IP Library Granted Patent US 12,201,709
Granted Patent B2
US 12,201,709 · App. 17/689,042 · Granted Jan 21, 2025

Hydroxyapatite, cosmetic, food, and method for producing the same

Inventors: Hideki Aoki (Tokyo, JP); Nobukiyo Tanaka (Urasoe, JP)
Assignee: Brainy Inc.
A61K8/24A23C9/1322A23L2/02A23L2/52A23L33/16A61K8/04A61Q19/00A61Q19/10C01B25/16A23V2002/00C01P2002/50C01P2004/64
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Quick Facts
Patent No.
US 12,201,709
App. No.
17/689,042
Granted
Jan 21, 2025
Kind
B2
Abstract

According to the present invention, provided is a carbonate- and magnesium-substituted hydroxyapatite having a particle size of 5 nm or more and 60 nm or less, wherein a portion of the calcium atoms in the hydroxyapatite are substituted with magnesium atoms and a portion of phosphate groups are substituted with carbonate groups.

Claims (12)

1. A method for producing a suspension comprising carbonate- and magnesium-substituted hydroxyapatite having a part of calcium substituted with magnesium and a part of phosphate group substituted with a carbonate group, and comprising primary particles in a non-aggregated state, the primary particles having a particle size of 5 nm or more and 60 nm or less,

the method comprising:

preparing a mixed suspension comprising magnesium hydroxide and calcium hydroxide;

preparing a phosphoric acid aqueous solution; and

mixing the mixed suspension and the phosphoric acid aqueous solution by stirring in the presence of pure carbon dioxide gas, causing a neutralization reaction, and obtaining, in a liquid state, the suspension comprising the carbonate- and magnesium-substituted hydroxyapatite comprising the primary particles in the non-aggregated state.

2. A method for producing a suspension comprising carbonate- and magnesium-substituted hydroxyapatite having a part of calcium substituted with magnesium and a part of phosphate group substituted with a carbonate group, and comprising primary particles in a non-aggregated state, the primary particles having a particle size of 5 nm or more and 60 nm or less,

the method comprising:

preparing a first solution comprising magnesium salt and calcium salt;

preparing a second solution comprising phosphate salt; and

mixing the first solution and the second solution by stirring in the presence of pure carbon dioxide gas, causing a reaction, and obtaining, in a liquid state, the suspension comprising the carbonate- and magnesium-substituted hydroxyapatite comprising the primary particles in the non-aggregated state.

3. The method of claim 1 , wherein the stirring is executed with an ultrasonic vibration device.

4. The method of claim 2 , wherein the stirring is executed with an ultrasonic vibration device.

Continuity (3)
Division 16665582 · Oct 28, 2019
Continuation PCTJP2017016855 · Apr 27, 2017
Related Publication 20220192943A1 · Jun 23, 2022
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