Preparation method and product of thermoplastic carbon fiber fabric prepreg
A preparation method and a product of thermoplastic carbon fiber fabric prepreg are provided. The preparation method includes: covering a thermoplastic polyimide non-woven fabric on a carbon fiber fabric to obtain a laminated structure, pressing the laminated structure, then spraying polyphenylene sulfide nanoparticles onto the thermoplastic polyimide non-woven fabric, and performing a two-stage hot melting preparation process which includes: in a first stage, heating up to make the polyphenylene sulfide nanoparticles be melted and infiltrate and keeping a hot melting time of 5-10 min; and in a second stage, heating up to make the thermoplastic polyimide non-woven fabric be melted and infiltrate into the carbon fiber fabric and cooling down after a duration of heat preservation to prepare the thermoplastic carbon fiber fabric prepreg. The thermoplastic carbon fiber fabric prepreg prepared by the two-stage hot melting has high strength and may be stored for a long period.
1. A method for preparing a thermoplastic carbon fiber fabric prepreg, comprising the following steps:
covering a carbon fiber fabric with a thermoplastic polyimide non-woven fabric to obtain a laminated structure, pressing the laminated structure together, then spraying polyphenylene sulfide nanoparticles onto the thermoplastic polyimide non-woven fabric, and carrying out a two-stage hot melting preparation process;
wherein the two-stage hot melting preparation process comprises: firstly, in a first stage, heating up to make the polyphenylene sulfide nanoparticles be melted and infiltrated into the carbon fiber fabric uniformly through pores on the thermoplastic polyimide non-woven fabric, and keeping a hot melting time of 5-10 minutes (min); and afterwards, in a second stage, heating up to make the thermoplastic polyimide non-woven fabric be melted and infiltrated into the carbon fiber fabric and cooling down after a duration of heat preservation to thereby prepare the thermoplastic carbon fiber fabric prepreg.
2. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein the carbon fiber fabric has a thickness of 0.05-0.2 mm and is made of a continuous carbon fiber tow of 3K, 6K or 12K.
3. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein carbon fibers in the carbon fiber fabric comprise any one of T300, T700, T800 and T1000 carbon fibers.
4. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein the thermoplastic polyimide non-woven fabric has a thickness of 0.05-0.1 mm and a gram weight of 20-50 grams per square meter (g/m 2 ).
5. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein particle sizes of polyphenylene sulfide nanoparticles are 20-50 nm.
6. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein an amount of the polyphenylene sulfide nanoparticles sprayed on thermoplastic polyimide non-woven fabric is 3-5 g/m 2 .
7. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein the heating up in the first stage is to rise the temperature up to 290-300° C.
8. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein the heating up in the second stage is to rise the temperature to 400-420° C.
9. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein the duration of heat preservation is 60-90 min.
10. The method for preparing the thermoplastic carbon fiber fabric prepreg according to claim 1 , wherein the cooling down is to cool the thermoplastic carbon fiber fabric prepreg to below 50° C.