IP Library Granted Patent US 12,466,737
Granted Patent B2
US 12,466,737 · App. 18/732,805 · Granted Nov 11, 2025

System and method for performing separation and dehydroxylation of fumed silica soot particles

Inventors: Sandeep Gaikwad (Gurugram, IN); Shivi Dixit (Gurugram, IN); Badri Gomatam (Gurugram, IN)
C01B33/18B01D45/16B01J8/0055B01J8/1827B04C5/02B04C5/20B01J2208/00769
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Quick Facts
Patent No.
US 12,466,737
App. No.
18/732,805
Granted
Nov 11, 2025
Kind
B2
Abstract

The present disclosure provides a separator system for performing separation and dehydroxylation of fumed silica particles. The separator system includes a first inlet, a second inlet, a main body, a first outlet and a second outlet. The first inlet collects a primary feed of fumed silica particles from a gaseous stream into a double entry cyclone. The second inlet collects a secondary feed of chlorine gas into the double entry cyclone. The main body of the double entry cyclone is utilized in treating the primary feed and the secondary feed along with heat inside the double entry cyclone. Furthermore, the first outlet is utilized for releasing the dehydrated fumed silica particles and the second outlet is utilized for releasing the water molecules and other gases.

Claims (9)

1 . A method for performing separation and dehydroxylation of fumed silica particles to manufacture a silica soot preform, the method comprising:

collecting a primary feed of fumed silica particles from a gaseous stream, where the primary feed of fumed silica particles is collected in a fluidized state;

collecting a secondary feed of chlorine gas, where the secondary feed of chlorine gas is collected for performing separation and dehydroxylation of the fluidized fumed silica particles;

treating the primary feed of the fumed silica particles and the secondary feed of chlorine gas in presence of heat;

releasing the dehydrated fumed silica particles, whereby separating and dehydroxylating the fumed silica particles; and

performing compaction of the dehydrated fumed silica particles to form the silica soot preform, where the compaction is performed after performing separation and dehydroxylation of the fumed silica particles; where collecting the primary feed of fumed silica particles from a gaseous stream into a double entry cyclone from a first inlet; where collecting the secondary feed of chlorine gas into a double entry cyclone from a second inlet.

2 . The method as claimed in claim 1 comprising, after performing separation of the fumed silica particles, releasing water molecules and gases from a second outlet.

3 . The method as claimed in claim 1 , where the fumed silica particles are treated at a temperature of less than or equal to 200 degree Celsius to remove physisorbed water molecules.

4 . The method as claimed in claim 1 , where the fumed silica particles are treated at a temperature of less than or equal to 1200 degree Celsius to remove chemisorbed water molecules.

Priority Claims (1)
IN 201921032781 · Aug 13, 2019 · national
Continuity (2)
Division 16849956 · Apr 15, 2020
Related Publication 20240327230A1 · Oct 3, 2024
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