IP Library Granted Patent US 11,761,913
Granted Patent B2
US 11,761,913 · App. 17/200,918 · Granted Sep 19, 2023

Transmission X-ray critical dimension (T-XCD) characterization of shift and tilt of stacks of high-aspect-ratio (HAR) structures

Inventors: Adam Ginsburg (Netanya, IL); Mark James Vermeulen (Durham, GB); Paul Anthony Ryan (Darligton, GB); Matthew Wormington (Highlands Ranch, CO)
Assignee: BRUKER TECHNOLOGIES LTD.
G01N23/201G01N23/2055G01N2223/054G01N2223/056G01N2223/6116
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Quick Facts
Patent No.
US 11,761,913
App. No.
17/200,918
Granted
Sep 19, 2023
Kind
B2
Abstract

A method for X-ray measurement includes generating and directing an X-ray beam to a sample including at least first and second layers stacked on one another, the X-ray beam incident on a sample location at which the first and second layers include respective first and second high aspect ratio (HAR) structures. X-ray scatter profiles are measured, that are emitted from the sample location in response to the X-ray beam as a function of tilt angle between the sample and the X-ray beam. A shift is estimated, between the first and second layers and a characteristic tilt of the first and second layers, based on the X-ray scatter profiles measured as a function of the tilt angle.

Claims (42)

1. A method for X-ray measurement, the method comprising:

generating and directing an X-ray beam to a sample comprising at least first and second layers stacked on one another, the X-ray beam incident on a sample location at which the first and second layers comprise respective first and second high aspect ratio (HAR) structures;

measuring X-ray scatter profiles emitted from the sample location in response to the X-ray beam as a function of tilt angle between the sample and the X-ray beam; and

estimating a shift between the first and second layers and a characteristic tilt of the first and second layers, based on the X-ray scatter profiles measured as a function of the tilt angle, including:

defining a model of an X-ray scatter profile as a function of the relative shift and the characteristic tilt; and

calculating a fit between the measured X-ray scatter profiles to the model, and extracting the estimated shift and the characteristic tilt from the fit.

2. The method according to claim 1 , wherein estimating the characteristic tilt of the first and second layers comprises estimating one or more of: an average tilt of the first and second layers, an extremum tilt of the first and second layers, and a relative tilt between the first and second layers.

3. The method according to claim 1 , wherein calculating the fit comprises applying a regression model to the measured X-ray scatter profiles.

4. The method according to claim 1 , wherein calculating the fit comprises:

fitting, to the X-ray scatter profiles, functions that comprise multiple peaks; and

solving a regression model for (i) relative intensities of the peaks and (ii) an angular position of a center peak, which best match the measured X-ray scatter profiles.

5. The method according to claim 1 , wherein calculating the fit comprises applying a non-linear regression model to the measured X-ray scatter profiles.

6. The method according to claim 1 , wherein measuring the X-ray scatter profiles comprises combining multiple X-ray scatter measurements from multiple different angular ranges into a combined measured X-ray scatter profile.

7. The method according to claim 1 , wherein the HAR structures are holes.

8. The method according to claim 4 , wherein estimating the shift and the characteristic tilt comprises deducing the shift and the characteristic tilt from the relative intensities and the angular position that best match the measured X-ray scatter profiles.

9. A method for X-ray measurement, the method comprising:

generating and directing an X-ray beam to a sample comprising at least first and second layers stacked on one another, the X-ray beam incident on a sample location at which the first and second layers comprise respective first and second high aspect ratio (HAR) structures;

measuring X-ray scatter profiles emitted from the sample location in response to the X-ray beam as a function of tilt angle between the sample and the X-ray beam; and

estimating a shift between the first and second layers and a characteristic tilt of the first and second layers, based on the X-ray scatter profiles measured as a function of the tilt angle, by applying a machine learning model to the measured X-ray scatter profiles.

10. A system for X-ray measurement, the system comprising:

an X-ray source configured to generate an X-ray beam;

optics configured to direct the X-ray beam to a sample comprising at least first and second layers stacked on one another, the X-ray beam incident on a sample location at which the first and second layers comprise respective first and second high aspect ratio (HAR) structures; and

a processor, which is configured to:

measure, using a detector, X-ray scatter profiles emitted from the sample location in response to the X-ray beam as a function of tilt angle between the sample and the X-ray beam; and

estimate a shift between the first and second layers and a characteristic tilt of the first and second layers, based on the X-ray scatter profiles measured as a function of the tilt angle, including:

defining a model of an X-ray scatter profile as a function of the relative shift and the characteristic tilt; and

calculating a fit between the measured X-ray scatter profiles to the model, and extracting the estimated shift and the characteristic tilt from the fit.

11. The system according to claim 10 , wherein the processor is configured to estimate the characteristic tilt of the first and second layers by estimating one or more of: an average tilt of the first and second layers, an extremum tilt of the first and second layers, and a relative tilt between the first and second layers.

12. The system according to claim 10 , wherein the processor is configured to calculate the fit by applying a regression model to the measured X-ray scatter profiles.

13. The system according to claim 10 , wherein the processor is configured to calculate the fit by:

fitting, to the X-ray scatter profiles, functions that comprise multiple peaks; and

solving a regression model for (i) relative intensities of the peaks and (ii) an angular position of a center peak, which best match the measured X-ray scatter profiles.

14. The system according to claim 10 , wherein the processor is configured to calculate the fit by applying a non-linear regression model to the measured X-ray scatter profiles.

15. The system according to claim 10 , wherein the processor is configured to measure the X-ray scatter profiles by combining multiple X-ray scatter measurements from multiple different angular ranges into a combined measured X-ray scatter profile.

16. The system according to claim 10 , wherein the HAR structures are holes.

17. The system according to claim 13 , wherein the processor is configured to deduce the shift and the characteristic tilt from the relative intensities and the angular position that best match the measured X-ray scatter profiles.

18. A system for X-ray measurement, the system comprising:

an X-ray source configured to generate an X-ray beam;

optics configured to direct the X-ray beam to a sample comprising at least first and second layers stacked on one another, the X-ray beam incident on a sample location at which the first and second layers comprise respective first and second high aspect ratio (HAR) structures; and

a processor, which is configured to:

measure, using a detector, X-ray scatter profiles emitted from the sample location in response to the X-ray beam as a function of tilt angle between the sample and the X-ray beam; and

estimate a shift between the first and second layers and a characteristic tilt of the first and second layers, based on the X-ray scatter profiles measured as a function of the tilt angle, by applying a machine learning model to the measured X-ray scatter profiles.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 15, 2021
From: GINSBURG, ADAM; VERMEULEN, MARK JAMES; RYAN, PAUL ANTHONY; WORMINGTON, MATTHEW
To: BRUKER TECHNOLOGIES LTD.
Reel/Frame 055585/0499 →
Continuity (2)
Provisional Application 63019498 · May 4, 2020
Related Publication 20210341397A1 · Nov 4, 2021