IP Library Granted Patent US 12,055,889
Granted Patent B2
US 12,055,889 · App. 17/196,555 · Granted Aug 6, 2024

Toner

Inventors: Koji Nishikawa (Shizuoka, JP); Yasuhiro Hashimoto (Shizuoka, JP); Yuujirou Nagashima (Shizuoka, JP); Tomoya Nagaoka (Tokyo, JP)
Assignee: CANON KABUSHIKI KAISHA
G03G9/08773G03G9/08724G03G9/08782
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Quick Facts
Patent No.
US 12,055,889
App. No.
17/196,555
Granted
Aug 6, 2024
Kind
B2
Abstract

A toner comprising: a toner particle that comprises a core particle comprising a binder resin, and a shell layer comprising a thermoplastic resin on a surface of the core particle; and organosilicon polymer particles on a surface of the toner particle, wherein a peak top molecular weight of the thermoplastic resin, according to measurement by gel permeation chromatography, is 30000 to 500000, a number-average primary particle diameter of the organosilicon polymer particles is 10 nm to 500 nm, and an absolute value of a difference (ΔSP) between an SP value (SP Si ) of the organosilicon polymer particles and an SP value (SP Sh ) of the thermoplastic resin present in the shell layer is not more than 2.30.

Claims (16)

1. A toner, comprising:

a toner particle that comprises a core particle, said core particle comprising a binder resin;

a shell layer on a surface of the core particle, said shell layer comprising a thermoplastic resin; and

organosilicon polymer particles on a surface of the toner particle, wherein

the thermoplastic resin is a polymer of styrene and at least one member selected from the group consisting of acrylic polymerizable monomers and methacrylic polymerizable monomers,

the thermoplastic resin has a peak top molecular weight of 30000 to 500000 measured by gel permeation chromatography,

the organosilicon polymer particles have a number-average primary particle diameter of 10 to 500 nm, and

an absolute value of a difference between SP values of the organosilicon polymer particles and the thermoplastic resin in the shell layer is not more than 2.30.

2. The toner according to claim 1 , wherein a glass transition temperature of the thermoplastic resin is 40 to 75° C. measured by differential scanning calorimetry.

3. The toner according to claim 1 , wherein the shell layer has an average thickness of 5 to 250 nm.

4. The toner according to claim 1 , wherein a ratio of coverage of the core particle by the shell layer is at least 30%.

5. The toner according to claim 1 , wherein a content of the organosilicon polymer particles in the toner is 0.3 to 10.0 mass %.

6. The toner according to claim 1 , wherein the organosilicon polymer particles have a structure in which a silicon atom and an oxygen atom are bonded in alternation, and have a T3 unit structure represented by R 1 —SiO 3/2 where R 1 represents a C 1-6 alkyl group or phenyl group, and

a proportion of a peak area originating with silicon having the T3 unit structure to a total peak area originating with all silicon element contained in the organosilicon polymer particles is 0.50 to 1.00 in 29 Si-NMR measurement.

7. The toner according to claim 1 , wherein an attachment index for the organosilicon polymer particles on a polycarbonate film is not more than 4.5 determined by (area ratio A for the organosilicon polymer particles transferred to the polycarbonate film/ratio of coverage B by the organosilicon polymer particles over the toner particle surface)×100.

8. The toner according to claim 1 , wherein a dispersity evaluation index for the organosilicon polymer particles on the toner surface is 0.5 to 2.0.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 2, 2021
From: NISHIKAWA, KOJI; HASHIMOTO, YASUHIRO; NAGASHIMA, YUUJIROU; NAGAOKA, TOMOYA
To: CANON KABUSHIKI KAISHA
Reel/Frame 057987/0894 →
Priority Claims (1)
JP 2020-045834 · Mar 16, 2020 · national
Continuity (1)
Related Publication 20210286281A1 · Sep 16, 2021