Method for preventing cracking of nickel-based superalloy fabricated by selective laser melting
A method for preventing cracking of nickel-based superalloy fabricated by selective laser melting (SLM) belongs to the field of additive manufacturing (AM). The method of preparing an as-built part with a high density, no crack defects, and good mechanical properties includes: reducing the content of elements Zr and B forming low melting point phase in a nickel-based superalloy, adjusting the total content of Al and Ti in the alloy to 4.5 wt % or below, and combining with the control of special SLM process parameters. The new method has the advantages of a reasonable component design, a simple preparation process, and good performance of the as-built part, and therefore is suitable for large-scale application.
1. A method for preventing cracking of a nickel-based superalloy fabricated by selective laser melting (SLM), comprising:
step 1: adjustment of alloy composition:
reducing a content of Zr to 0 wt % and a content of B to 0-0.02 wt % in the nickel-based superalloy, and adjusting a content of Al to 4.5 wt % or below and a content of Ti to 4.5 wt % or below in the nickel-based superalloy, to obtain a required nickel-based superalloy powder; and
step 2: SLM building:
preparing an as-built part under a protective atmosphere by an SLM building process using the required nickel-based superalloy powder as a raw material.
2. The method according to claim 1 , wherein
in the SLM building process, a substrate heating temperature is controlled to 150° C., a rotation angle between scanning layers is controlled to 67.5°, a laser input power is controlled to 300-350 W, a scanning speed is controlled to 750-850 mm/s, a scanning space is controlled to 0.11-0.13 mm, and a powder layer thickness is controlled to 30-40 μm.
3. The method according to claim 1 , wherein
in the SLM building process, a laser spot diameter is controlled to 0.12 mm; and
in the SLM building process, a snake scanning strategy is used for laser scanning.
4. The method according to claim 1 , wherein
in the step 2, the required nickel-based superalloy powder is prepared by argon atomization or by plasma rotating electrode process (PREP).
5. The method according to claim 1 , wherein
in the step 2, the protective atmosphere is an argon atmosphere.
6. The method according to claim 1 , wherein
the required nickel-based superalloy powder comprises the following components in percentage by mass:
Co: 20.6 wt %;
Cr: 13.0 wt %;
Mo: 3.8 wt %;
W: 2.1 wt %;
Al: 2.0 wt %;
Ti: 2.5 wt %;
Ta: 2.4 wt %;
Nb: 0.9 wt %;
Zr: 0 wt %;
B: 0.01 wt %;
C: 0.04 wt %; and
Ni: the balance;
the required nickel-based superalloy powder is prepared by argon atomization, and is sieved to obtain powder suitable for the SLM building; and
the SLM building is used, a substrate heating temperature is adjusted to 150° C., a rotation angle between scanning layers is set to 67°, a laser input power is set to 325 W, a scanning speed is set to 800 mm/s, a scanning space is set to 0.12 mm, a powder layer thickness is set to 30 μm, a laser spot diameter is selected as 0.12 mm, a snake scanning strategy is selected for laser scanning, and after argon gas is introduced, printing is started, to obtain an as-built part with a density of 99.35%, no cracks, and a tensile strength of 1145 MPa at room temperature on an X-Y plane.
7. The method according to claim 1 , wherein
the required nickel-based superalloy powder comprises the following components in percentage by mass:
Co: 8.5 wt %;
Cr: 16 wt %;
Mo: 1.75 wt %;
W: 2.6 wt %;
Al: 2.0 wt %;
Ti: 2.5 wt %;
Ta: 1.75 wt %;
Nb: 0.9 wt %;
Zr: 0 wt %;
B: 0.01 wt %;
C: 0.11 wt %; and
Ni: the balance;
the required nickel-based superalloy powder is prepared by argon atomization, and is sieved to obtain powder suitable for the SLM building; and
the SLM building is used, a substrate heating temperature is adjusted to 150° C., a rotation angle between scanning layers is set to 67°, a laser input power is set to 300 W, a scanning speed is set to 750 mm/s, a scanning space is set to 0.12 mm, a powder layer thickness is set to 30 μm, a laser spot diameter is selected as 0.12 mm, a snake scanning strategy is selected for laser scanning, and after argon gas is introduced, printing is started, to obtain an as-built part with a density of 99.28%, no cracks, and a tensile strength of 1127 MPa at room temperature on an X-Y plane.