IP Library Granted Patent US 12,221,385
Granted Patent B2
US 12,221,385 · App. 18/367,544 · Granted Feb 11, 2025

Preceramic polymer grafted nanoparticles and methods of making and using same

Inventors: Matthew B. Dickerson (Beavercreek, OH); Kara L. Martin (Beavercreek, OH)
Assignee: United States of America as represented by the Secretary of the Air Force
C04B35/589C04B35/571C04B35/626C04B35/628B82Y30/00B82Y40/00C04B2235/3813C04B2235/3826C04B2235/3873C04B2235/3886C04B2235/5454C04B2235/60
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Quick Facts
Patent No.
US 12,221,385
App. No.
18/367,544
Granted
Feb 11, 2025
Kind
B2
Abstract

The present invention relates to preceramic polymer grafted nanoparticles and as well as methods of making and using same. Advantages of such preceramic polymer grafted nanoparticles include, reduced out gassing, desired morphology control and desirable, distinct rheological properties that are not found in simple mixtures. As a result, Applicants' preceramic polymer grafted nanoparticles can be used to provide significantly improved, items including but not limited to hypersonic vehicles, jets, rockets, mirrors, signal apertures, furnaces, glow plugs, brakes, and armor.

Claims (16)

1. A process of making a preceramic polymer grafted nanoparticle comprising: combining a carbosilane monomer comprising at least one silane moiety and at least one vinyl moiety and/or a cyclic carbosilane monomer, with a core comprising a material selected from the group consisting of Hydrogen, Lithium, Beryllium, Boron, Carbon, Nitrogen, Oxygen, Fluorine, Sodium, Magnesium, Aluminum, Silicon, Phosphorus, Sulfur, Chlorine, Potassium, Calcium, Scandium, Titanium, Vanadium, Chromium, Manganese, Iron, Cobalt, Nickel, Copper, Zinc, Gallium, Germanium, Arsenic, Selenium, Bromine, Strontium, Yttrium, Zirconium, Niobium, Molybdenum, Technetium, Ruthenium, Rhodium, Palladium, Silver, Cadmium, Indium, Tin, Antimony, Tellurium, Iodine, Cesium, Barium, Lanthanum, Cerium, Praseodymium, Neodymium, Promethium, Samarium, Europium, Gadolinium, Terbium, Dysprosium, Holmium, Erbium, Thulium, Ytterbium, Lutetium, Hafnium, Tantalum, Tungsten, Rhenium, Osmium, Iridium, Platinum, Gold, Mercury, Thallium, Lead, Bismuth, Polonium, Radium, Actinium, Thorium, Protactinium, Uranium, Neptunium, Plutonium, Americium, and mixtures thereof, said core having an outer surface, said outer surface being functionalized and allowing said core and said monomer to react for 24 hours to 72 hours at a temperature of from about 20° C. to 80° C., and at a pressure of from about 0.1 atm to about 100 atm.

2. The process of making a preceramic polymer grafted nanoparticle according to claim 1 , wherein:

a) said carbosilane monomer is selected from the group consisting of allyldimethylsilane, vinyldimethylsilane, allyldichlorosilane, vinyldichlorosilane, 1,1,-dimethylsilylcyclobutane, 1,1-dichlorosilylcyclobutane, 1,1-dimethyldisilylcyclobutane, 1,1-dichlorodisilylcyclobutane and mixtures thereof; and

b) said core comprises a ceramic and said core's functionalization comprises a silane moiety comprising a catalyst and/or a vinyl moiety comprising a catalyst.

3. The process of making a preceramic polymer grafted nanoparticle according to claim 2 , wherein said core comprises a nonoxide ceramic and said catalyst is platinum and/or a carbanion.

4. The process of making a preceramic polymer grafted nanoparticle according to claim 3 , wherein said core comprises SiC, ZrC, HfC, Si 3 N 4 , ZrN, HfN, ZrB 2 , HfB 2 , and mixtures thereof.

