IP Library › Granted Patent US 11,905,227
Granted Patent B2
US 11,905,227 · App. 17/284,714 · Granted Feb 20, 2024

Oligomerization of olefins

Inventors: Shiwen Li (Etterbeek, BE); Alan A. Galuska (Ellijay, GA); Teng Xu (Houston, TX)
Assignee: ExxonMobil Chemical Patents Inc.
C07C2/12B01J29/7046B01J29/7096B01J29/7292B01J2229/18B01J2229/36B01J2229/37B01J2229/42C07C2529/70
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,905,227
App. No.
17/284,714
Granted
Feb 20, 2024
Kind
B2
Abstract

A process for olefin oligomerization can include contacting a feedstock comprising C n and C 2n olefins/paraffins under oligomerization conditions in the presence of an oligomerization catalyst, wherein n is 2 to 15; and recovering an oligomeric product comprising C 3n oligomers having a branching index of less than 2.1. Optionally, the feedstock can further comprise C 3n olefins/paraffins.

Claims (16)

1. A process for olefin oligomerization, the process comprising:

contacting a feedstock comprising C n and C 2n olefins/paraffins under oligomerization conditions in a reactor in the presence of an oligomerization catalyst wherein the catalyst comprises a ZSM-23 catalyst having no amine treatment, wherein n is 4 and the feedstock comprises 45 wt % to 75 wt % C 4 and 15 wt % to 50 wt % C 8 ;

forming an oligomeric product comprising C 12 oligomers, wherein the C 12 oligomers have a branching index of less than 2.1; and

recycling at least a first portion of the oligomeric product to the reactor.

2. The process of claim 1 , wherein the catalyst comprises a a Si/Al 2 molar ratio of 20 to 60.

3. The process of claim 1 , wherein the catalyst comprises a Si/Al/Ti ZSM-23 catalyst having no amine treatment, a Si/Al 2 molar ratio of 20 to 60, and a Ti/Al molar ratio of 0.1 to 3.

4. The process of claim 1 , wherein the catalyst is impregnated with a metal selected from the group consisting of yttrium, tungsten, vanadium, molybdenum, rhenium, nickel, cobalt, chromium, manganese, lanthanum, lanthanides, platinum, palladium, and any combination thereof.

5. The process of claim 1 , wherein the process further comprises treating the catalyst before contacting with the feedstock, wherein the treatment is selected from the group consisting of steaming, acid washing, depositing coke, and any combination thereof.

6. The process of claim 1 , wherein the catalyst is an extrudate comprising a binder at 1 wt % to 90 wt % and the catalyst at 10 wt % to 99 wt %.

7. The process of claim 1 , wherein the oligomerization conditions are a temperature of 150° C. to 350° C. and a weight hourly space velocity of 0.1 hr −1 to 30 hr −1 .

8. The process of claim 1 , wherein the branching index is 1.0 to 1.5.

9. The process of claim 1 , further comprising:

converting a portion of the oligomeric product to aldehydes and/or alcohols.

10. The process of claim 1 , further comprising:

converting a portion of the oligomeric product to alcohols; and

converting the alcohols to surfactants.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 12, 2021
From: LI, SHIWEN; GALUSKA, ALAN A.; XU, TENG
To: EXXONMOBIL CHEMICAL PATENTS INC.
Reel/Frame 055895/0576 →
Priority Claims (1)
EP 18205815 · Nov 13, 2018 · regional
Continuity (2)
Provisional Application 62746845 · Oct 17, 2018
Related Publication 20210355048A1 · Nov 18, 2021