IP Library › Granted Patent US 11,739,188
Granted Patent B2
US 11,739,188 · App. 16/991,171 · Granted Aug 29, 2023

Method for manufacturing photoacoustic ultrasound generator with high laser-induced damage threshold and high-amplitude ultrasound generator manufactured using the method

Inventors: Hyoung Won Baac (Anyang-si, KR); Pil Gyu Sang (Suwon-si, KR); Jeong Min Heo (Seoul, KR)
Assignee: Research & Business Foundation Sungkyunkwan University
C08J5/18A61B5/0095B05D7/546B32B27/08B32B27/18B32B27/283C08K3/041C08L83/04B05D2201/02B05D2301/00B05D2518/12B32B2250/02B32B2250/24B32B2313/04B32B2383/00B32B2535/00B82Y20/00B82Y30/00B82Y40/00
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Quick Facts
Patent No.
US 11,739,188
App. No.
16/991,171
Granted
Aug 29, 2023
Kind
B2
Abstract

A method for manufacturing a photoacoustic ultrasound generator includes forming an uncured prepolymer polydimethylsiloxane (PDMS) film on a substrate, spraying a solution of light-absorbing nano-particles onto a surface of the uncured PDMS film, and then permeating and diffusing the light-absorbing nano-particles into the uncured PDMS film; and curing the uncured PDMS film containing the light-absorbing nano-particles distributed therein to form a composite film of nano-particles and PDMS.

Claims (12)

1. A method for manufacturing a photoacoustic ultrasound generator, the method comprising:

forming an uncured prepolymer polydimethylsiloxane (PDMS) film on a substrate;

spraying a solution of light-absorbing nano-particles onto a surface of the uncured PDMS film, and then permeating and diffusing the light-absorbing nano-particles into the uncured PDMS film; and

curing the uncured PDMS film containing the light-absorbing nano-particles distributed therein to form a composite film of nano-particles and PDMS.

2. The method of claim 1 , wherein the light-absorbing nano-particles permeated and diffused into the uncured PDMS film are dispersed such that a mean distance between the light-absorbing nano-particles in the uncured PDMS film is substantially equal to or larger than a thermal diffusion length during the temporal width of an irradiation laser pulse.

3. The method of claim 2 , wherein the PDMS composite film is obtained by dispersing the light-absorbing nano-particles in the uncured PDMS film such that the mean distance between the nano-particles is substantially equal to or larger than the thermal diffusion length, and the PDMS composite film has a laser-induced damage threshold that is higher than non-particle-PDMS composite films in which light-absorbing nano-particles are densely packed with a mean distance smaller than the thermal diffusion length.

4. The method of claim 2 , wherein the PDMS composite film is obtained by dispersing the light-absorbing nano-particles in the uncured PDMS film such that the mean distance between the nano-particles is substantially equal to or larger than the thermal diffusion length, and the PDMS composite film, in response to being irradiated with a laser pulse width of 5 to 20 ns, has a laser-induced damage threshold that exceeds 300 mJ/cm 2 .

5. The method of claim 1 , wherein the formation of the uncured PDMS film includes the application procedure of a solution of PDMS dissolved in a solvent onto the substrate using drop-casting or spin-coating methods.

6. The method of claim 1 , wherein the light-absorbing nano-particles comprise at least one nano-particle selected from the a-group consisting of metallic nano-particles, graphene flake, carbon nanotube (CNT), carbon nanofiber, and carbon nanosoot.

7. The method of claim 1 , wherein the method further comprises:

forming an additional PDMS coating layer by applying a PDMS solution on top of the PDMS composite film; and

curing the PDMS coating layer.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 12, 2020
From: BAAC, HYOUNG WON; SANG, PIL GYU; HEO, JEONG MIN
To: RESEARCH & BUSINESS FOUNDATION SUNGKYUNKWAN UNIVERSITY
Reel/Frame 053467/0624 →
Priority Claims (1)
KR 10-2019-0098955 · Aug 13, 2019 · national
Continuity (1)
Related Publication 20210047486A1 · Feb 18, 2021