5. The process according to claim 1 , wherein said core and said monomer are combined and allowed to react at a temperature of from about 55° C. to 70° C. and at a from about 0.5 atm to about 10 atm.

6. A process of making a preceramic polymer grafted nanoparticle comprising: combining a carbosilane monomer comprising at least one silane moiety and at least one vinyl moiety and/or a cyclic carbosilane monomer, with a core comprising a material selected from the group consisting of Hydrogen, Lithium, Beryllium, Boron, Carbon, Nitrogen, Oxygen, Fluorine, Sodium, Magnesium, Aluminum, Silicon, Phosphorus, Sulfur, Chlorine, Potassium, Calcium, Scandium, Titanium, Vanadium, Chromium, Manganese, Iron, Cobalt, Nickel, Copper, Zinc, Gallium, Germanium, Arsenic, Selenium, Bromine, Strontium, Yttrium, Zirconium, Niobium, Molybdenum, Technetium, Ruthenium, Rhodium, Palladium, Silver, Cadmium, Indium, Tin, Antimony, Tellurium, Iodine, Cesium, Barium, Lanthanum, Cerium, Praseodymium, Neodymium, Promethium, Samarium, Europium, Gadolinium, Terbium, Dysprosium, Holmium, Erbium, Thulium, Ytterbium, Lutetium, Hafnium, Tantalum, Tungsten, Rhenium, Osmium, Iridium, Platinum, Gold, Mercury, Thallium, Lead, Bismuth, Polonium, Radium, Actinium, Thorium, Protactinium, Uranium, Neptunium, Plutonium, Americium, and mixtures thereof, said core having an outer surface, said outer surface being functionalized by a process selected from silanization, phosphination; and/or sulfonization followed by oxidative addition of platinum to said silane moiety and/or reacting an alkyllithium with said vinyl moiety.

7. The process of making a preceramic polymer grafted nanoparticle according to claim 6 , wherein:

a) said carbosilane monomer is selected from the group consisting of allyldimethylsilane, vinyldimethylsilane, allyldichlorosilane, vinyldichlorosilane, 1,1,-dimethylsilylcyclobutane, 1,1-dichlorosilylcyclobutane, 1,1-dimethyldisilylcyclobutane, 1,1-dichlorodisilylcyclobutane and mixtures thereof; and

b) said core comprises a ceramic and said core's functionalization comprises a silane moiety comprising a catalyst and/or a vinyl moiety comprising a catalyst.

8. The process of making a preceramic polymer grafted nanoparticle according to claim 7 , wherein said core comprises a nonoxide ceramic and said catalyst is platinum and/or a carbanion.

9. The process of making a preceramic polymer grafted nanoparticle according to claim 8 , wherein said core comprises SiC, ZrC, HfC, Si 3 N 4 , ZrN, HfN, ZrB 2 , HfB 2 , and mixtures thereof.

10. The process of making a preceramic polymer grafted nanoparticle according to claim 6 , wherein said core and said monomer are combined and allowed to react for 1 hour to 168 hours.

11. The process of making a preceramic polymer grafted nanoparticle according to claim 10 , wherein said core and said monomer are combined and allowed to react for 24 hours to 72 hours at a temperature of from about 20° C. to 80° C., and at a pressure of from about 0.1 atm to about 100 atm.

12. The process of making a preceramic polymer grafted nanoparticle according to claim 11 , wherein said core and said monomer are combined and allowed to react at a temperature of from about 55° C. to 70° C. and at a from about 0.5 atm to about 10 atm.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 13, 2023
From: DICKERSON, MATTHEW B.; MARTIN, KARA L.
To: THE GOVERNMENT OF THE UNITED STATES AS REPRESENTED BY THE SECRETARY OF THE AIR FORCE
Reel/Frame 064888/0559 →
Continuity (4)
Continuation 17114628 · Dec 8, 2020
Provisional Application 62965323 · Jan 24, 2020
Provisional Application 62965184 · Jan 24, 2020
Related Publication 20230416159A1 · Dec 28, 2023
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