IP Library › Granted Patent US 12,007,372
Granted Patent B2
US 12,007,372 · App. 17/258,996 · Granted Jun 11, 2024

Gas chromatograph device and analysis support method for gas chromatograph device

Inventors: Yasuhiro Kimoto (Kyoto, JP); Takuya Isoi (Kyoto, JP)
Assignee: SHIMADZU CORPORATION
G01N30/78G01N2030/025G06F3/04847
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Quick Facts
Patent No.
US 12,007,372
App. No.
17/258,996
Granted
Jun 11, 2024
Kind
B2
Abstract

A gas chromatograph device ( 100 ) includes a calculator ( 2 ) configured to acquire information on conduits ( 36 ) between a branch unit ( 33 ) and detectors ( 34 ) and information that identifies types of the detectors connected to the conduits, the calculator being configured to calculate at least one of gas flow rates in the conduits, gas linear velocities in the conduits, or a pressure in the branch unit based on the acquired information.

Claims (40)

1. A gas chromatograph device comprising:

a sample introduction unit configured to send a carrier gas and a sample gas;

a column configured to separate components of the sample gas introduced from the sample introduction unit;

a branch unit provided downstream of the column where a conduit of the sample gas is branched into a plurality of branched conduits;

a plurality of detectors connected to the branch unit; and

a calculator configured to acquire;

information on a connection of the plurality of branched conduits between the branch unit and the plurality of detectors; and

information for identifying types of the plurality of detectors connected to the plurality of branched conduits,

the calculator being configured to calculate at least one of;

gas flow rates in the plurality of branched conduits,

gas linear velocities in the plurality of branched conduits, or

a pressure in the branch unit based on the acquired information,

wherein the branch unit is connected to the plurality of detectors via a plurality of resistance tubes as the plurality of branched conduits and is configured to distribute the sample gas from the column to each of the plurality of resistance tubes, and

wherein the calculator is further configured to calculate a branch ratio of a gas distributed to each of the plurality of resistance tubes connected to the plurality of detectors based on both information of the plurality of resistance tubes and information that identifies types of the plurality of detectors respectively connected to the plurality of resistance tubes.

2. The gas chromatograph device according to claim 1 , wherein

the calculator is configured to:

acquire information on lengths and inner diameters of the plurality of branched conduits as the information on the plurality of branched conduits;

acquire information on pressures in the plurality of detectors connected to the plurality of branched conduits based on the information that identifies the types of the plurality of detectors; and

acquire information on an analysis condition including any one of the gas flow rates, the gas linear velocities, and the pressure in the branch unit so as to calculate any other of the gas flow rates, the gas linear velocities, and the pressure in the branch unit based on the acquired information.

3. The gas chromatograph device according to claim 1 , further comprising:

a display configured to display an interface screen configured to receive an information input; wherein

the calculator is configured to cause the display to display the interface screen configured to allow the information on the plurality of branched conduits and the information that identifies the types of the plurality of detectors connected to the plurality of branched conduits to be entered in association with each other for respective conduits of the plurality of branched conduits branched from the branch unit.

4. The gas chromatograph device according to claim 3 , wherein the calculator is configured to cause the display to display the interface screen including a first entry field for entering the information on the plurality of branched conduits and a second entry field for entering the information that identifies the types of the plurality of detectors connected to the plurality of branched conduits identified by the first entry field.

5. The gas chromatograph device according to claim 4 , further comping:

a plurality of connectors configured to allow the plurality of branched conduits from the branch unit and the plurality of detectors to be connected thereto; wherein

the calculator is configured to selectably display the types of the plurality of detectors connected to the plurality of connectors in the second entry field.

6. The gas chromatograph device according to claim 1 , wherein

the branch unit is connected to one of the plurality of detectors via a second column a one of the plurality of branched conduits, the second column being provided separately from a first column on an upstream side thereof; and

the calculator is configured to calculate at least one of a gas flow rate in the second column, a gas linear velocity in the second column, or the pressure in the branch unit for achieving a flow rate or a linear velocity specified as an analysis condition based on information on the second column and information that identifies a type of detector connected to the second column.

7. An analysis support method for a gas chromatograph device comprising a branch unit provided downstream of a column configured to separate components of a sample gas introduced from a sample introduction unit where a conduit of the sample gas is branched into a plurality of branched conduits, and a plurality of detectors connected to the branch unit, the analysis support method comprising:

acquiring information on a connection of the plurality of branched conduits between the branch unit and the plurality of detectors; and

acquiring information for identifying types of the plurality of detectors connected to the plurality of branched conduits; and

calculating at least one of:

gas flow rates in the plurality of branched conduits,

gas linear velocities in the plurality of branched conduits, or

a pressure in the branch unit based on the acquired information,

wherein the branch unit is connected to the plurality of detectors via a plurality of resistance tubes as the plurality of branched conduits, and

wherein the analysis support method further comprises:

distributing the sample gas from the column to each of the plurality of resistance tubes, and

calculating a branch ratio of a gas distributed to each of the plurality of resistance tubes connected to the plurality of detectors based on both information of the plurality of resistance tubes and information that identifies types of the plurality of detectors respectively connected to the plurality of resistance tubes.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 8, 2021
From: KIMOTO, YASUHIRO; ISOI, TAKUYA
To: SHIMADZU CORPORATION
Reel/Frame 054863/0539 →
Continuity (1)
Related Publication 20210311000A1 · Oct 7, 2021