IP Library › Granted Patent US 12,504,229
Granted Patent B2
US 12,504,229 · App. 17/757,044 · Granted Dec 23, 2025

Apparatus for continuous thermal separation of a multi-component substance

Inventor: Agnar Hellenes (Førde, NO)
Assignee: GRANT PRIDECO, INC.
F26B17/20B01D3/08F26B3/20F26B3/24F26B11/16
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,504,229
App. No.
17/757,044
Granted
Dec 23, 2025
Kind
B2
Abstract

A separation apparatus for continuous thermal separation of a substance is fed into a treatment chamber. The substance includes two or more components where at least one of the components is evaporable at an evaporation temperature (T e ). The separation apparatus includes a vessel including a vessel wall with an inner surface enclosing the treatment chamber having a length I C , a height H and a width W, a substance inlet for feeding the substance into the treatment chamber, a first outlet for releasing non--evaporated parts of the substance from the treatment chamber, a second outlet for releasing evaporated parts of the substance from the treatment chamber, and a rotary mechanism. The rotary mechanism includes a rotatable axle arranged within the treatment chamber having an orientation directed along the treatment chamber's length L and a mixing device fixed to, and extending perpendicular from, the rotatable axle. A radial outermost part of the mixing device includes a plurality of radially separated mixing protrusions, a rotary drive operatively connected to the rotatable axis, and a heating device arranged outside the treatment chamber. The heating device is configured to transfer thermal energy to a minimum peripheral volume (Vp) of the treatment chamber via the inner surface. The minimum peripheral volume (V p ) is defined as a volume between the inner surface and outer radial boundaries of the mixing device. The mixing device includes a plurality of rotary discs fixed with axial offsets to the rotatable axle. The heating device and the rotary drive are configured such that, when both the heating device and the rotary drive are operated at their respective operational input powers (P hd , P rm ), a resulting operational temperature (T op ) is obtained within at least part of the minimum peripheral volume (V p ) which is equal or higher than the evaporation temperature (T e ).

Claims (51)

1 . A separation apparatus for continuous thermal separation of a substance being fed into a treatment chamber, the substance comprising two or more components where at least one of the components is evaporable at an evaporation temperature (T e ),

wherein the separation apparatus comprises a vessel comprising:

a vessel wall with an inner surface enclosing the treatment chamber having a length l c , a height H and a width W,

a substance inlet for feeding the substance into the treatment chamber,

a vapor cloud formed comprising non-evaporated parts and evaporated parts of the substance,

a first outlet for releasing non-evaporated parts of the substance from the treatment chamber,

a second outlet for releasing evaporated parts of the substance from the treatment chamber, and

a rotor comprising a rotatable axle arranged within the treatment chamber having an orientation directed along the treatment chamber's length l c and a mixing device fixed to, and extending perpendicular from, the rotatable axle, wherein a radial outermost part of the mixing device comprises a plurality of radially separated mixing protrusions,

a rotary drive operatively connected to the rotatably axis, and

a heater arranged outside the treatment chamber, wherein the heater is configured to transfer thermal energy to a minimum peripheral volume (Vp) of the treatment chamber via the inner surface, wherein the minimum peripheral volume (V p ) is defined as a volume between the inner surface and outer radial boundaries of the mixing device, wherein the mixing device comprises:

a plurality of rotary discs fixed with axial offsets to the rotatable axle, and

wherein the heater and the rotary drive are configured such that, when both the heater and the rotary drive are operated at their respective operational input powers (P hd , P rm ), a resulting operational temperature (T op ) is obtained from the powers of the heater and rotary drive within at least part of the minimum peripheral volume (V p ) which is equal or higher than the evaporation temperature (T e ),

wherein the mixing device further comprises a plurality of elongated objects interconnecting the plurality of rotary discs,

wherein the plurality of elongated objects are arranged in a vicinity of a circumference of the plurality of the rotary discs,

wherein the radially separated mixing protrusions comprises a plurality of radially protruding elements distributed with offsets along the length (l c ) of the treatment chamber, the plurality of radially protruding elements configured to intensely mix the vapor cloud,

wherein the plurality of radially protruding elements are replaceably connected directly to the plurality of elongated objects, such that the plurality of radially protruding elements are removable directly from the plurality of elongated objects.

