IP Library › Granted Patent US 11,858,817
Granted Patent B2
US 11,858,817 · App. 17/104,676 · Granted Jan 2, 2024

Nanodiamond reduction photochemistry

Inventors: Bradford B. Pate (Arlington, VA); William Maza (Camp Spring, MD); Vanessa Breslin (Alexandria, VA); Paul A. DeSario (Alexandria, VA); Tatyana I. Feygelson (Springfield, VA); Albert Epshteyn (Potomac, MD); Jeffrey C. Owrutsky (Silver Spring, MD); Carlos Hangarter (Alexandria, VA)
Assignee: The Government of the United States of America, as represented by the Secretary of the Navy
C01B32/28B01J19/123B01J2219/089B01J2219/1203B82Y30/00B82Y40/00C01P2004/64
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Quick Facts
Patent No.
US 11,858,817
App. No.
17/104,676
Granted
Jan 2, 2024
Kind
B2
Abstract

Disclosed is a method of irradiating a composition having water and hydrogen-terminated nanodiamonds with light that generates water-solvated electrons from the nanodiamonds. The method can be used to degrade fluoroalkyl compounds such as perfluorooctane sulfonate.

Claims (13)

1. A method comprising:

providing a composition comprising:

water; and

hydrogen-terminated nanodiamonds;

wherein the nanodiamonds have an average size of less than 10 nm; and

irradiating the composition with light having a wavelength that generates water-solvated electrons from the nanodiamonds.

2. The method of claim 1 , wherein the wavelength is 225-295 nm.

3. The method of claim 1 , wherein the composition is suspected of containing a fluoroalkyl compound.

4. The method of claim 3 , wherein the fluoroalkyl compound is a perfluoroalkyl surfactant, a perfluoroalkane sulfonate, a perfluoroalkyl acid, perfluorooctane sulfonate, or perfluorooctyl acid.

5. The method of claim 3 , further comprising:

monitoring the amount of the fluoroalkyl compound in the composition.

6. The method of claim 5 , further comprising:

continuing the irradiation of the composition until the amount of the fluoroalkyl compound in the composition has been reduced to a target amount.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 5, 2021
From: PATE, BRADFORD B; DESARIO, PAUL A; FEYGELSON, TATYANA I; EPSHTEYN, ALBERT; OWRUTSKY, JEFFREY C; HANGARTER, CARLOS; MAZA, WILLIAM; BRESLIN, VANESSA
To: THE GOVERNMENT OF THE UNITED STATES, AS RESPRESENTED BY THE SECRETARY OF THE NAVY
Reel/Frame 055160/0783 →
Continuity (2)
Provisional Application 62940611 · Nov 26, 2019
Related Publication 20210163298A1 · Jun 3, 2021
Cited By (8)
US 12,275,661 US 12,304,850 US 12,351,498 US 12,473,222 US 12,515,974 US 12,534,390 US 12,545,601 US 12,655,051