IP Library › Granted Patent US 12,620,585
Granted Patent B2
US 12,620,585 · App. 18/050,598 · Granted May 5, 2026

Nickel and cobalt-free cathode for lithium-ion batteries and method of manufacture

Inventors: Akihiro Kushima (Orlando, FL); Yoshiya Fujiwara (Wako, JP); Yoshiyuki Morita (Wako, JP); Akihisa Tanaka (Wako, JP); Kazuki Chiba (Wako, JP)
Assignees: University of Central Florida Research Foundation, Inc.; Honda Motor Co., Ltd.
H01M4/505H01M4/0416H01M4/0471H01M4/131H01M4/1391H01M4/485H01M4/525H01M10/0525
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Quick Facts
Patent No.
US 12,620,585
App. No.
18/050,598
Granted
May 5, 2026
Kind
B2
Abstract

A nickel-free and cobalt-free cathode material for a lithium (Li) battery is provided. The cathode material includes, Li a Al 1-x-y-z Fe x Mn y Zn 2 O 2-δ , wherein a, x, y, z, and δ are in the following ranges: 0.95≤a≤1.2; 0≤x≤0.3; 0≤y≤0.3; 0≤z≤0.3; 0.5≤x+y+z≤0.99; 0≤δ≤0.1. In various embodiments, the present invention provides an improved Co-free/Ni-free Li-ion battery (LIB) cathode that exhibits good thermal stability and is capable of realizing a high cell voltage and specific capacity comparable to, or exceeding, currently known Li(NiCoMn)O 2 cathodes. The novel cathode chemistry in accordance with the embodiments of the present invention eliminates any potential cobalt supply issues and lowers the overall cost of the battery.

Claims (10)

1 . A cathode material for use in a lithium (Li)-ion battery, the cathode material comprising:

Li a Al 1-x-y-z Fe x Mn y Zn z O 2-δ , wherein a, x, y, z, and δ are in a range of 0.95≤a≤1.2; 0≤x≤0.3; 0≤y≤0.3; 0≤z≤0.3; 0.5≤x+y+z≤0.99; 0≤δ≤0.1, wherein the cathode material comprises Zn and at least one of Mn or Fe, and wherein the cathode material does not comprise Ni or Co.

2 . The cathode material of claim 1 , wherein the cathode material has a layered rock-salt structure characterized by an X-ray diffraction (XRD) pattern obtained using Cu-Kα radiation (λ=0.15418 nm) comprising at least one characteristic peak corresponding to (104), (110), (113), (101), (102) or (003) lattice spacings and wherein the observed (003) peak is located between 2θ=17.5° to 20.5°.

3 . The cathode material of claim 1 , wherein the cathode material is synthesized using a method selected from co-precipitation, citrate process, hydrothermal, ion exchange and solid-state reactions.

4 . A lithium (Li)-ion battery (LIB) comprising:

a cathode composed of a cathode material comprising Li a Al 1-x-y-z Fe x Mn y Zn z O 2-δ , wherein a, x, y, z, and δ are in a range of 0.95≤a≤1.2; 0≤x≤0.3; 0≤y≤0.3; 0≤z≤0.3; 0.5≤x+y+z ≤0.99; 0≤δ≤0.1, wherein the cathode material comprises Zn and at least one of Mn or Fe, and wherein the cathode material does not comprise Ni or Co;

an anode; and

an electrolyte positioned between the anode and the cathode.

5 . The LIB of claim 4 , wherein the cathode material has a layered rock-salt structure characterized by an X-ray diffraction (XRD) pattern obtained using Cu-Kα radiation (λ=0.15418 nm) comprising at least one characteristic peak corresponding to (104), (110), (113), (101), (102) or (003) lattice spacings and wherein the observed (003) peak is located between 2θ=17.5° to 20.5°.

6 . The LIB of claim 4 , wherein the cathode material is synthesized using a method selected from co-precipitation, citrate process, hydrothermal, ion exchange and solid-state reactions.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 25, 2023
From: FUJIWARA, YOSHIYA; MORITA, YOSHIYUKI; TANAKA, AKIHISA; CHIBA, KAZUKI
To: HONDA MOTOR CO., LTD.
Reel/Frame 062482/0037 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 29, 2022
From: KUSHIMA, AKIHIRO
To: UNIVERSITY OF CENTRAL FLORIDA RESEARCH FOUNDATION, INC.
Reel/Frame 062235/0358 →
Continuity (2)
Provisional Application 63275208 · Nov 3, 2021
Related Publication 20230155124A1 · May 18, 2023
References Cited (22)
US 6960335B1 · Singhal et al. · 2005 [cited by applicant]
US 20010053483A1 · Yamaura · 2001 [cited by examiner]
US 20070122703A1 · Whitfield et al. · 2007 [cited by applicant]
US 20200235390A1 · Belharouak · 2020 [cited by examiner]
CN 1658426A · 2005 [cited by applicant]
CN 1795574A · 2006 [cited by applicant]
CN 102593443A · 2012 [cited by applicant]
CN 102593459A · 2012 [cited by applicant]
CN 104269517A · 2015 [cited by applicant]
EP 1058325A2 · 2000 [cited by applicant]
JP 10067517A · 1998 [cited by applicant]
JP 2000348722A · 2000 [cited by applicant]
JP 2001122628A · 2001 [cited by applicant]
Bennett, JW et al. Emerging investigator series: first-principles and thermodynamics comparison of compositionally-tuned delafossites: cation release from the (001) surface of complex metal oxides. Environ. Sci.: Nano. … [cited by examiner]
Komaba, S. and Kubota, K. Na-Ion Batteries. 1.2 Crystal Structures of Layered Materials [online]. John Wiley & Sons, 2020 [retrieved on Oct. 6, 2025]. Retrieved from the internet: <URL: https://app.knovel.com/hotlink/pd… [cited by examiner]
First Office Action issued Dec. 10, 2024 by the State Intellectual Property Office of People's Republic of China for corresponding Chinese Patent Application No. 202211367018.6. Original and machine translation attached. [cited by applicant]
Machine translation of CN102593443A with Mar. 7, 2012, filing date and Jul. 18, 2012, publication date. [cited by applicant]
Machine translation of CN1795574A with May 27, 2004, filing date and Jun. 28, 2006, publication date. [cited by applicant]
Muralidharan, N. et al. LiNixFeyAlzO2, a new cobalt-free layered cathode material for advanced Li-ion batteries, Journal of Power Sources 471 (2020) 228389. [cited by applicant]
Hirayama, M. et al. Structure and electrode reactions of layered rocksalt LiFeO2 nanoparticles for lithium battery cathode, Journal of Power Sources 196 (2011) 6809-6814. [cited by applicant]
Decision on Rejection issued Jul. 9, 2025 by the State Intellectual Property Office of People's Republic of China for corresponding Chinese Patent Application No. 202211367018.6. Original document attached. [cited by applicant]
Notice of Reasons for Refusal issued Jan. 26, 2026 by the Japan Patent Office for corresponding Japanese Patent Application No. 2022-176111. Original document and machine translation attached. [cited by applicant]