IP Library › Granted Patent US 11,993,821
Granted Patent B2
US 11,993,821 · App. 16/055,266 · Granted May 28, 2024

Co-crystallized sweeteners

Inventors: Christopher M. Gregson (Princeton, NJ); Matthew P. Sillick (Belle Mead, NJ); Jérôme Barra (Geneva, CH); Angela Di Pietro (Geneva, CH)
Assignee: Firmenich SA
C13B50/002A21D2/181A23C9/1307A23C9/156A23G3/36A23G4/06A23L2/60A23L5/00A23L27/31A23L27/33A23L27/60A23L29/30A23P10/20A23P10/22C13B50/004A23V2002/00A23V2250/628A23V2300/31A23V2300/36
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Quick Facts
Patent No.
US 11,993,821
App. No.
16/055,266
Granted
May 28, 2024
Kind
B2
Abstract

Sweeteners made from the co-crystallization of 3-(4-amino-2,2-dioxide-1H-benzo[c][1,2,6]thiadiazin-5-yloxy)-2′,2′-dimethyl-N-propylpropanamide (Compound I) having the structure: or salt thereof, with sugar in various ratios. The sugar co-crystallized sweeteners are very soluble in water and have no dusting problems.

Claims (20)

1. A process for forming a co-crystallized composition, wherein the process comprises the steps of:

a. mixing a sugar with water with agitation in the presence of a base to form a sugar composition;

b. heating the sugar composition to evaporate at least a portion of the water and form a sugar syrup;

c. incorporating into the sugar syrup a dry powder of a sweetener to form a uniform dispersion, wherein the sweetener is 3-(4-amino-2,2-dioxide-1H-benzo[c][1,2,6]-thiadiazin-5-yloxy)-2′,2′-dimethyl-N-propylpropanamide;

d. removing the uniform dispersion from the heat; and

e. allowing the uniform dispersion to cool with vigorous agitation to form a co-crystallized composition comprising the sugar and the sweetener.

2. The process of claim 1 , wherein the sugar is selected from the group consisting of sucrose, fructose and glucose.

3. The process of claim 2 , wherein the sugar is sucrose.

4. A method of sweetening a product, the method comprising by including the co-crystallized composition formed by the process of claim 1 in an amount effective to sweeten the product.

5. The method of claim 4 , wherein the product is a beverage selected from the group consisting of carbonated soft drinks, powdered soft drinks, coffees, teas, juices, sweetened and flavored waters, sport/energy/health drinks, alcoholic beverages, beverages processed with heating and hot-filled packaging and cold-filled beverages.

6. The method of claim 4 , wherein the product is a fluid dairy product selected from the group consisting of non-frozen, partially frozen and frozen milks, ice creams, sorbets and yogurts.

7. The method of claim 4 , wherein the product is a condiment selected from the group consisting of ketchup, mayonnaise, salad dressing, Worcestershire sauce, tomato sauce, chili sauce, and mustard.

8. The method of claim 4 , wherein the product is a baked good selected from the group consisting of cakes, cookies, pastries, breads and donuts.

9. The method of claim 4 , wherein the product is a frosting.

10. The method of claim 4 , wherein the product is a bakery filling of a low or neutral pH filling, a high, medium or low solids filling, a fruit or milk based filling, a hot or cold make-up filling and a non-fat to full-fat filling.

11. The method of claim 4 , wherein the product is a candy or chewing gum.

12. The method of claim 4 , wherein the product is a table-top sweetener.

13. A composition comprising the co-crystallized composition formed according to the process of claim 1 .

14. The method of claim 1 , further comprising sieve-screening the co-crystallized composition.

15. The method of claim 1 , wherein the co-crystallized composition comprises from 1% to 5% of the sweetener, based on the weight of the co-crystallized composition.

Continuity (3)
Continuation 14654841
Provisional Application 61745412 · Dec 21, 2012
Related Publication 20180363074A1 · Dec 20, 2018