IP Library Granted Patent US 11,679,980
Granted Patent B2
US 11,679,980 · App. 17/252,776 · Granted Jun 20, 2023

Lithium-containing chalcophosphates for thermal neutron detection

Inventors: Mercouri G. Kanatzidis (Wilmette, IL); Daniel G. Chica (Evanston, IL); Yihui He (Evanston, IL); Duck Young Chung (Bolingbrook, IL)
Assignees: Northwestern University; UChicago Argonne, LLC
C01B25/14C30B23/00C30B29/46G01T1/24G01T3/08
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,679,980
App. No.
17/252,776
Granted
Jun 20, 2023
Kind
B2
Abstract

Inorganic compounds having the formula LiMP 2 Q 6 , where M is Ga, In, Bi, Sb, As, Al, or a combination thereof, and Q is S and/or Se, are provided. Methods and devices for detecting incident neutrons and alpha-particles using the compounds are also provided. For thermal neutron detection applications, the compounds can be enriched with lithium-6 isotope ( 6 Li) to enhance their neutron detecting capabilities.

Claims (11)

1. A method for detecting thermal neutrons or alpha particles, the method comprising:

applying an electric field across a single-crystal of a lithium-containing chalcophosphate compound having the formula LiMP 2 Q 6 , where M is Ga, In, Bi, Sb, As, Al, or a combination thereof, and Q is S, Se, or a combination thereof;

exposing the single-crystal to incident neutrons or alpha particles, wherein the single-crystal absorbs incident neutrons or alpha particles, resulting in the generation of an electrical signal; and

detecting the electrical signal.

2. The method of claim 1 , wherein the Li comprises 6 Li.

3. The method of claim 1 , wherein the compound is a quaternary compound.

4. The method of claim 3 , wherein the compound is doped with an external dopant.

5. The method of claim 4 , wherein the compound has the formula LiIn x M 1-x P 2 Se 6 , where M is the external dopant and x has a value in the range from 0.00001 to 0.05.

6. The method of claim 5 , wherein the compound is LiIn x Cd 1-x P 2 Se 6 , where Cd is the dopant and x has a value in the range from 0.00001 to 0.03.

7. The method of claim 3 having the formula LiInP 2 Se 6 .

8. The method of claim 7 , wherein the Li comprises 6 Li.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 16, 2021
From: KANATZIDIS, MERCOURI G.; HE, YIHUI; CHICA, DANIEL GEORGE
To: NORTHWESTERN UNIVERSITY
Reel/Frame 055273/0818 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 16, 2021
From: CHUNG, DUCK YOUNG
To: UCHICAGO ARGONNE, LLC
Reel/Frame 055312/0636 →
Continuity (3)
Provisional Application 62701144 · Jul 20, 2018
Provisional Application 62687430 · Jun 20, 2018
Related Publication 20210206638A1 · Jul 8, 2021