Systems and methods for additive manufacturing of metal nitride ceramics
Described herein are embodiments directed to additive manufacturing (AM), including three-dimensional (3D) printing, of metal nitride ceramics. In some embodiments herein, AM may comprise powder bed fusion (PBF) techniques. Also described herein are metal nitride ceramic components formed by AM techniques and methods for forming metal nitrides capable of being used in AM processes.
1. A process for producing a metal nitride ceramic component, the process comprising:
preparing a metal nitride powder by contacting metal powder with a microwave plasma, the microwave plasma generated using a nitrogen-containing plasma gas;
directing a laser beam or an electron beam to a powder consisting essentially of the metal nitride powder within a process chamber; and
maintaining the process chamber at a temperature of 1,200° C. or less throughout the process.
2. The process of claim 1 , wherein the process comprises electron beam melting (EBM) or selective laser melting (SLM) of the metal nitride powder.
3. The process of claim 1 , wherein the metal nitride powder comprises a particle size range between about 15-45 microns or about 45-106 microns.
4. The process of claim 1 , wherein the metal nitride component has a density percent of 95% or higher under an optical microscope.
5. The process of claim 1 , wherein the metal nitride ceramic component consists essentially of metal nitride.
6. The process of claim 5 , wherein the metal nitride comprises titanium nitride.
7. The process of claim 1 , wherein the metal nitride powder comprises titanium nitride powder.