IP Library › Granted Patent US 12,252,674
Granted Patent B2
US 12,252,674 · App. 17/960,975 · Granted Mar 18, 2025

Preparation of a powdered vinegar

Inventors: Renee Boerefijn (Vlaardingen, NL); Marija Orlovic (Rotterdam, NL); Kees Van Der Voort Maarschalk (Wijchen, NL)
Assignee: PURAC BIOCHEM B.V.
C12J1/00A23B2/729A23B4/12A23B4/20A23L13/42A23L13/72
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Quick Facts
Patent No.
US 12,252,674
App. No.
17/960,975
Granted
Mar 18, 2025
Kind
B2
Abstract

The present invention provides a powdered vinegar that comprises partly neutralized vinegar, i.e. vinegar derived acid that is partly neutralized with e.g. sodium and/or potassium hydroxide, and free vinegar derived acid. The invention also provides a process for producing such a powdered vinegar and the use of this powdered vinegar in a foodstuff or a beverage, e.g. as a preservative. The present process offers the advantage that it yields a stable, free flowing powdered vinegar that can suitably be used as a preservative in e.g. processed meat products. The powdered vinegar has a high content of free acid, is easy to dissolve and acts as an acidulant.

Claims (9)

1. A process of producing a free flowing powdered vinegar comprising free vinegar derived acid and neutralized vinegar derived acid, wherein more than 90% of the free vinegar derived acid and neutralized vinegar derived acid is acetic acid in free and neutralized form, wherein Na+ represents at least 50 mol. % of the cations of salts that are contained in the powdered vinegar, wherein the powdered vinegar has a water content of 9-15 wt. %, at least a fraction of the water being present as a component of hydrated salt, wherein free vinegar derived acid and neutralized vinegar derived acid are contained in the powdered vinegar in a weight ratio of not more than 1:8, the process comprising:

(a) adjusting the pH of a first liquid vinegar to a value within the range of 5.5-7.0 to obtain a neutralized vinegar;

(b) drying the neutralized vinegar to produce vinegar derived particles having a water content of less than 5 wt. %; and

(c) combining a second liquid vinegar with the vinegar derived particles in a weight ratio of 1:15 to 1:1, wherein the vinegar derived particles are agitated and the temperature of the vinegar derived particles and second liquid vinegar is controlled to stay below 54° C.

2. The process according to claim 1 , wherein the first liquid vinegar contains 10-40% (w/v) free acid.

3. The process according to claim 1 , wherein the neutralized vinegar is dried to produce vinegar derived particles having a volume weighted average diameter of 50-500 μm.

4. The process according to claim 1 , wherein the second liquid vinegar comprises 20-55% (w/v) free acid.

5. The process according to claim 1 , wherein the second liquid vinegar is combined with the vinegar derived particles by spraying the second liquid vinegar onto the vinegar derived particles.

6. The process according to claim 1 , wherein the pH of the first liquid vinegar is adjusted to a value within the range of 6.0-7.0.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 13, 2025
From: BOEREFIJN, RENEE; ORLOVIC, MARIJA; VAN DER VOORT MAARSCHALK, KEES
To: PURAC BIOCHEM B.V.
Reel/Frame 069842/0852 →
Priority Claims (1)
EP 12178789 · Aug 1, 2012 · regional
Continuity (4)
Continuation 16928822 · Jul 14, 2020
Continuation 14418396
Provisional Application 61678133 · Aug 1, 2012
Related Publication 20230025074A1 · Jan 26, 2023
References Cited (14)
US 3445244A · Noznick et al. · 1969 [cited by applicant]
US 5127953A · Hamaguchi · 1992 [cited by applicant]
US 7387808B2 · Ha et al. · 2008 [cited by applicant]
US 20040109897A1 · Annis · 2004 [cited by applicant]
US 20070059423A1 · Toledo · 2007 [cited by examiner]
US 20080305228A1 · Knikker et al. · 2008 [cited by applicant]
US 20100310738A1 · Ludwig · 2010 [cited by applicant]
US 20120142531A1 · Mazeaud et al. · 2012 [cited by applicant]
CN 102399676A · 2012 [cited by applicant]
JP 60164475A · 1985 [cited by applicant]
JP 2006087389A · 2006 [cited by applicant]
JP 2012044907A · 2012 [cited by applicant]
“Mesh to Micron Conversion Chart”, retrieved from http://www.showmegold.org/news/Mesh.htm, dated Oct. 22, 2007 (2 pages). [cited by applicant]
Ault, Addison, “Techniques and Experiments for Organic Chemistry”, 6th Edition, 1998, University Science Books, pp. 303-304 (2 pages). [cited by applicant]