Method and system for measuring a liquid level in a pressure vessel of a urea synthesis plant
A method and system for measuring a liquid level in a pressure vessel, the method comprising: transmitting an electromagnetic signal through a wave guide in the form of an elongate solid rod ( 5 ) with bottom end immersed in the liquid and detecting a signal generated by the reflection on the surface of the liquid.
1. A method for measuring a liquid level in a pressure vessel of a urea synthesis plant, the method comprising:
emitting a first electromagnetic signal from above the liquid level and towards the liquid level, over an outside surface of a wave guide, wherein said wave guide is an elongate solid rod, wherein the solid rod extends below the liquid level;
detecting a second electromagnetic signal which is generated by the first signal reflected by the surface of the liquid;
determining the liquid level on the basis of the elapsed time between the emission of the first signal and the detection of the second signal,
wherein a gaseous phase contained in the pressure vessel above said liquid level, which is a gaseous phase including ammonia and carbon dioxide, has a pressure equal to or greater than 80 bar and a temperature equal to or greater than 120° C., wherein the determination of the liquid level comprises a step of a compensation of a dielectric of said gaseous phase.
2. The method according to claim 1 , wherein said compensation includes the generation of a reference reflection at a known location of said rod above the liquid level, and calculation of the actual speed of the signal based on said reference reflection.
3. The method according to claim 2 , wherein the reference reflection is generated by a change of diameter of the rod.
4. The method according to claim 1 , wherein said first signal has a frequency of less than 1.5 GHz.
5. The method according to claim 4 , wherein said first signal has a frequency of 100 MHz to 1.5 GHz.
6. The method according to claim 5 , wherein said first signal has a frequency of 100 MHz to 1 GHz.
7. The method according to claim 1 , wherein said rod wave guide is either straight or bended.
8. The method according to claim 7 , wherein said rod wave guide is a curved rod with a 90° bend.
9. The method according to claim 1 , wherein said gaseous phase has at least one of temperature and pressure above the critical value.
10. The method according to claim 1 , the solid rod wave guide having a length of no more than 5 meters.
11. The method according to claim 10 , the solid rod wave guide having a length of no more than 3 meters.
12. The method according to claim 1 , said solid rod wave guide being a cylindrical rod.
13. The method according to claim 12 , said rod having a diameter of 12 to 20 mm.
14. The method according to claim 13 , said rod having a diameter of 14 to 18 mm.
15. The method according to claim 1 , the pressure vessel being any of a high-pressure reactor, a high-pressure stripper or a high-pressure condenser of a urea synthesis plant.
16. The method according to claim 1 , wherein said gaseous phase above the liquid level comprises ammonia and carbon dioxide.
17. The method according to claim 1 , wherein said gaseous phase above the liquid level has a pressure equal to or greater than 120 bar, and a temperature of 140 to 210° C.
18. The method according to claim 17 , wherein said gaseous phase above the liquid level has a pressure in the range 140 to 220 bar, and a temperature of 140 to 210° C.
19. A system for measuring a liquid level in a pressure vessel of a urea synthesis plant according to the method of claim 18 , the system comprising an emitter, an elongate solid rod wave guide and a receiver, wherein:
the emitter is located above the liquid level and is arranged to transmit a first electromagnetic signal over an outside surface of said elongate solid rod wave guide towards the liquid level;
the rod wave guide extends from above the liquid level and has a bottom end below the liquid level;
the receiver is arranged to detect a second electromagnetic signal which is generated by the first signal reflected by the surface of the liquid;
the system outputs a measure of the liquid level determined on the basis of the elapsed time between the transmission of the first signal from the emitter and the detection of the second signal by the receiver, and
the vessel operates at a pressure equal to or greater than 80 bar abs and a temperature equal to or greater than 120° C., and
wherein the rod wave guide comprises at least one source for a reference reflection for the calculation of the actual speed of the signal in the gaseous phase above the liquid level.
20. The system according to claim 19 , wherein the emitter and the receiver are part of a combined emitter/receiver.
21. The method according to claim 1 , wherein said rod wave guide has a modular structure comprising several pieces.