IP Library Granted Patent US 12,485,073
Granted Patent B2
US 12,485,073 · App. 17/594,639 · Granted Dec 2, 2025

Oral care compositions and methods of use

Inventors: Zhigang Hao (Bridgewater, NJ); Erin Laskowski (Manville, NJ); Victoria Yeung (Livingston, NJ); Mania Bankova (Highland Park, NJ); Long Pan (Somerset, NJ); Yun Xu (Langhorne, PA); Peng Yan (Guangzhou, CN); Fusong Sun (Martinsville, NJ); Zheng Yang (Guangzhou, CN); Chi-Yuan Cheng (Hillsborough, NJ); Tatiana Brinzari (Piscataway, NJ)
Assignee: Colgate-Palmolive Company
A61K8/21A61K8/24A61K8/27A61K8/44A61K8/463A61K8/731A61K8/92A61Q11/00A61K2800/28A61K2800/48A61K2800/524
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Quick Facts
Patent No.
US 12,485,073
App. No.
17/594,639
Granted
Dec 2, 2025
Kind
B2
Abstract

A stabilized oral care composition comprises amino acids and traditionally incompatible flavor components. Methods of making and use are further provided.

Claims (16)

1 . An oral care composition comprising:

a) an amino acid wherein the amino acid is selected from the group consisting of arginine, lysine and glycine;

b) wintergreen flavor, wherein the wintergreen flavor is wintergreen oil comprising methyl salicylate;

c) an abrasive or particulate; and

d) an orally acceptable vehicle,

wherein the amino acid is from 0.1 wt. % to 3.0 wt. %, wherein the wintergreen flavor is present in an amount of about 0.1 to 5.0 wt. %, calculated relative to the total weight of the composition,

wherein the composition has a pH of about 6.5 to less than 7.3, and

wherein the composition is capable of stabilizing the methyl salicylate such that less than 50% of the methyl salicylate degrades after 6 weeks under accelerated aging conditions.

2 . The composition according to claim 1 , wherein the amino acid is arginine.

3 . The composition according to claim 1 , wherein the wintergreen flavor is wintergreen oil further comprising members selected from the group consisting of menthol, anethole, eugenol or combinations thereof.

4 . The composition according to claim 1 , wherein the composition is capable of stabilizing the methyl salicylate such that less than 45% of the methyl salicylate degrades after 6 weeks under accelerated aging conditions, less than 40% of the methyl salicylate degrades after 6 weeks under accelerated aging conditions, less than 35% of the methyl salicylate degrades after 6 weeks under accelerated aging conditions, or less than 30% of the methyl salicylate degrades after 6 weeks under accelerated aging conditions.

5 . The composition according to claim 1 , wherein the abrasive or particulate is selected from alumina, aluminum hydroxide, calcium carbonate, precipitated calcium carbonate, dicalcium phosphate, mica, sodium bicarbonate, calcium pyrophosphate or combinations thereof.

6 . The composition according to claim 1 , further comprising a fluoride source selected from: sodium fluoride, potassium fluoride, sodium monofluorophosphate, sodium fluorosilicate, ammonium fluorosilicate, amine fluoride, ammonium fluoride, titanium fluoride, hexafluorosulfate, and combinations thereof.

7 . The composition according to claim 1 , further comprising a zinc ion source selected from zinc oxide, zinc citrate, zinc lactate, zinc phosphate and combinations thereof.

8 . The composition according to claim 7 , wherein the zinc ion source comprises or consists of a combination of zinc oxide and zinc citrate.

9 . The composition according to claim 1 , wherein the accelerated aging conditions is a 49° C. environment.

Continuity (1)
Related Publication 20220192940A1 · Jun 23, 2022
References Cited (34)
US 4272513A · Gaffar · 1981 [cited by applicant]
US 4314990A · Denny et al. · 1982 [cited by applicant]
US 6261540B1 · Nelson · 2001 [cited by applicant]
US 8226931B2 · Kindel et al. · 2012 [cited by applicant]
US 9005585B2 · Deckner et al. · 2015 [cited by applicant]
US 9713586B2 · Shi et al. · 2017 [cited by applicant]
US 10058493B2 · Manus · 2018 [cited by applicant]
US 10588841B2 · Pan et al. · 2020 [cited by applicant]
US 10744077B2 · Manus · 2020 [cited by applicant]
US 20080081023A1 · Deckner · 2008 [cited by examiner]
US 20080175801A1 · Ramji · 2008 [cited by applicant]
US 20150313813A1 · Rege · 2015 [cited by applicant]
US 20170368375A1 · Chen et al. · 2017 [cited by applicant]
US 20180015016A1 · Huang · 2018 [cited by examiner]
US 20180344596A1 · Manus et al. · 2018 [cited by applicant]
US 20190038531A1 · Rege et al. · 2019 [cited by applicant]
US 20200337959A1 · Manus · 2020 [cited by applicant]
CN 101573097 · 2009 [cited by applicant]
CN 104822362 · 2015 [cited by applicant]
CN 106236612 · 2016 [cited by applicant]
CN 106913470 · 2017 [cited by applicant]
CN 108078798 · 2018 [cited by applicant]
CN 108210351 · 2018 [cited by applicant]
EP 0449782 · 1991 [cited by applicant]
GB 1469398 · 1977 [cited by applicant]
WO 2008042279 · 2008 [cited by applicant]
WO 2014088572 · 2014 [cited by applicant]
WO 2016106069 · 2016 [cited by applicant]
“Dentar Amino Lion (Winter Green)”, Company: Lion Corporation, Japan, Brand: Dentar, Published on MINTEL GNPD, URL: https://www.gnpd.com/sinatra/recordpage/233912/, Published Oct. 2003, Last Retrieved Nov. 10, 2022. [cited by applicant]
“Premium Natural Toothpaste”, Company: Davids Natural Toothpaste, USA, Brand: Davids, Published on MINTEL GNPD, URL: https://www.gnpd.com/sinatra/recordpage/6361519/, Published Feb. 2019, Last Retrieved Nov. 10, 2022. [cited by applicant]
“Toothpaste Travel Pack”, Company: Yunnan Baiyao Group, China, Brand: Yunnan Baiyao, Published on MINTEL GNPD, URL: https://www.gnpd.com/sinatra/recordpage/1788850/, Published May 2012, Last Retrieved Nov. 10, 2022. [cited by applicant]
“Toothpaste”, Company: Yunnan Baiyao Group, China, Brand: Yunnan Baiyao, Published on MINTEL GNPD, URL: https://www.gnpd.com/sinatra/recordpage/3378783/, Published Aug. 2015, Last Retrieved Nov. 10, 2022. [cited by applicant]
Gavic et al, “Influence of Toothpaste pH on Its Capacity to Prevent Enamel Demineralization”, Contemporary Clinical Dentistry (2018), vol. 9, No. 4, pp. 554-559, DOI: 10.4103/ccd.ccd_667_18. [cited by applicant]
International Search Report and the Written Opinion of the International Searching Authority issued in International Application PCT/CN2019/084164 mailed Feb. 20, 2020. [cited by applicant]