2 . The separation apparatus according to claim 1 , wherein a ratio between the radial diameter (d md ) of the mixing device and a radial diameter (d c ) of the treatment chamber is between 0.8 and 1.0.

3 . The separation apparatus according to claim 1 , wherein the plurality of radially separated mixing protrusions is divided into one or more sets distributed axially along the rotatable axle, across the axial length (l md ) of the mixing device, the number of mixing protrusions in each set being defined as the number of mixing protrusions in a complete circle around the rotatable axle when seen along the direction of the rotatable axle, and wherein the number of radially separated mixing protrusions in each set is determined according to the relation

# mp =C ( d md /v p,min ),

wherein # mp is rounded to the nearest integer, where

C is a constant equal to, or higher than, 12π and not higher than 80π,

# mp is the number of the radially separated mixing protrusions in each set,

d md [m] is the radial diameter of the mixing device, and

V p,min [m/s] is a minimum peripheral rotation velocity at a location on each of the mixing protrusions closest to the inner surface,

wherein the minimum peripheral rotation velocity exceeds 20 meters per second.

4 . The separation apparatus according to claim 1 , wherein the plurality of radially protruding elements is arranged radially symmetric around the rotatable axle.

5 . The separation apparatus according to claim 1 , wherein at least one of the plurality of radially protruding elements comprises a disturbing means at or near the end closest to the inner surface, designed to enhance mixing rate of the substance.

6 . The separation apparatus according to claim 1 , wherein the plurality of radially separated mixing protrusions is divided into one or more sets distributed axially along the rotatable axle, across the axial length (l md ) of the mixing device, the number of mixing protrusions in each set being defined as the number of mixing protrusions in a complete circle around the rotatable axle when seen along the direction of the rotatable axle and wherein the number of radially separated mixing protrusions in each set is determined according to the relation

# mp =C ( d md /v p,min ),

wherein # mp is rounded to the nearest integer, where

C is a constant equal to, or higher than, 45π and not higher than 80π,

# mp is the number of the radially separated mixing protrusions in each set,

d md [m] is the radial diameter of the mixing device, and

V p,min [m/s] is a minimum peripheral rotation velocity at a location on each of the mixing protrusions closest to the inner surface,

wherein the minimum peripheral rotation velocity exceeds 20 meters per second.

7 . The separation apparatus according to claim 1 , wherein the heater is configured to provide at least 60% of the total thermal energy required to reach and maintain the operational temperature (T op ) within the at least part of the minimum peripheral volume (V p ).

8 . The separation apparatus according to claim 1 , wherein the treatment chamber has a cylindrical shape with a radial diameter dc, wherein the ratio between the treatment chamber's length l c and the treatment chamber's radial diameter d c is equal or less than 4.0.

9 . The separation apparatus according to claim 1 , wherein at least one of the plurality of rotary discs displays at least one through-going opening for allowing the evaporated parts of the substance to flow through during operation.

10 . The separation apparatus according to claim 9 , wherein the at least one through-going opening is designed radially symmetric around the rotational axis.

11 . The separation apparatus according to claim 1 , wherein the vessel further comprises:

a plurality of inner ribs arranged on at least part of the inner surface, wherein each inner rib is protruding radially into the treatment chamber.

12 . The separation apparatus according to claim 11 , wherein the plurality of inner ribs are distributed with offsets around an inner surface circumference.

