IP Library Granted Patent US 11,782,007
Granted Patent B2
US 11,782,007 · App. 16/986,340 · Granted Oct 10, 2023

CO

Inventors: Jeffrey Frederick Rhoads (West Lafayette, IN); George Tsu-Chih Chiu (West Lafayette, IN); Bryan W Boudouris (West Lafayette, IN); Nikhil Bajaj (West Lafayette, IN); Allison Kelly Murray (West Lafayette, IN); Zachary A Siefker (West Lafayette, IN); Xikang Zhao (West Lafayette, IN)
Assignee: Purdue Research Foundation
G01N27/127B32B9/007B32B9/045B32B27/302C01B32/174C08G73/0206C08L71/02C08L79/02G01N27/126B82Y15/00B82Y30/00G01N33/004
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Quick Facts
Patent No.
US 11,782,007
App. No.
16/986,340
Granted
Oct 10, 2023
Kind
B2
Abstract

The present disclosure relates to a novel composite film configured for CO 2 sensing, and the method of making and using the novel composite film. The novel composite film comprises a carbon nanotube film and a CO 2 absorbing layer deposited on the carbon nanotube film, wherein the CO 2 absorbing layer comprises a mixture of a branched polyethylenimine, a polyethylene glycol, and poly[1-(4-vinylbenzyl)-3-methylimidazolium tetrafluoroborate] of formula I: wherein n ranges from 10-300.

Claims (8)

1. A composite film configured for CO 2 sensing, wherein the composite film comprises a carbon nanotube film and a CO 2 absorbing layer deposited on the carbon nanotube film, wherein the CO 2 absorbing layer comprises a mixture of a branched polyethylenimine, a polyethylene glycol, and poly[1-(4-vinylbenzyl)-3-methylimidazolium tetrafluoroborate] of formula I:

wherein n ranges from 10-300.

2. The composite film of claim 1 , wherein the thickness of said carbon nanotube film is 10-500 nm, the thickness of said CO 2 absorbing layer is 100-1000 nm.

3. The composite film of claim 1 , wherein said carbon nanotube film comprises chlorosulfonic acid.

4. The composite film of claim 1 , wherein said branched polyethylenimine has a molar molecular weight of 10 kg/mol, wherein said polyethylene glycol has a molar molecular weight of 0.5 kg/mol to 50 kg/mol.

5. The composite film of claim 1 , wherein said branched polyethylenimine has a weight percentage of 40-60% of the total weight of the CO 2 absorbing layer.

6. The composite film of claim 1 , wherein said polyethylene glycol has a weight percentage of 40-60% of the total weight of the CO 2 absorbing layer.

7. The composite film of claim 1 , wherein said poly[1-(4-vinylbenzyl)-3-methylimidazolium tetrafluoroborate] has a weight percentage of 1-5% of the total weight of the CO 2 absorbing layer.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 14, 2024
From: PURDUE UNIVERSITY
To: US DEPARTMENT OF ENERGY
Reel/Frame 067411/0121 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 15, 2023
From: CHIU, GEORGE TSU-CHIH; RHOADS, JEFFREY FREDERICK; BOUDOURIS, BRYAN WILLIAM; BAJAJ, NIKHIL; MURRAY, ALLISON KELLY; SIEFKER, ZACHARY A; ZHAO, XIKANG
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 064595/0518 →
Continuity (2)
Provisional Application 62884390 · Aug 8, 2019
Related Publication 20210041387A1 · Feb 11, 2021