Granted Patent B2

US 12,287,263 · App. 18/013,397 · Granted Apr 29, 2025

Inventors: Kazuteru Takahashi (Kyoto, JP); Masahito Ueda (Kyoto, JP); Hidefumi Yamagata (Kyoto, JP); Shinsuke Inoue (Kyoto, JP); Shinji Hamasaki (Kyoto, JP)

Assignee: SHIMADZU CORPORATION

G01N1/34G01N1/16

Abstract

Claims (32)

1. A sample purification apparatus that purifies a mixed sample, the sample purification apparatus comprising:

a container for separating, with a heavy solution, the mixed sample based on a specific gravity difference, the container having a central axis direction; and

a collector that collects a component in the mixed sample lighter in specific gravity than the heavy solution by receiving a supernatant flowed out from the container,

wherein

the container includes

a flow-out port provided at an uppermost end of the container in the central axis direction, wherein the flow-out port is located on the central axis, and

a flow-out path that guides the supernatant flowed out through the flow-out port to the collector, and

the container has a horizontal cross-sectional area which decreases upward starting from a prescribed height of the container to a height where the flow-out port is located.

2. The sample purification apparatus according to claim 1 , wherein

the container includes a first main body portion, a second main body portion provided above the first main body portion, and a third main body portion provided above the second main body portion,

a horizontal cross-sectional area of the third main body portion is constructed to continuously decrease in an upward direction where the flow-out port is located, and

a horizontal cross-sectional area of the second main body portion is constructed to continuously increase from each of an upper portion and a lower portion of the second main body portion toward a portion located between the upper portion and the lower portion.

3. The sample purification apparatus according to claim 2 , wherein

the third main body portion is formed as being integrated with the second main body portion.

4. The sample purification apparatus according to claim 1 , wherein

the flow-out port is connected to the flow-out path and connected to an introduction path for introduction of the mixed sample into the container.

5. The sample purification apparatus according to claim 4 , comprising at least one switching unit provided between each of the introduction path and the flow-out path and the flow-out port, the at least one switching unit switching between entry and exit of a solution.

6. The sample purification apparatus according to claim 1 , comprising:

a first pipe for introduction into the container, of an oxidizing agent for treatment of a contaminant contained in the mixed sample;

a second pipe for introduction of the heavy solution into the container;

a third pipe for discharge of a waste solution in the container; and

a fourth pipe for introduction into the container, of a rinse solution for cleaning of inside of the container; and

at least one port provided in the container, a solution coming in and going out between the at least one port and the first pipe, the second pipe, the third pipe, and the fourth pipe.

7. The sample purification apparatus according to claim 6 , wherein

the at least one port corresponding to each of the first pipe, the second pipe, and the fourth pipe is different from the at least one port corresponding to the third pipe.

8. The sample purification apparatus according to claim 6 , wherein

the at least one port corresponding to the second pipe is identical to the at least one port corresponding to the fourth pipe.

9. The sample purification apparatus according to claim 6 , wherein

the at least one port includes a filter.

10. An analysis system comprising:

the sample purification apparatus according to claim 1 ; and

an analysis apparatus that analyzes the component collected by the collector of the sample purification apparatus.

Assignments (1)

Priority Claims (1)

Continuity (1)

References Cited (18)