Crack sensor, preparation method therefor, and application thereof in micro-force measurement
A crack sensor, comprising a flexible film, wherein a first side of the flexible film is provided with a plurality of linear protrusions, and an opposite second side of the flexible film is configured with a linear structure; the linear structure comprises, in order from bottom to top, a silver layer, a chromium layer, and a CNT-PDMS layer, wherein the CNT-PDMS layer is composed of polydimethylsiloxane doped with carbon nanotubes; the silver layer is configured with a crack structure, the crack structure being a crack that changes in response to the deformation of the silver layer. The crack sensor effectively resists crack propagation, significantly improving the stability of the crack sensor while also exhibiting high sensitivity. Further provided is a preparation method for the crack sensor.
1 . A method for preparing a crack sensor, comprising: coating a photoresist layer on a surface of a substrate; etching a plurality of microchannels on a surface of the photoresist layer; coating a layer of polydimethylsiloxane (PDMS) on the same surface, and curing to obtain a PDMS layer, wherein the PDMS layer has a first face with a plurality of linear protrusions and a second face that is smooth; covering the second face of the PDMS layer with a template having linear through-holes; successively forming a silver layer, a chromium layer, and a CNT-PDMS layer on a side of the template; removing the template to obtain a structure; and pre-stretching the structure to obtain the crack sensor; wherein the crack sensor comprises a flexible film, wherein a first side of the flexible film is provided with a plurality of linear protrusions, and an opposite second side of the flexible film is configured with a linear structure; the linear structure comprises, in order from bottom to top, a silver layer, a chromium layer, and a carbon nanotubes (CNT)-PDMS layer, wherein the CNT-PDMS layer is composed of PDMS doped with CNT; the silver layer is configured with a crack structure, the crack structure being a crack that changes in response to the deformation of the silver layer; wherein the flexible film is a PDMS film; the CNT-PDMS layer has a thickness of 5-20 μm; and the CNT-PDMS layer contains carbon nanotubes in an amount of 0.01-5 wt %.
2 . The method according to claim 1 , wherein the substrate is glass, and before coating the photoresist layer, the substrate is treated with O 2 plasma.
3 . The method according to claim 1 , wherein the silver layer and the chromium layer are formed by vacuum evaporation.
4 . The method according to claim 1 , wherein the CNT-PDMS layer is formed on a surface of the chromium layer by screen printing.
5 . The method according to claim 1 , wherein the pre-stretching is conducted under a strain of 1.5-2.5%.
6 . A crack sensing device, comprising a crack sensor, a support, and a cell culture component, wherein the crack sensor is positioned between the support and the cell culture component, the support is provided with a groove or a through-hole, the crack sensor covers the groove or the through-hole, and a portion or the entirety of the linear structure of the crack sensor is located within the groove or the through-hole; wherein the crack sensor comprises a flexible film, wherein a first side of the flexible film is provided with a plurality of linear protrusions, and an opposite second side of the flexible film is configured with a linear structure; the linear structure comprises, in order from bottom to top, a silver layer, a chromium layer, and a carbon nanotubes (CNT)-PDMS layer, wherein the CNT-PDMS layer is composed of PDMS doped with CNT; the silver layer is configured with a crack structure, the crack structure being a crack that changes in response to the deformation of the silver layer; wherein the flexible film is a PDMS film; the CNT-PDMS layer has a thickness of 5-20 μm; and the CNT-PDMS layer contains carbon nanotubes in an amount of 0.01-5 wt %.
7 . The crack sensing device according to claim 6 , wherein further comprising a glass substrate, wherein the support is bonded to the glass substrate.
8 . The crack sensing device according to claim 7 , wherein the glass substrate is treated with O 2 plasma.
9 . The crack sensing device according to claim 6 , wherein the support is treated with O 2 plasma.