IP Library › Granted Patent US 12,187,821
Granted Patent B2
US 12,187,821 · App. 17/505,679 · Granted Jan 7, 2025

Fluorosulfonyl group-containing compound, fluorosulfonyl group-containing monomer, and their production methods

Inventors: Takeshi Hirai (Tokyo, JP); Daisuke Jomuta (Tokyo, JP); Chikaya Tamitsuji (Tokyo, JP)
Assignee: AGC Inc.
C08F14/26B01D67/0093B01D69/02B01D71/32B01D71/36B01D71/82B01J39/20C07C303/22C07C309/80C07C309/82C08F8/12C08F16/24C08F16/30C08F214/26C08F214/262C08F216/1475C08J5/2237C08J5/225C08L27/22C25B1/02C25B1/04C25B1/46C25B13/08H01B1/122H01M4/8663H01M8/10H01M8/1004H01M8/1007H01M8/1023H01M8/1039H01M8/188H01M10/0565H01M50/411B01D69/145B01D2325/04B01D2325/14B01D2325/42H01M2008/1095H01M2300/0082Y02E60/10Y02E60/36Y02E60/50Y02P70/50
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Quick Facts
Patent No.
US 12,187,821
App. No.
17/505,679
Granted
Jan 7, 2025
Kind
B2
Abstract

A method for producing a fluorosulfonyl group-containing compound to obtain a compound represented by the following formula 5 from a compound represented by the following formula 1 as a starting material and a method for producing a fluorosulfonyl group-containing monomer in which the fluorosulfonyl group-containing compound is used: wherein R 1 and R 2 are a C 1-3 alkylene group, and R F1 and R F2 are a C 1-3 perfluoroalkylene group.

Claims (9)

1. A fluorosulfonyl group-containing polymer, comprising:

a plurality of copolymerized units comprising tetrafluoroethylene and a monomer of Formula 9a:

wherein each of R F1 and R F2 is C F2 , and

wherein

a content of the copolymerized units of the monomer of Formula 9a is in a range of 13.4 to 18.3 mole %, of the total copolymerized units, and

a volume flow rate TQ of the fluorosulfonyl group-containing polymer is in a range of 200° C. to 330° C.

2. The fluorosulfonyl group-containing polymer of claim 1 , further comprising a copolymerized unit selected from the group consisting of chlorotrifluoroethylene, trifluoroethylene, vinylidene fluoride, vinyl fluoride, ethylene, propylene, perfluoro (3-butenyl vinyl ether), a perfluoro (allyl vinyl ether), a perfluoro α-olefin, a (perfluoroalkyl) ethylene, a (perfluoroalkyl) propene, a perfluoro (alkyl vinyl ether) and a perfluoromonomer having a 5-membered ring.

3. A sulfonic acid containing polymer obtained by hydrolysis of the fluorosulfonyl groups of the fluorosulfonyl group-containing polymer of claim 1 ; wherein an ion exchange capacity of the sulfonic acid containing polymer is from 0.5 to 2.5 meq/g dry resin.

4. A sulfonic acid containing polymer obtained by hydrolysis of the fluorosulfonyl groups of the fluorosulfonyl group-containing polymer of claim 2 ; wherein an ion exchange capacity of the sulfonic acid containing polymer is from 0.5 to 2.5 meq/g dry resin.

Priority Claims (3)
JP 2017-168659 · Sep 1, 2017 · national
JP 2018-091756 · May 10, 2018 · national
JP 2018-091757 · May 10, 2018 · national
Continuity (3)
Division 16801222 · Feb 26, 2020
Continuation PCTJP2018032433 · Aug 31, 2018
Related Publication 20220041765A1 · Feb 10, 2022
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