IP Library › Granted Patent US 12,180,111
Granted Patent B2
US 12,180,111 · App. 17/909,236 · Granted Dec 31, 2024

Method for modifying a vitreous material

Inventors: Xermán Francisco De La Fuente Leis (Saragossa, ES); Luis Carlos Estepa Millán (Saragossa, ES); Luis Alberto Angurel Lambán (Saragossa, ES)
Assignee: CONSEJO SUPERIOR DE INVESTIGACIONES CIENTÍFICAS and UNIVERSIDAD DE ZARAGOZA
C03C23/0025B23K26/083B23K26/0869B23K26/352B23K26/60C03C23/007B23K2103/54
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Quick Facts
Patent No.
US 12,180,111
App. No.
17/909,236
Granted
Dec 31, 2024
Kind
B2
Abstract

Vitreous material treatment uses a piece of vitreous material having two opposite faces and a laser emission beam source. The vitreous material is heated, and a laser beam radiated on one of the faces of the vitreous material to scan following a line surpassing the opposite edges of the face of the vitreous material while the vitreous material oscillates along a path. The scan is performed while the vitreous material is heated. The vitreous material is cooled. The laser beam scan follows a line surpassing the opposite edges of the face. The scan performed oscillating between a first point and a second point.

Claims (23)

1. A method of treating a vitreous material comprising the following steps:

i. providing

a. a piece of vitreous material; wherein said piece of vitreous material comprises at least two opposite faces; and

b. at least one laser beam source;

ii. heating the piece of vitreous material of step (i) at a temperature comprised between 400 and 640° C.;

iii. applying at least one laser beam with the at least one laser beam source of step (i) on at least one of the faces of the piece of vitreous material of step (ii), performing a scan following a line surpassing the opposite edges of the at least one of the faces of the piece of vitreous material;

while the piece of vitreous material moves following a path forming an angle of between 30 and 120° with the scan line of the laser beam; wherein said scan is performed while the piece of vitreous material is at a temperature comprised between 400° C. and 640° C.;

iv. heating the piece of vitreous material obtained in step (iii) at a temperature comprised between 450° C. and 650° C.; and

v. cooling the piece of vitreous material of step (iv);

wherein the laser beam and the at least one of the faces of the piece of vitreous material form an angle of between 15 and 90°; wherein the laser beam is focused on a point of the face of the piece of material, wherein the scan follows a line surpassing the opposite edges of the face of the piece of vitreous material of step (iii), said scan being performed in a direction from a first point to a second point; once said laser beam reaches the second point, the laser beam performs the same scan but in the opposite direction until reaching the first point; wherein the scan is performed by oscillating movement following a straight line surpassing the two opposite edges of the face of the piece of vitreous material.

2. The method according to claim 1 , wherein the piece of vitreous material of step (i) is a piece of glass.

3. The method according to claim 1 , wherein the scan follows a straight line surpassing the two opposite edges of the at least one of the faces of the piece of vitreous material; and

the path that the piece of vitreous material follows by a translational movement follows a straight line which is perpendicular to the scan line of the laser beam.

4. The method according to claim 1 , wherein the movement of the piece of vitreous material is performed at a constant speed.

5. The method according to claim 1 , wherein the scanning of the laser beam is performed at a constant speed greater than 1 m/s.

6. The method according to claim 1 , wherein the laser beam source is a CO 2 laser source.

7. The method according to claim 1 , wherein the laser beam application is performed on two opposite faces of the piece of vitreous material.

8. The method according to claim 1 , wherein the temperature of the piece of vitreous material in step (v) is reduced at a speed of less than 70° C./min.

9. The method according to claim 1 , wherein the temperature of the piece of vitreous material in step (iv) is greater than the temperature of said piece in step (iii), and/or wherein the temperature of said piece in step (v) is reduced until reaching room temperature.

10. A modified vitreous material obtainable by the method defined in claim 1 .

11. The vitreous material according to claim 10 , wherein said vitreous material has a fracture stress value “σ 0 ” between 56 MPa and 89 MPa.

12. The vitreous material according to claim 10 , wherein said vitreous material has a defect distribution measurement value “m” comprised between 2 and 10.

13. The vitreous material according to claim 10 , wherein said vitreous material allows cutting without multiple fracturing in the volume of the vitreous material.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 6, 2023
From: DE LA FUENTE LEIS, XERMÁN FRANCISCO; ESTEPA MILLÁN, LUIS CARLOS; ANGUREL LAMBÁN, LUIS ALBERTO
To: CONSEJO SUPERIOR DE INVESTIGACIONES CIENTÍFICAS; UNIVERSIDAD DE ZARAGOZA
Reel/Frame 064815/0537 →
Priority Claims (1)
ES P202030176 · Mar 2, 2020 · national
Continuity (1)
Related Publication 20230322618A1 · Oct 12, 2023