IP Library › Granted Patent US 12,320,008
Granted Patent B2
US 12,320,008 · App. 18/543,115 · Granted Jun 3, 2025

Apparatuses and methods for producing covetic materials using microwave reactors

Inventors: Michael W. Stowell (Sunnyvale, CA); Bruce Lanning (Littleton, CO); Peter Todd Williams (San Carlos, CA); Daniel Cook (Woodside, CA)
Assignee: Lyten, Inc.
C23C4/067H05H1/30H05H1/461B22F1/16B22F3/115B22F2007/042B22F2202/13C23C4/134H05H1/26H05H1/46
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Quick Facts
Patent No.
US 12,320,008
App. No.
18/543,115
Granted
Jun 3, 2025
Kind
B2
Abstract

Apparatuses and methods for producing covetic materials by exciting a hydrocarbon gas with pulse microwaves to form hydrocarbon radicals in a hot first region of a microwave reactor. Graphene nanoplatelets are formed by the nucleation, growth, and assembly of the hydrocarbon radicals, and contact a metal melt introduced downstream of the hot region to produce a mixture of molten metal and graphene nanoplatelets which assemble in-flight to form covetic materials.

Claims (25)

1. An apparatus for producing covetic materials, comprising:

an energy source configured to generate a microwave energy;

a reactor including:

a first region including a first inlet port through which a hydrocarbon gas flows into the reactor, the first region configured to dissociate the hydrocarbon gas into carbon species and hydrogen species based on the microwave energy; and

a second region disposed downstream of the first region and including a second inlet port through which a metal is received into the reactor, the second region configured to form a mixture of the carbon species and the metal; and

an output port configured to form the covetic materials by cooling the mixture.

2. The apparatus of claim 1 , further comprising a control circuit configured to pulse the microwave energy.

3. The apparatus of claim 2 , wherein the pulsed microwave energy is associated with transverse electromagnetic wave propagation.

4. The apparatus of claim 2 , wherein the pulsed microwave energy is associated with transverse electric wave (TE) propagation.

5. The apparatus of claim 1 , further comprising a heating element disposed in thermal communication with the reactor and configured to melt the metal prior to the formation of the mixture.

6. The apparatus of claim 1 , wherein a cross-sectional area of the reactor decreases along a length of the reactor from the first inlet port to the output port.

7. The apparatus of claim 1 , wherein a temperature of the first region is greater than a temperature of the second region.

8. The apparatus of claim 1 , wherein the output port is configured to spray the covetic materials onto a substrate.

9. The apparatus of claim 1 , further comprising a torch coupled to the output port.

10. The apparatus of claim 9 , wherein the torch is one or more of a metal plasma torch or a microwave plasma torch.

11. The apparatus of claim 1 , further comprising a pair of electrodes configured to generate an electric field within the reactor.

12. The apparatus of claim 11 , wherein the electric field is configured to generate a current through the mixture.

13. The apparatus of claim 1 , wherein at least some of the disassociated carbon species comprise plasma.

14. The apparatus of claim 13 , further comprising one or more control circuits configured to adjust a temperature of the metal independently of a temperature of the plasma.

15. The apparatus of claim 1 , wherein the metal includes one or more of aluminum, copper, or silver.

16. The apparatus of claim 1 , further comprising a melting apparatus configured to transform the metal into molten metal.

17. The apparatus of claim 16 , wherein the melting apparatus comprises a tungsten inert gas (TIG) welder power supply.

18. The apparatus of claim 1 , further comprising one or more of a cyclone apparatus, a mechanical tumbler agitator, or a fluidized bed apparatus disposed downstream of the output port.

19. The apparatus of claim 18 , wherein the one or more of the cyclone apparatus, the mechanical tumbler agitator, or the fluidized bed apparatus is configured to cool the mixture.

20. The apparatus of claim 1 , wherein the covetic materials comprise graphene planes.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 18, 2023
From: STOWELL, MICHAEL W.; LANNING, BRUCE; WILLIAMS, PETER TODD; COOK, DANIEL
To: LYTEN, INC.
Reel/Frame 065895/0815 →
Continuity (11)
Continuation 18197842 · May 16, 2023
Continuation 17241852 · Apr 27, 2021
Division 16752693 · Jan 27, 2020
Continuation In Part 16460177 · Jul 2, 2019
Provisional Application 62903649 · Sep 20, 2019
Provisional Application 62868493 · Jun 28, 2019
Provisional Application 62839995 · Apr 29, 2019
Provisional Application 62797306 · Jan 27, 2019
Provisional Application 62720677 · Aug 21, 2018
Provisional Application 62714030 · Aug 2, 2018
Related Publication 20240150884A1 · May 9, 2024
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