13 . The separation apparatus according to claim 1 , wherein the heater further comprises:

an enclosure arranged around the vessel such that a void is created between an outer surface of the vessel wall and an inner surface of the enclosure, wherein the enclosure comprises a heat inlet for feeding a heated fluid into the void and a heat outlet for releasing said heated fluid from the void.

14 . The separation apparatus according to claim 13 , wherein at least a part of the void comprises a plurality of outer fins extending in direction perpendicular to the length direction of the treatment chamber.

15 . The separation apparatus according to claim 13 , wherein the heated fluid is at least one of steam, hot vapor, molten matters, heated liquid, surplus exhaust from a generator and surplus exhaust from an engine.

16 . The separation apparatus according to claim 1 , wherein the heater comprises at least one heating elements arranged within the vessel wall.

17 . The separation apparatus according to claim 1 , wherein the separation apparatus further comprises:

a feeding device for feeding the flow of the substance into the treatment chamber,

a scrubber for scrubbing evaporated parts of the substance released from the second outlet during operation and

a solid discharge tank for collection of non-evaporated parts of the substance released from the first outlet during operation.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 9, 2024
From: NATIONAL OILWELL VARCO NORWAY AS
To: GRANT PRIDECO, INC.
Reel/Frame 067940/0192 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 9, 2024
From: HELLENES HOLDING AS
To: NATIONAL OILWELL VARCO NORWAY AS
Reel/Frame 067940/0195 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2022
From: HELLENES, AGNAR
To: HELLENES HOLDING AS
Reel/Frame 060228/0335 →
Priority Claims (1)
EP 19214523 · Dec 9, 2019 · regional
Continuity (1)
Related Publication 20230013608A1 · Jan 19, 2023
References Cited (28)
US 3808701A · Bachmann · 1974 [cited by applicant]
US 4194296A · Pagnozzi · 1980 [cited by examiner]
US 4869810A · Ellingsen et al. · 1989 [cited by applicant]
US 5375343A · Egger · 1994 [cited by applicant]
US 6061924A · Bolton · 2000 [cited by examiner]
US 6165349A · Madar · 2000 [cited by applicant]
US 6380517B2 · Morgan · 2002 [cited by examiner]
CN 101432051A · 2009 [cited by applicant]
CN 103347598A · 2013 [cited by applicant]
CN 104602777A · 2015 [cited by applicant]
EP 1236015A1 · 2002 [cited by applicant]
EP 1535888A1 · 2005 [cited by applicant]
GB 1575576A · 1980 [cited by applicant]
JP S6039400U · 1985 [cited by applicant]
JP 2003519768A · 2003 [cited by applicant]
JP 2004091280A · 2004 [cited by applicant]
KR 101007990B1 · 2011 [cited by examiner]
WO 200125709A1 · 2001 [cited by applicant]
WO 02092187A1 · 2002 [cited by applicant]
WO 2012103596A1 · 2012 [cited by applicant]
Translation, KR-101007990-B1 (Year: 2011). [cited by examiner]
International Search Report issued in PCT/EP2020/085346, mailed on Feb. 2, 2021 (3 pages). [cited by applicant]
Written Opinion of the International Searching Authority issued in PCT/EP2020/085346, mailed on Feb. 2, 2021 (8 pages). [cited by applicant]
Extended European Search Report issued in counterpart European Patent Application No. 19214523.3, mailed on Feb. 20, 2020 (9 pages). [cited by applicant]
Office Action issued in Chinese Application No. 2020800850442; Dated Nov. 28, 2023 (11 pages). [cited by applicant]
Office Action issued in Japanese Application No. 2022-534658, mailed Jun. 26, 2024 (9 pages). [cited by applicant]
“Building Construction Machinery”, edited by the Cadre College of the Department of Construction, Huazhong University of Science and Technology Press, dated Sep. 30, 2009, p. 162 (4 pages). [cited by applicant]
Office Action issued in Chinese Application No. 2020800850442, mailed Jul. 7, 2024 (18 pages). [cited by applicant]