IP Library › Granted Patent US 12,365,849
Granted Patent B2
US 12,365,849 · App. 18/480,557 · Granted Jul 22, 2025

Lubricant composition containing metal alkanoate

Inventors: Benjamin G. N. Chappell (Abingdon, GB); Mark Peter Driver (Abingdon, GB); Emily C. Mason (Abingdon, GB); Alice H. Leung (Reading, GB)
Assignee: Infineum International Limited
C10M169/044C10M125/04C10M125/22C10M129/54C10M129/70C10M139/00C10M141/12C10M155/02C10M161/00F01M9/02C10M2201/05C10M2201/06C10M2207/281C10M2225/00C10M2227/00C10M2229/046C10M2290/00C10N2030/02C10N2030/04C10N2030/06C10N2030/10C10N2030/12C10N2030/18C10N2030/52C10N2040/25C10N2040/252
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Quick Facts
Patent No.
US 12,365,849
App. No.
18/480,557
Granted
Jul 22, 2025
Kind
B2
Abstract

This invention relates to a lubricating composition comprising or resulting from the admixing of: base oil, detergent, and one or more metal alkanoates having a quaternary carbon atom at the 2 position, the 2′ position, or both the 2 and 2′ positions, where the lubricating composition preferably has an adhesive wear of 100 hours or more, a foam volume of 70 ml or less at 24° C., and 50 ml or less at 93.5° C., and, optionally, a total base number of 7 mgKOH/g or more.

Claims (49)

1. A lubricating composition comprising or resulting from the admixing of: base oil at from 70 to 85 wt. %, detergent at from 0.5 to 2.3 wt. % selected from the group consisting of calcium sulfonate, magnesium sulfonate, calcium phenate and combinations thereof, zinc dialkyl dithiophosphate at from 0.64 wt. % to 1.0 wt. % to contribute from 500 to 800 ppm phosphorous to the lubricating composition, and zinc neodecanoate at from 0.5 wt. % to 3.0 wt. %, wherein the lubricating composition has a zinc to phosphorous ratio ranging from 3.0 to 3.5 by wt. %, and where the lubricating composition has: an adhesive wear of 100 hours or more, as determined by ASTM D8074-16, and optionally a total base number of 7 mgKOH/g or more.

2. The lubricating composition of claim 1 , wherein the base oil is selected from the group consisting of Group I, Group II and combinations thereof.

3. The lubricating composition of claim 1 , further comprising one or more of the following components:

D) one or more friction modifiers;

E) one or more antioxidants;

F) one or more pour point depressants;

G) one or more anti-foaming agents;

H) one or more viscosity modifiers;

I) one or more dispersants; and/or

J) one or more inhibitors and/or anti-rust agents.

4. The lubricating composition of claim 1 , wherein:

A) the base oil is present at 79.8 to 82.2 mass % based upon the weight of the lubricating composition; and

B) the detergent is present at from 1.0 to 1.65 wt % based on total weight of the lubricating composition; and

C) the zinc neodecanoate is present at from 0.5 to 1.0 wt % based on total weight of the lubricating composition.

5. The lubricating composition of claim 4 wherein:

E) optionally, one or more antioxidants are present at from 0.01 to 5 wt %, based on total weight of the lubricating composition;

F) optionally, one or more pour point depressants are present at from 0.01 to 5 wt %, based on total weight of the lubricating composition;

G) optionally, one or more anti-foaming agents are present at from 0.001 to 5 wt %, based on total weight of the lubricating composition;

H) optionally, one or more viscosity modifiers are present at from 0.001 to 6 wt %, based on total weight of the lubricating composition;

I) optionally, one or more dispersants are present at from 0.01 to 20 wt %, based on total weight of the lubricating composition; and

J) optionally, one or more inhibitors and/or anti-rust agents are present at from 0.01 to 5 wt %, based on total weight of the lubricating composition.

