IP Library Granted Patent US 12,105,067
Granted Patent B2
US 12,105,067 · App. 16/694,995 · Granted Oct 1, 2024

Droplet generator system, detector for samples, corresponding method and use

Inventor: Joachim Wiechers (Planegg, DE)
Assignee: Dionex Softron GmbH
G01N30/84G01N30/64G01N2015/0003G01N2030/027G01N2030/8452
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Quick Facts
Patent No.
US 12,105,067
App. No.
16/694,995
Granted
Oct 1, 2024
Kind
B2
Abstract

A detector system includes a droplet generator system, wherein the droplet generator system includes a droplet generator unit. The droplet generator unit is configured to create droplets from a liquid supplied to the droplet generator unit with a droplet generator liquid flow. The droplet generator unit is configured to create the droplets with a defined droplet generation frequency.

Claims (43)

1. A detector system comprising:

a droplet generator system, wherein the droplet generator system comprises:

a droplet generator unit, wherein the droplet generator unit is configured to create droplets from a liquid supplied to the droplet generator unit with a droplet generator liquid flow,

wherein the droplet generator unit is further configured to create the droplets with a droplet generation frequency,

wherein the droplet generator system further comprises:

a controller configured to control the droplet generator unit, wherein the controller is also configured to control the droplet generation frequency,

wherein the droplet generation frequency is adjustable and wherein the controller is configured to control the droplet generation frequency proportionally to the droplet generator liquid flow,

a flow control unit upstream of the droplet generator unit, wherein the flow control unit comprises a splitter element;

wherein the splitter element is configured and located to split the incoming liquid flow into an outgoing flow path towards the droplet generator unit and into an additional flow path.

2. The detector system according to claim 1 , wherein the droplet generator unit is configured to generate disturbances and to transmit the disturbances to the droplet generator liquid flow,

wherein the droplet generation frequency corresponds to a frequency of the disturbances.

3. The detector system according to claim 1 , wherein the droplet generator unit comprises an orifice, and

wherein the droplet generator unit is configured to generate a liquid jet by the droplet generator liquid flow being guided through the orifice,

wherein the orifice has an orifice diameter,

wherein, for each droplet generator liquid flow in a droplet generator flow range having a lower limit and an upper limit, the upper limit being at least 2 times the lower limit,

the controller is configured to control the droplet generation frequency to be within a range defined by 0.5·v and 1.5·v, wherein v=0.28·F/D 3 , wherein D is the orifice diameter and F is the droplet generator liquid flow to the droplet generator.

4. The detector system according to claim 1 , wherein the droplet generator system further comprises a flow control unit upstream of the droplet generator unit.

5. The detector system according to claim 4 ,

wherein for each incoming liquid flow in an incoming flow range, the flow control unit is configured to direct the droplet generator liquid flow in an outgoing flow range towards the droplet generator unit,

wherein the incoming flow range has an incoming lower limit and an incoming upper limit, wherein the incoming upper limit is at least 10 times the incoming lower limit,

wherein the outgoing flow range has an outgoing lower limit and an outgoing upper limit, wherein the outgoing upper limit is at most 5 times the outgoing lower limit.

6. The detector system according to claim 4 , wherein the detector system is a charged aerosol detector system.

7. An analytical method using a detector system, the detector system comprising:

a droplet generator system, wherein the droplet generator system comprises:

a droplet generator unit, wherein the droplet generator unit is configured to create droplets from a liquid supplied to the droplet generator unit with a droplet generator liquid flow,

wherein the droplet generator unit is further configured to create the droplets with a droplet generation frequency, the method comprising:

creating the droplets with the droplet generation frequency,

wherein the droplet generator system further comprises a controller configured to control the droplet generator unit, wherein the controller is also configured to control the droplet generation frequency,

wherein the droplet generator system further comprises a flow control unit upstream of the droplet generation unit, wherein the flow control unit comprises a splitter element,

wherein the splitter element is configured and located to split the incoming liquid flow into an outgoing flow path towards the droplet generator unit and into an additional flow path,

wherein the method further comprises

adjusting the droplet generation frequency,

the controller controlling the droplet generator unit,

the controller controlling the droplet generation frequency, and

the controller controlling the droplet generation frequency proportionally to the droplet generator liquid flow.

8. The analytical method according to claim 7 further comprises:

generating disturbances with the droplet generator unit;

transmitting the disturbances to the droplet generator liquid flow, wherein the droplet generation frequency corresponds to a frequency of the disturbances; and

controlling the droplet generation frequency to be within a range defined by 0.5·v and 1.5·v, wherein v=0.28·F/D 3 , wherein D is the orifice diameter and F is the droplet generator liquid flow to the droplet generator.

9. The analytical method according to claim 8 further comprises:

controlling the droplet generation frequency to be within the range defined by 0.8·v and 1.2·v.

10. The analytical method according to claim 8 further comprises:

controlling the droplet generation frequency to be within the range defined by 0.9·v and 1.1·v.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 2, 2020
From: WIECHERS, JOACHIM
To: DIONEX SOFTRON GMBH
Reel/Frame 053964/0341 →
Priority Claims (1)
DE 102018129812.9 · Nov 26, 2018 · national
Continuity (1)
Related Publication 20200166490A1 · May 28, 2020