IP Library › Granted Patent US 12,129,553
Granted Patent B2
US 12,129,553 · App. 17/255,232 · Granted Oct 29, 2024

Method for manufacturing an abradable layer

Inventors: Serge Georges Vladimir Selezneff (Moissy-Cramayel, FR); Philippe Charles Alain Le Biez (Moissy-Cramayel, FR); Arnaud Louis Gabriel Fregeac (Moissy-Cramayel, FR); Florence Ansart (Labege, FR); Claude Gilbert Jean-Pierre Estournes (Rieumes, FR)
Assignees: SAFRAN AIRCRAFT ENGINES; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; UNIVERSITE PAUL SABATIER—TOULOUSE III
C23C24/085C04B41/0018C04B41/0072C04B41/4545B82Y40/00F01D11/122F05D2230/90F05D2240/55F05D2300/2118
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Quick Facts
Patent No.
US 12,129,553
App. No.
17/255,232
Granted
Oct 29, 2024
Kind
B2
Abstract

A process for manufacturing an abradable layer, includes compressing a powder composition including at least micrometric ceramic particles having a number-average form factor greater than or equal to 3, a mass content of said micrometric ceramic particles in the powder composition being greater than or equal to 85%, the form factor of a particle being defined as the ratio [largest dimension of the particle]/[largest cross-sectional dimension of the particle], and sintering the powder composition thus compressed to obtain the abradable layer, wherein a temperature imposed during sintering, the sintering time and the compression pressure applied are selected so as to obtain a volume porosity rate of the abradable layer greater than or equal to 20%.

Claims (21)

1. A process for manufacturing a substrate coated with an abradable layer, the substrate being a turbomachine part and the process comprising:

forming the abradable layer on a separate substrate comprising a powder composition comprising at least micrometric ceramic particles having a number-average form factor greater than or equal to 3, a mass content of said micrometric ceramic particles in the powder composition being greater than or equal to 85%, the form factor of a particle being defined as the ratio [largest dimension of the particle]/[largest cross-sectional dimension of the particle], by heating said micrometric ceramic particles, as well as any nanometric ceramic particles that may be present, to a first temperature T 1 greater than or equal to 600° C. and while the assembly is brought to the first temperature T 1 , increasing a compression pressure until it reaches, at a first time t 1 , a plateau at a value Pc which corresponds to the compression pressure to be applied during the sintering of the powder composition; then

increasing the temperature of the powder composition and the separate substrate to the sintering temperature T f reached at a second time t 2 ; then

maintaining the sintering temperature T f and the compression pressure P c until the third time t 3 to obtain the abradable layer; and

separating the abradable layer from the separate substrate;

depositing the abradable layer thus formed on a surface of the substrate, and

bonding the abradable layer thus deposited on the surface of the substrate wherein a temperature imposed during sintering, a sintering time and a compression pressure applied are selected so as to obtain a volume porosity rate of the abradable layer greater than or equal to 20%.

2. The process as claimed in claim 1 , wherein the powder composition further comprises nanometric ceramic particles having a number-average form factor comprised between 0.7 and 1.3, a mass content of said nanometric ceramic particles in the powder composition being less than or equal to 15%.

3. The process as claimed in claim 2 , wherein the mass content of said nanometric ceramic particles in the powder composition is comprised between 1% and 10%.

4. The process as claimed in claim 1 , wherein the powder composition consists essentially of said micrometric ceramic particles.

5. The process as claimed in claim 1 , wherein the mass content of said micrometric ceramic particles in the powder composition is greater than or equal to 90%.

6. The process as claimed in claim 1 , wherein said micrometric ceramic particles comprise at least acicular particles having a number-average form factor comprised between 3 and 5.

7. The process as claimed in claim 1 , wherein said micrometric ceramic particles comprise at least fibrous particles having a number-average form factor strictly greater than 5.

8. The process as claimed in claim 1 , wherein a compression pressure comprised between 12.5 MPa and 100 MPa is applied to the powder composition during sintering.

9. The process as claimed in claim 1 , wherein the sintering time is comprised between 1 minute and 10 minutes.

10. The process as claimed in claim 1 , wherein the temperature (T f ) imposed during sintering is comprised between 900° C. and 1150° C.

11. The process as claimed in claim 1 , wherein the powder composition is sintered by a spark plasma sintering technique.

12. The process as claimed in claim 1 , wherein one of the following two conditions is verified:

the substrate is metallic, and said micrometric ceramic particles, as well as any nanometric ceramic particles that may be present, comprise at least zirconia, or

the substrate is made of a ceramic matrix composite material, and said micrometric ceramic particles, as well as any nanometric ceramic particles that may be present, are made of rare-earth silicate.

13. The process as claimed in claim 1 , wherein the substrate is a turbine or compressor ring sector.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 14, 2021
From: SELEZNEFF, SERGE GEORGES VLADIMIR; LE BIEZ, PHILIPPE CHARLES ALAIN; FREGEAC, ARNAUD LOUIS GABRIEL; ANSART, FLORENCE; ESTOURNES, CLAUDE GILBERT JEAN-PIERRE
To: SAFRAN AIRCRAFT ENGINES; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; UNIVERSITE PAUL SABATIER - TOULOUSE III
Reel/Frame 055919/0379 →
Priority Claims (1)
FR 1855682 · Jun 25, 2018 · national
Continuity (1)
Related Publication 20210317584A1 · Oct 14, 2021