6. The lubricating composition of claim 1 having at least 1000 ppm zinc.

7. The lubricating composition of claim 1 , wherein the ratio of Zn to P is 3.03 to 3.38 by wt %.

8. A method to obtain an adhesive wear of 100 hours or more, as determined by ASTM D8074-16, for a lubricating composition have 1000 ppm zinc or more comprising:

(i) providing to a crankcase of the internal combustion engine of the lubricating composition of claim 1 ;

(ii) providing a hydrocarbon fuel in the internal combustion engine; and

(iii) combusting the fuel in the internal combustion engine.

9. A method of lubricating an internal combustion engine during operation of the engine comprising:

(i) providing to a crankcase of the internal combustion engine the lubricating composition of claim 1 ;

(ii) providing a hydrocarbon fuel in the internal combustion engine; and

(iii) combusting the fuel in the internal combustion engine.

10. A method of lubricating an internal combustion engine during operation of the engine comprising:

(i) providing to a crankcase of the internal combustion engine a lubricating composition comprising base oil at from 70 to 85 wt. %; detergent at from 0.5 to 2.3 wt. % selected from the group consisting of calcium sulfonate, magnesium sulfonate, calcium phenate and combinations thereof; zinc dialkyl dithiophosphate at from 0.64 wt. % to 1.0 wt. % to contribute from 500 to 800 ppm phosphorous to the lubricating composition; and zinc neodecanoate at from 0.5 wt. % to 3.0 wt. %;

(ii) providing a hydrocarbon fuel in the internal combustion engine;

(iii) combusting the fuel in the internal combustion engine;

(iv) obtaining an adhesive wear of 100 hours or more, as determined by ASTM D8074-16, in the internal combustion engine lubricated by the composition; and

(v) wherein the lubricating composition has a zinc to phosphorous ratio ranging from 3.0 to 3.5 by wt. %, and a total base number of 7 mgKOH/g or more.

11. The method of claim 9 wherein the zinc to phosphorus ratio is between 3.03 to 3.38 by wt %, and wherein the base oil is selected from Group I, Group II, and combinations thereof.

12. The method claim 9 wherein the engine is a diesel engine.

13. The method claim 9 wherein the engine is a marine engine.

14. The method claim 9 wherein the engine is an automotive engine.

15. The lubricating composition of claim 1 where the lubricating composition has an adhesive wear of 120 hours or more.

16. The lubricating composition of claim 1 wherein the zinc neodecanoate is liquid at −15° C. and liquid at 80° C.

17. The lubricating composition of claim 1 wherein the lubricating composition is a heavy-duty diesel engine oil or a marine engine oil.

18. A method of lubricating a hydrogen and or ammonia fueled internal combustion engine during operation of the engine comprising:

(i) providing to a crankcase of the internal combustion engine a lubricating composition comprising base oil at from 70 to 85 wt. %, detergent at from 0.5 to 2.3 wt. % selected from the group consisting of calcium sulfonate, magnesium sulfonate, calcium phenate and combinations thereof; zinc dialkyl dithiophosphate at from 0.64 wt. % to 1.0 wt. % to contribute from 500 to 800 ppm phosphorous to the lubricating composition; and zinc neodecanoate at from 0.5 wt. % to 3.0 wt. %;

(ii) providing fuel comprising hydrogen and or ammonia in the internal combustion engine; and

(iii) combusting the fuel in the internal combustion engine; and

wherein the lubricating composition has a zinc to phosphorous ratio ranging from 3.0 to 3.5 by wt. %, an adhesive wear of 100 hours or more, as determined by ASTM D8074-16, and a total base number of 7 mgKOH/g or more.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2024
From: CHAPPELL, BENJAMIN; MASON, EMILY C.; LEUNG, ALICE HEI MAN; DRIVER, MARK P.
To: INFINEUM INTERNATIONAL LIMITED
Reel/Frame 066670/0157 →
Priority Claims (1)
GB 22200963 · Oct 11, 2022 · national
Continuity (1)
Related Publication 20240141252A1 · May 2, 2024
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