IP Library › Granted Patent US 12,000,050
Granted Patent B2
US 12,000,050 · App. 17/910,867 · Granted Jun 4, 2024

Dielectric coating

Inventor: Sébastien Le Craz (Liège, BE)
Assignee: ArcelorMittal
C23C18/122C23C18/1241C23C18/1254C23C18/127H01L31/022425H01L31/0392
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Quick Facts
Patent No.
US 12,000,050
App. No.
17/910,867
Granted
Jun 4, 2024
Kind
B2
Abstract

A sol composition for producing dielectric layers on a metallic substrate including 10 to 30%, by weight of the sol composition, of a precursor including a trialkoxysilane, 10 to 40%, by weight of the sol composition, of titanium dioxide particles whose median size is below 500 nm, 4.5 to 36%, by weight of the sol composition, of silica particles whose particle size distribution D90 is below 100 nm, 5 to 15%, by weight of the sol composition, of a solvent capable of making the precursor miscible in water, 0.1 to 2%, by weight of the sol composition, of an acidic catalyst, the remainder being water.

Claims (14)

1. A sol composition for producing dielectric layers on a metallic substrate comprising:

to 30%, by weight of the sol composition, of a precursor including a trialkoxysilane;

to 40%, by weight of the sol composition, of titanium dioxide particles whose median size is below 500 nm;

4.5 to 36%, by weight of the sol composition, of silica particles whose particle size distribution D90 is below 100 nm;

to 15%, by weight of the sol composition, of a solvent capable of making the precursor miscible in water; and

to 2%, by weight of the sol composition, of an acidic catalyst;

a remainder being water.

2. The sol composition as recited in claim 1 wherein the trialkoxysilane is chosen from the group consisting of methyltrialkoxysilanes, ethyltrialkoxysilanes and propyltrialkoxysilanes.

3. The sol composition as recited in claim 1 wherein the precursor is a mixture of at least one tetraalkoxysilane and at least one trialkoxysilane.

4. The sol composition as recited in claim 1 wherein the content of the precursor is comprised between 15 to 25% by weight of the sol composition.

5. The sol composition as recited in claim 1 wherein the solvent is chosen from the group consisting of alcohols, ketones and mixtures thereof.

6. The sol composition as recited in claim 1 wherein the size of the titanium dioxide particles is comprised between 200 and 1000 nm.

7. The sol composition as recited in claim 1 wherein the titanium dioxide particles are coated with 2 to 6% of alumina by weight of TiO 2 particles.

8. The sol composition as recited in claim 1 wherein the silica particles are in the form of a mix of silica particles of two different size ranges: a first range between 50 and 120 nm and a second range between 3 and 25 nm.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 26, 2022
From: LE CRAZ, SEBASTIEN
To: ARCELORMITTAL
Reel/Frame 061544/0652 →
Priority Claims (1)
WO PCT/IB2020/052462 · Mar 18, 2020 · international
Continuity (1)
Related Publication 20230113179A1 · Apr 13, 2023