IP Library › Granted Patent US 12,276,003
Granted Patent B2
US 12,276,003 · App. 17/617,681 · Granted Apr 15, 2025

Method of heat treating a high strength steel and a product obtained therefrom

Inventors: Hongliang Yi (Liaoning, CN); Shu Zhou (Shanghai, CN); Dapeng Yang (Liaoning, CN); Huajie Qin (Liaoning, CN); Xiaochuan Xiong (Jiangsu, CN); Guodong Wang (Liaoning, CN)
Assignee: IRONOVATION MATERIALS TECHNOLOGY CO., LTD.
C21D1/26C21D1/18C21D6/002C21D6/005C21D6/008C22C38/02C22C38/04C22C38/22C22C38/24C22C38/26C22C38/28C22C38/38C22C38/44C22C38/46C22C38/48
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Quick Facts
Patent No.
US 12,276,003
App. No.
17/617,681
Granted
Apr 15, 2025
Kind
B2
Abstract

Provided in the present disclosure is a method of heat treating a high-strength steel, wherein the high-strength steel comprises, by weight: 0.30-0.45% C, 1.0% or less Si, 0.20-2.5% Mn, 0.20-2.0% Cr, 0.15-0.50% Mo, 0.10-0.40% V, 0.2% or less Ti, 0.2% or less Nb, and a balance of Fe and other alloy elements and impurities, wherein the above alloy elements make Eq(Mn) according to the following formula (1) no less than 1.82, which method comprises the steps of 1) austenitizing; 2) carbide precipitation; and 3) tempering. The heat-treated steel in accordance with the present invention has high strength, high ductility and high toughness at the same time, especially improved reduction in area of tensile sample, so that it is particularly suitable for preparing spring members for vehicle suspension. Eq(Mn)=Mn+0.26Si+3.50P+1.30Cr+2.67Mo  (1)

Claims (18)

1. A method of heat treating a high-strength steel, wherein the high-strength steel comprises, by weight: 0.30-0.45% C, 1.0% or less Si, 0.20-2.5% Mn, 0.20-2.0% Cr, 0.15-0.50% Mo, 0.10-0.40% V, 0.2% or less Ti, 0.2% or less Nb, and a balance of Fe and other alloy elements and impurities, wherein the above alloy elements make Eq(Mn) according to the following formula (1) no less than 1.82,

Eq(Mn)=Mn+0.26 Si+3.50P+1.30 Cr+2.67 Mo  (1)

which method comprises the steps of:

1) Austenitizing: heating the high-strength steel to Ac3+20° C. to 950° C. for a time of 1-300 min;

2) Carbide precipitation: cooling the high-strength steel after the step of austenitizing to Ar3-10° C. to 870° C. for a time of 5-300 min, then further cooling to 100° C. or less, wherein the average cooling rate of the further cooling is not less than 1° CS; and

3) Tempering: heating the high-strength steel after the step of carbide precipitation to 120-280° C. for a time of 5-360 min.

2. The method of claim 1 , wherein the high-strength steel comprises 0.20% by weight or less of Ti and Nb.

3. The method of claim 1 , wherein the austenitizing comprises: heating the high-strength steel to AC3+30° C. to 910° C. for a time of 1-30 min.

4. The method of claim 1 , wherein the carbide precipitation comprises: cooling the high-strength steel to Ar3+10° C. to 850° C. for a time of 5-60 min, then further cooling to 100° C. or less.

5. The method of claim 1 , further comprises the step of forming the high-strength steel into a preform before the step of austenitizing.

6. A steel obtained by the method of claim 1 , wherein the steel comprises, by area, the microstructures of: greater than or equal to 90% martensite, less than or equal to 3% ferrite, less than or equal to 5% retained austenite, and less than or equal to 10% bainite,

wherein the steel comprises 0.1-0.5% by weight of carbide particles, wherein the carbide particles comprise particles of composite carbides of V and Mo, and the carbide particles have an average particle size of 1-30 nm, and

wherein the steel has a yield strength of greater than or equal to 1400 MPa, a tensile strength of greater than or equal to 1800 MPa, and a reduction in area of tensile sample of greater than or equal to 38%.

7. The steel of claim 6 , wherein the carbide particles further comprise nitrogen.

8. The steel of claim 6 , wherein the carbide particles have an average particle size of about 1-15 nm.

9. The steel of claim 6 , wherein the steel has a yield strength of greater than or equal to 1550 MPa, a tensile strength of greater than or equal to 1900 MPa, and a reduction in area of tensile sample of greater than or equal to 45%.

10. A spring member for vehicle suspension prepared from the steel of claim 6 .

11. The spring member for vehicle suspension of claim 10 , which is a leaf spring, a stabilizer bar, or a coil spring.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE ADDRESS PREVIOUSLY RECORDED AT REEL: 71992 FRAME: 41. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Aug 18, 2025
From: IRONOVATION MATERIALS TECHNOLOGY CO., LTD.
To: EASYFORMING TECHNOLOGY CO., LTD.
Reel/Frame 072480/0220 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 12, 2025
From: IRONOVATION MATERIALS TECHNOLOGY CO., LTD.
To: EASYFORMING TECHNOLOGY CO., LTD.
Reel/Frame 071992/0041 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2022
From: ZHOU, SHU; QIN, HUAJIE; WANG, GUODONG
To: IRONOVATION MATERIALS TECHNOLOGY CO., LTD.
Reel/Frame 060148/0200 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 27, 2021
From: YI, HONGLIANG; CHANG, ZHIYUAN; LIU, ZHAOYUAN; YANG, DAPENG; XIONG, XIAOCHUAN
To: IRONOVATION MATERIALS TECHNOLOGY CO., LTD.
Reel/Frame 058480/0751 →
Priority Claims (1)
CN 201910496707.9 · Jun 10, 2019 · national
Continuity (1)
Related Publication 20220251673A1 · Aug 11, 2022
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