IP Library Granted Patent US 12,337,302
Granted Patent B2
US 12,337,302 · App. 18/820,823 · Granted Jun 24, 2025

NiCeOx aerogels for methane suppression in the water-gas shift reaction

Inventors: Travis G. Novak (Lorton, VA); Matthew R. Buck (Columbia, MD); Paul A. DeSario (Alexandria, VA); Debra R. Rolison (Arlington, VA)
Assignee: The Government of the United States of America, as represented by the Secretary of the Navy
B01J23/83B01J35/67C01B3/16C01G53/70C01B2203/0283C01B2203/1029C01B2203/1058C01P2002/72C01P2002/82C01P2006/17
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Quick Facts
Patent No.
US 12,337,302
App. No.
18/820,823
Granted
Jun 24, 2025
Kind
B2
Abstract

An oxide-based aerogel having cerium and nickel may be used as a water-gas shift reaction catalyst without producing methane as a byproduct. It may be made by forming a gel from a cerium salt and a nickel salt solution and converting the gel to an aerogel.

Claims (20)

1. A composition comprising:

an oxide-based aerogel comprising cerium and nickel;

wherein the nickel atoms are atomically dispersed in the aerogel.

2. The composition of claim 1 , wherein the at % of nickel relative to cerium is from 1 at % to 15 at %.

3. The composition of claim 1 , wherein at least 50% of the nickel atoms are not adjacent to each other.

4. The composition of claim 1 , wherein at least 90% of the nickel atoms are not adjacent to each other.

5. A method comprising:

providing the composition of claim 1 ;

flowing a feed gas comprising water and carbon monoxide over the composition; and

performing a water-gas shift reaction.

6. The method of claim 5 , wherein the water-gas shift reaction does not produce methane.

7. The method of claim 5 , wherein the water-gas shift reaction converts at least 90% of the carbon monoxide to carbon dioxide.

8. A method comprising:

providing a solution comprising a cerium salt and a nickel salt;

forming an oxide-based gel comprising cerium, nickel, and oxygen from the solution; and

converting the gel to an aerogel;

wherein the nickel atoms are atomically dispersed in the aerogel.

9. The method of claim 8 , wherein the at % of nickel relative to cerium in the aerogel is from 1 at % to 15 at %.

10. The method of claim 8 , wherein at least 50% of the nickel atoms are not adjacent to each other.

11. The method of claim 8 , wherein at least 90% of the nickel atoms are not adjacent to each other.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 21, 2025
From: HERZOG, AUSTIN E.
To: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY
Reel/Frame 072994/0334 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 28, 2025
From: NOVAK, TRAVIS G.; BUCK, MATTHEW R.; DESARIO, PAUL A.; ROLISON, DEBRA R.
To: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY
Reel/Frame 070032/0783 →
Continuity (2)
Provisional Application 63579693 · Aug 30, 2023
Related Publication 20250073685A1 · Mar 6, 2025
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