR.; MOTTALEB, M. ABDUL, DR.
To: UNIVERSITY OF KENTUCKY RESEARCH FOUNDATION
Reel/Frame 053520/0365 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 28, 2020
From: BHATTACHARYYA, DIBAKAR, DR.; SAAD, ANTHONY; MILLS, ROLLIE; ORMSBEE, LINDELL, DR.; MOTTALEB, M. ABDUL, DR.
To: UNIVERSITY OF KENTUCKY RESEARCH FOUNDATION
Reel/Frame 052771/0193 →
Continuity (1)
Related Publication 20210370241A1 · Dec 2, 2021
Cited By (8)
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