IP Library Granted Patent US 12,064,533
Granted Patent B2
US 12,064,533 · App. 18/324,951 · Granted Aug 20, 2024

Synthetic hydrogel composite

Inventors: Benjamin J. Wiley (Durham, NC); Huayu Tong (Durham, NC); Jiacheng Zhao (Durham, NC)
Assignee: Duke University
A61L27/48A61F2/30756A61F2/3094A61L27/52A61F2002/30024A61F2002/30471A61F2002/30761A61L2400/12A61L2430/06
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Quick Facts
Patent No.
US 12,064,533
App. No.
18/324,951
Granted
Aug 20, 2024
Kind
B2
Abstract

Cellulose-reinforced hydrogels may include a cellulose nanofiber network and an interstitial hydrogel portion within interstitial regions of the cellulose nanofiber network, the interstitial hydrogel portion comprising polyvinyl alcohol (PVA), wherein the hydrogel component has a crystallinity of 20% or greater.

Claims (17)

1. An articular cartilage implant, comprising:

an implant body having a top bearing surface;

an anchoring base; and

a cellulose-reinforced hydrogel comprising:

a cross-linked cellulose nanofiber network secured over the top bearing surface of the implant body; and

an interstitial hydrogel portion infiltrated within interstitial regions of the cross-linked cellulose nanofiber network,

wherein the interstitial hydrogel portion is annealed such that a crystalline content of the annealed interstitial hydrogel portion has a crystallinity of 20% or greater,

wherein the cellulose-reinforced hydrogel comprises at least 20% by weight of water,

wherein the cellulose-reinforced hydrogel has a tensile strength exceeding 40 MPa,

wherein the cross-linked cellulose nanofiber network comprises bacterial cellulose (BC).

2. The articular cartilage implant of claim 1 , wherein the interstitial hydrogel portion comprises polyvinyl alcohol (PVA).

3. The articular cartilage implant of claim 1 , wherein the cross-linked cellulose nanofiber network is chemically cross-linked.

4. The articular cartilage implant of claim 1 , wherein the cellulose-reinforced hydrogel has a compressive strength exceeding 59 MPa.

5. The articular cartilage implant of claim 1 , wherein the cross-linked cellulose nanofiber network is secured over the top bearing surface by a clamp.

6. The articular cartilage implant of claim 5 , wherein the cross-linked cellulose nanofiber network comprises one or more sheets of bacterial cellulose (BC) held over the top bearing surface by a clamp secured to a lip or rim of the top bearing surface.

7. The articular cartilage implant of claim 1 , wherein the cellulose-reinforced hydrogel is attached to a metallic base of the top bearing surface with a shear strength exceeding 0.2 MPa.

8. The articular cartilage implant of claim 1 , wherein the top bearing surface has a coefficient of friction (COF) that is not statistically greater than that of cartilage.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 31, 2023
From: WILEY, BENJAMIN J.; TONG, HUAYU; ZHAO, JIACHENG
To: DUKE UNIVERSITY
Reel/Frame 064764/0893 →
Continuity (3)
Division 17845881 · Jun 21, 2022
Provisional Application 63338439 · May 4, 2022
Related Publication 20230381376A1 · Nov 30, 2023