IP Library › Granted Patent US 11,866,557
Granted Patent B2
US 11,866,557 · App. 16/932,747 · Granted Jan 9, 2024

Composite articles with reduced discoloration and methods of promoting or reducing color changes in composite articles

Inventors: Peng Cheng (Forest, VA); Hongyu Chen (Forest, VA); Liqing Wei (Forest, VA); Ruomiao Wang (Forest, VA)
Assignee: Hanwha Azdel, Inc.
C08J5/10C08J5/043C08K3/016C08K3/22C08K5/005C08K5/13C08J2323/06C08J2323/12C08K2003/2224C08K2003/2227
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Quick Facts
Patent No.
US 11,866,557
App. No.
16/932,747
Granted
Jan 9, 2024
Kind
B2
Abstract

Composite articles that can resist discoloration or color changes are described. In some instances, the composite articles can include a compounded material that is substantially free of an antioxidant that changes from a first color to a second color upon exposure to an environment comprising an oxidizing agent. The composite articles can be flame retardant and may provide sound reduction as well.

Claims (12)

1. A method comprising producing a flame retardant thermoplastic fiber-reinforced porous core by combining reinforcing fibers, a first thermoplastic polyolefin material and a compounded material comprising a flame retardant compounded with a second thermoplastic polyolefin material, wherein the flame retardant thermoplastic fiber-reinforced porous core comprises a web formed from the reinforcing fibers held in place by the first thermoplastic material and the second thermoplastic material, wherein the compounded material comprises an antioxidant that turns from a first color to a second color upon exposure to an environment comprising oxidizing agent present at a first concentration, and wherein the antioxidant turns from the second color back to the first color upon exposure to an environment comprising oxidizing agent present at a second concentration lower than the first concentration, and wherein the flame retardant thermoplastic fiber-reinforced porous core is stored in the environment comprising oxidizing agent present at or below the second concentration to maintain the flame retardant thermoplastic fiber-reinforced porous core at the first color.

2. The method of claim 1 , wherein the antioxidant comprises a phenolic antioxidant.

3. The method of claim 1 , wherein the first thermoplastic polyolefin material is polypropylene.

4. The method of claim 1 , wherein the first thermoplastic polyolefin material is polyethylene.

5. The method of claim 1 , wherein the first thermoplastic polyolefin material consists of polypropylene.

6. The method of claim 5 , wherein the second thermoplastic polyolefin material is polypropylene.

7. A method comprising:

producing a flame retardant thermoplastic fiber-reinforced porous core by combining reinforcing fibers, a first thermoplastic material and a compounded material comprising a flame retardant compounded with a second thermoplastic material, wherein the flame retardant thermoplastic fiber-reinforced porous core comprises a web formed from the reinforcing fibers held in place by the first thermoplastic material and the second thermoplastic material, wherein the compounded material comprises an antioxidant that turns from a first color to a second color upon exposure to an environment comprising oxidizing agent present at a first concentration, and wherein the antioxidant turns from the second color back to the first color upon exposure to an environment comprising oxidizing agent present at a second concentration lower than the first concentration, wherein the flame retardant thermoplastic fiber-reinforced porous core is stored in the environment comprising oxidizing agent present at or below the second concentration to maintain the flame retardant thermoplastic fiber-reinforced porous core at the first color; and

storing the produced flame retardant thermoplastic fiber-reinforced porous core layer in the environment comprising NO X present at the first concentration for at least 24 hours to turn the antioxidant in the flame retardant thermoplastic fiber-reinforced porous core from the first color to the second color.

8. The method of claim 7 , further comprising removing the flame retardant thermoplastic fiber-reinforced porous core layer from the environment comprising NO X present at the first concentration and storing the flame retardant thermoplastic fiber-reinforced porous core layer in the environment comprising NO X at or below the second concentration to turn the antioxidant in the flame retardant thermoplastic fiber-reinforced porous core from the second color to the first color.

9. The method of claim 1 , wherein the first thermoplastic polyolefin material comprises polypropylene and the reinforcing fibers comprise glass fibers.

10. The method of claim 9 , wherein the flame retardant comprises magnesium hydroxide, aluminum hydroxide or both, wherein the second thermoplastic polyolefin material comprises polypropylene and wherein the flame retardant thermoplastic fiber-reinforced porous core meets ASTM E84, Class A specification.

Continuity (2)
Provisional Application 62875891 · Jul 18, 2019
Related Publication 20210130558A1 · May 6, 2021