Chemical agent detector with 30 second cycle
A gas chromatography instrument is provided that is capable of analyzing samples both quickly and accurately. The detector includes a first unit and a second unit that alternate between collection mode and desorption mode. This allows one unit to collect the sample, while the other unit desorbs another sample before the units switch operations. The alternating collection and desorption modes allows the detector to generate a data point approximately every thirty seconds, with each alternating unit.
1 . An air sampling device comprising:
a first unit and a second unit each comprising at least a respective one of the following:
a port switch valve,
a sample inlet in fluid communication with a first port of the port switch valve,
a cylindrical pre-concentrator tube curved in a C-shape, the pre-concentrator tube containing a sorbent, the pre-concentrator tube formed from a material capable of conducting electricity, a first end of the pre-concentrator tube in fluid communication with a sixth port of the port switch valve, and a second end of the pre-concentrator tube in fluid communication with a third port of the port switch valve,
an exhaust line in fluid communication with a second port of the port switch valve,
a carrier inlet in fluid communication with a fourth port of the port switch valve,
a main column in fluid communication with a fifth port of the port switch valve, and
a flame photometric detector in fluid communication with the main column,
wherein the first unit and the second unit each have a first and second configuration,
wherein the first unit is in the first configuration when the second unit is in the second configuration, and vice versa,
wherein in the first configuration, the first port is in fluid communication with the sixth port, the second port is in fluid communication with the third port, and the fourth port is in fluid communication with the fifth port,
wherein in the second configuration, the first port is in fluid communication with the second port, the third port is in fluid communication with the fourth port, and the fifth port is in fluid communication with the sixth port,
wherein the first unit and the second unit each are capable of alternating between a collection mode in the first configuration and desorption mode in the second
configuration, the first and second unit each completing one cycle every sixty seconds or less such that one of the first unit and second unit generates a data point every thirty seconds or less.
2 . The air sampling device of claim 1 , wherein the port switch valve of the first unit includes a plurality of ports.
3 . The air sampling device of claim 2 , wherein when the first unit is in the collection mode, the plurality of ports are in a first configuration, and wherein when the first unit is in the desorption mode, the plurality of ports are in a second configuration.
4 . The air sampling device of claim 2 , wherein when the first unit is in the collection mode, a carrier gas may be provided to the main column via two or more of the plurality of ports.
5 . The air sampling device of claim 1 , wherein the port switch valve of the second unit includes a plurality of ports.
6 . The air sampling device of claim 5 , wherein when the second unit is in the collection mode, the plurality of ports are in a first configuration, and wherein when the second first unit is in the desorption mode, the plurality of ports are in a second configuration.
7 . The air sampling device of claim 5 , wherein when the second unit is in the collection mode, a carrier gas may be provided to the main column via two or more of the plurality of ports.
8 . The air sampling device of claim 1 , wherein the first and second units are located within a single housing.
9 . The air sampling device of claim 1 , wherein when the first unit is in the desorption mode, a sample provided in the pre-concentrator tube is heated.
10 . The air sampling device of claim 1 , wherein when the second unit is in the desorption mode, a sample provided in the pre-concentrator tube is heated.
11 . An air sampling device comprising:
a first unit and a second unit,
the first unit and the second unit each being capable of alternating between a collection mode and desorption mode, each unit being in an opposite mode from the other, and the first and second unit working in conjunction with each other so that the device generates a data point in thirty seconds or less;
wherein the first and second unit each include a respective cylindrical pre-concentrator tube curved in a C-shape, the pre-concentrator tube containing a sorbent, the pre-concentrator tube formed from a material capable of conducting electricity.
12 . The air sampling device of claim 11 , wherein
the first unit comprises:
a port switch valve;
a main column; and
a flame photometric detector; and
the second unit comprises:
a port switch valve;
a main column; and
a flame photometric detector.
13 . The air sampling device of claim 12 , wherein the port switch valve of the first unit includes a plurality of ports.
14 . The air sampling device of claim 13 , wherein when the first unit is in the collection mode, the plurality of ports are in a first configuration, and wherein when the first unit is in the desorption mode, the plurality of ports are in a second configuration.
15 . The air sampling device of claim 13 , wherein when the first unit is in the collection mode, a carrier gas may be provided to the main column via two or more of the plurality of ports.
16 . The air sampling device of claim 12 , wherein the port switch valve of the second unit includes a plurality of ports.
17 . The air sampling device of claim 16 , wherein when the second unit is in the collection mode, the plurality of ports are in a first configuration, and wherein when the second first unit is in the desorption mode, the plurality of ports are in a second configuration.
18 . The air sampling device of claim 16 , wherein when the second unit is in the collection mode, a carrier gas may be provided to the main column via two or more of the plurality of ports.
19 . The air sampling device of claim 12 , wherein when the first unit is in the desorption mode, a sample provided in the pre-concentrator tube is heated.
20 . The air sampling device of claim 12 , wherein when the second unit is in the desorption mode, a sample provided in the pre-concentrator tube is heated.