IP Library Granted Patent US 12,181,421
Granted Patent B2
US 12,181,421 · App. 17/808,944 · Granted Dec 31, 2024

Test capsules for measuring a change in at least one property of a material, and related methods

Inventors: Robert A. Roach (Idaho Falls, ID); Andrea M. Jokisaari (Idaho Falls, ID); Michael D. McMurtrey (Idaho Falls, ID); Geoffrey L. Beausoleil (Idaho Falls, ID); Carolyn L. Seepersad (Austin, TX)
Assignees: Battelle Energy Alliance, LLC; Board of Regents, The University of Texas System
G01N23/00
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Quick Facts
Patent No.
US 12,181,421
App. No.
17/808,944
Granted
Dec 31, 2024
Kind
B2
Abstract

A test capsule for measuring at least one property of a material exposed to nuclear radiation comprises a lattice structure configured to exhibit a change in at least one property responsive to exposure to nuclear radiation. The lattice structure comprises a first strut and a second strut connected to the first strut at a node. Related test capsules and methods are also described.

Claims (34)

1. A test capsule for measuring at least one property of a material exposed to nuclear radiation, the test capsule comprising:

at least one lattice structure configured to exhibit a change in at least one property responsive to exposure to nuclear radiation, the at least one lattice structure comprising:

a first strut; and

a second strut connected to the first strut at a node.

2. The test capsule of claim 1 , wherein the second strut comprises a different material composition than the first strut.

3. The test capsule of claim 1 , wherein the first strut comprises a piezoelectric material.

4. The test capsule of claim 1 , further comprising an additional lattice structure comprising a different material composition than the at least one lattice structure and in contact with the at least one lattice structure.

5. The test capsule of claim 1 , further comprising an additional lattice structure comprising a different geometry than the at least one lattice structure and in contact with the at least one lattice structure.

6. The test capsule of claim 1 , wherein the first strut is configured to be deformed in a direction opposite a direction in which the second strut is configured to be deformed responsive to exposure to nuclear radiation.

7. The test capsule of claim 1 , wherein the first strut is configured to be deformed in a same direction as the second strut is configured to be deformed responsive to exposure to nuclear radiation.

8. The test capsule of claim 1 , wherein the at least one lattice structure comprises:

a first unit cell comprising the first strut and the second strut; and

a second unit cell connected to the first unit cell at an additional node.

9. The test capsule of claim 8 , wherein the second unit cell comprises a different material composition than the first unit cell.

10. A test capsule for measuring a change in at least one property of a material responsive to exposure to nuclear radiation, the test capsule comprising:

a shell defining a volume; and

at least one lattice structure within the volume and configured to exhibit a change in at least one property responsive to exposure to nuclear radiation.

11. The test capsule of claim 10 , wherein the at least one lattice structure comprises:

a first lattice structure; and

a second lattice structure.

12. The test capsule of claim 11 , wherein the second lattice structure exhibits a geometry different from a geometry of the first lattice structure.

13. The test capsule of claim 12 , wherein the second lattice structure directly contacts the first lattice structure.

14. The test capsule of claim 10 , wherein the at least one lattice structure comprises unit cells having one or more of an octet truss structure, a body centered cubic structure, a reinforced body centered cubic structure, a face-centered cubic structure, a diamond structure, an octahedral structure, and a snap-through structure.

15. The test capsule of claim 10 , wherein the at least one lattice structure comprises unit cells defined by struts extending from nodes.

16. The test capsule of claim 15 , wherein a ratio of a length of the struts to a diameter of the struts is within a range from about 2:1 to about 20:1.

17. The test capsule of claim 10 , wherein the at least one lattice structure comprises unit cells, a size of the unit cells varying in one or more directions.

18. The test capsule of claim 10 , wherein the at least one lattice structure comprises one or more of steel, iron, nickel, molybdenum, nitrogen, zirconium, aluminum, zircaloy, graphite, hafnium, tin, and niobium.

19. The test capsule of claim 10 , wherein the change of at least one property of the at least one lattice structure comprises a change in shape, a change in volume, or both responsive to the exposure to the nuclear radiation.

20. A method of qualifying a material for use in a nuclear reactor, the method comprising:

placing at least one lattice structure within a test capsule, the at least one lattice structure comprising struts connected to nodes;

disposing the test capsule in a nuclear reactor and exposing the test capsule to radiation for a duration of time;

after the duration of time, removing the test capsule from the nuclear reactor; and

measuring a displacement of at least one of the struts of the at least one lattice structure to measure at least one property of the at least one lattice structure.

21. The method of claim 20 , wherein measuring a displacement of the at least one lattice structure to measure the at least one property of the lattice structure comprises determining an irradiated assisted creep of the lattice structure.

Assignments (1)
CONFIRMATORY LICENSE Recorded Nov 21, 2022
From: BATTELLE ENERGY ALLIANCE, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 061837/0046 →
Continuity (2)
Provisional Application 63203072 · Jul 7, 2021
Related Publication 20230010473A1 · Jan 12, 2023