IP Library › Granted Patent US 12,064,746
Granted Patent B2
US 12,064,746 · App. 17/945,195 · Granted Aug 20, 2024

Mercury adsorbent and method for producing same

Inventors: Kiyoto Otsuka (Bizen, JP); Shuichi Ishida (Bizen, JP); Hideharu Iwasaki (Osaka, JP)
Assignee: KURARAY CO., LTD.
B01J20/20B01J20/0288B01J20/0292B01J20/28064B01J20/28066B01J20/28076B01J20/2808B01J20/3204B01J20/3234C10G17/095C10G25/003C10G2300/1044C10G2300/205
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Quick Facts
Patent No.
US 12,064,746
App. No.
17/945,195
Granted
Aug 20, 2024
Kind
B2
Abstract

Provided is a mercury adsorbent that can efficiently adsorb and remove mercury and/or a mercury compound contained in a liquid hydrocarbon and can suppress corrosive action even when used for a long time. The mercury adsorbent comprises an activated carbon including a mineral acid supported thereon, the activated carbon having a specific surface area of 1000 m 2 /g or larger and a volume of micropores of 80 cm 3 /g or larger, each of the micropores having a pore radius of 8 Å or smaller, and the mercury adsorbent has a moisture content of from 0.1 to 3 wt %.

Claims (15)

1. A mercury adsorbent for adsorbing mercury and/or a mercury compound in a liquid hydrocarbon, the mercury adsorbent comprising:

an activated carbon including a mineral acid supported thereon,

wherein

the activated carbon has a specific surface area of 1000 m 2 /g or larger and a volume of micropores of 80 cm 3 /g or larger,

each of the micropores has a pore radius of 0.8 nm or smaller, and

the mercury adsorbent has a moisture content of from 0.1 to 3 wt %.

2. The mercury adsorbent of claim 1 , wherein the activated carbon contains oxygen and carbon in a weight ratio (O/C) of from 0.010 to 0.100.

3. The mercury adsorbent of claim 1 , wherein when measured by a combustion ion chromatography method, at least one ion selected from the group consisting of a chloride ion, a bromide ion, a phosphate ion, a phosphite ion, a sulfate ion, and a sulfite ion is detected in an amount of from 1000 to 5000 ppm.

4. The mercury adsorbent of claim 1 , wherein the mineral acid is at least one acid selected from the group consisting of hydrochloric acid, sulfuric acid, and phosphoric acid.

5. A method of producing the mercury adsorbent as of claim 1 , the method comprising:

bringing a mineral acid solution into contact with an activated carbon having a specific surface area of 1000 m 2 /g or larger and a volume of micropores of 80 cm 3 /g or larger, each of the micropores having a pore radius of 0.8 nm or smaller, to obtain an acid-treated activated carbon; and

adjusting a moisture content of the acid-treated activated carbon within a range of from 0.1 to 3 wt %.

6. The method of claim 5 , wherein the activated carbon contains oxygen and carbon in a weight ratio (O/C) of from 0.010 to 0.100.

7. A method for adsorbing mercury and/or a mercury compound, the method comprising:

bringing the mercury adsorbent of claim 1 into contact with a liquid hydrocarbon containing the mercury and/or the mercury compound.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 15, 2022
From: OTSUKA, KIYOTO; IWASAKI, HIDEHARU
To: KURARAY CO., LTD.
Reel/Frame 061103/0212 →
Priority Claims (1)
JP 2020-046208 · Mar 17, 2020 · national
Continuity (2)
Continuation PCTJP2021005481 · Feb 15, 2021
Related Publication 20230026065A1 · Jan 26, 2023