IP Library Granted Patent US 12,454,795
Granted Patent B2
US 12,454,795 · App. 17/401,712 · Granted Oct 28, 2025

Moisture/oil-resistant fiber/starch composite materials

Inventors: Gregory M. Glenn (Grand Junction, CO); Xing Jin (Albany, CA); Randal L. Shogren (Columbia Falls, MT)
Assignees: The United States of America, as represented by the Secretary of Agriculture; WORLD CENTRIC
D21H17/28B65D65/38D21H17/17D21H21/16D21H23/04D21J3/12
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,454,795
App. No.
17/401,712
Granted
Oct 28, 2025
Kind
B2
Abstract

The invention relates to uncoated, fiber/starch composite materials manufactured without the use of fluorochemicals or additional binders that offer superior oil and grease resistance properties. Addition of an internal sizing agent in the preparation of the fiber/starch composite materials results in superior hot water and cold water resistance properties. The fiber/starch composite materials may be used for the manufacture of food service containers. The invention also relates to methods of preparation of the fiber/starch composite materials.

Claims (18)

1. An oil, grease, and water-resistant composition comprising a matrix of starch, cellulosic fiber, and an internal sizing agent; wherein the composition is prepared by:

blending cellulosic fiber in water to create a fiber/water mixture;

blending the fiber/water mixture with starch granules and a sizing agent;

forming the fiber/starch/sizing agent blend into a sheet;

compressing and heating the sheet until nearly dry but still pliable;

forming the nearly dry sheet into an article; and

drying the article;

wherein the starch is about 30 to about 50 wt % of the composition;

wherein no fluorocarbons or auxiliary binders are in the composition;

wherein the composition is not covered by oil resistant, hot-water resistant, or cold-water resistant coatings;

wherein the composition optionally comprises a filler material; and

wherein the composition is oil, grease, and water-resistant.

2. An article of manufacture comprising the composition of claim 1 .

3. The article of manufacture of claim 2 , wherein the article of manufacture is a food container.

4. The article of manufacture of claim 3 , wherein the food container is a box, a cup, a clamshell, a plate, a bowl, a tray, a carton, an envelope, a sack, a bag, a baggie, a liner, a partition, a wrapper, a film, or a cushioning material.

5. The composition of claim 1 , wherein the internal sizing agent is an alkyl, alkenyl, aryl, alkaryl ketene dimer, alkenyl succinic anhydride, rosin, wax, stearic anhydride, or other fatty acid anhydride.

6. The composition of claim 5 , wherein the internal sizing agent is an alkene ketene dimer.

7. The composition of claim 1 , wherein the internal sizing agent is present from at least about 0.03% to less than about 90% by weight of the composition.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 25, 2023
From: JIN, XING; SHOGREN, RANDAL L.
To: WORLD CENTRIC
Reel/Frame 062480/0251 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 26, 2021
From: GLENN, GREGORY M
To: THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF AGRICULTURE
Reel/Frame 057295/0858 →
Continuity (2)
Provisional Application 63065688 · Aug 14, 2020
Related Publication 20220049428A1 · Feb 17, 2022
References Cited (26)
US 5756194A · Shogren · 1998 [cited by applicant]
US 5961708A · Zetter · 1999 [cited by applicant]
US 6168857B1 · Andersen · 2001 [cited by applicant]
US 6878199B2 · Bowden · 2005 [cited by applicant]
US 7083673B2 · Bowden · 2006 [cited by applicant]
US 7967904B2 · Bowden · 2011 [cited by applicant]
US 10145068B2 · Hans · 2018 [cited by applicant]
US 10378152B2 · Kinast · 2019 [cited by applicant]
US 10626557B2 · Colin · 2020 [cited by applicant]
US 20020123624A1 · Qiao · 2002 [cited by applicant]
US 20050120915A1 · Bowden · 2005 [cited by examiner]
US 20190092931A1 · Glenn · 2019 [cited by applicant]
US 20200095731A1 · Spender · 2020 [cited by examiner]
US 20200308359A1 · Glenn · 2020 [cited by applicant]
US 20210040693A1 · Glenn · 2021 [cited by applicant]
CN 108130788A · 2018 [cited by examiner]
EP 0415385 · 1991 [cited by applicant]
C. Dang, et al., 2017, “Preparation and Characterization of Hydrophobic Non-Crystal Microporous Starch (NCMS) and its Application in Food Wrapper Paper as a Sizing Agent,” BioResources 12(3): 5775-5789. [cited by applicant]
K. El-Tahlawy, et al., 2008 Effect pf Alkyl Ketene Dimer Reacted Starch on the Properties of Starch Microcellular Foam Using a Solvent Exchange Techniques, Carbohydrate Polymers 73: 133-142. [cited by applicant]
J.K. Fink, 2019, “The Chemistry of Bio-based Polymers,” pp. 256-257, John Wiley & Sons. M.A. Hubbe, 2006, Paper's Resistance to Wetting—A Review of Internal Sizing Chemicals and Their Effects, BioResources 2(1): 106-145. [cited by applicant]
S. Kumar, et al., 2016, “Separation and Analysis Techniques for Bound and Unbound Alkyl Ketene Dimer (AKD) in Paper: A Review,” Arab. J. Chem. 9:S1636 to S1642. [cited by applicant]
M.A. Hubbe, 2006, Paper's Resistance to Wetting—A Review of Internal Sizing Chemicals and Their Effects, BioResources 2(1): 106-145. [cited by applicant]
D.R. Lu, et al., 2009, “Starch-Based Completely Biodegradable Polymer Materials,” EXPRESS Polym. Lett. 3(6): 366-375. [cited by applicant]
G.M. Glenn, et al., 2001, “In situ laminating process for baked starch-based foams,” Ind. Crops Prod.14: 125-134. [cited by applicant]
P.B. Aebersold, et al., 1987, “Manual for Starch Gel Electrophoresis: A Method for the Detection of Genetic Variation,” NOAA Technical Report NMFS 61. [cited by applicant]
El-Tahlawy, et al., 2008, “Effect of alkyl ketene dimer reacted starch on the properties of starch microcellular foam using a solvent exchange technique,” Carbohydr. Polym. 73(1): 133-142. [cited by applicant]