IP Library › Granted Patent US 12,624,268
Granted Patent B2
US 12,624,268 · App. 18/142,674 · Granted May 12, 2026

Semi-solid biodegradable refrigerant gel

Inventor: Benjamin Wyckoff Shore (Islandia, NY)
Assignee: TEMPERATSURE, LLC
C09K5/066B65D81/18C08K13/02C08L1/286F25D5/02C08K2003/262C08K2003/3081C08K5/092C08K5/098
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Quick Facts
Patent No.
US 12,624,268
App. No.
18/142,674
Granted
May 12, 2026
Kind
B2
Abstract

A semi-solid biodegradable refrigerant gel and methods of making same are disclosed. The semi-solid biodegradable refrigerant gel includes water, a biodegradable thickening agent, a crosslinking agent, an optional secondary crosslinking agent, and a chelating agent. The semi-solid biodegradable refrigerant gel does not require encasement in a high-barrier containment material.

Claims (42)

1 . A semi-solid biodegradable refrigerant gel comprising:

water;

sodium carboxymethyl cellulose;

aluminum sulfate;

sodium aluminum sulfate;

sodium benzoate;

potassium sorbate;

citric acid; and

sodium carbonate.

2 . The semi-solid biodegradable refrigerant gel according to claim 1 , wherein the gel is encapsulated in a paper material consisting of over 85% fiber content by weight.

3 . The semi-solid biodegradable refrigerant gel according to claim 1 , wherein the semi-solid biodegradable refrigerant gel includes:

about 0.86% sodium carboxymethyl cellulose by weight relative to the water;

about 0.019% aluminum sulfate by weight relative to the water;

about 0.064% sodium aluminum sulfate by weight relative to the water;

about 0.139% sodium benzoate by weight relative to the water;

about 0.034% potassium sorbate by weight relative to the water;

about 0.024% citric acid by weight relative to the water; and

about 0.014% sodium carbonate by weight relative to the water.

4 . The semi-solid biodegradable refrigerant gel according to claim 1 , wherein the gel does not flow or leak.

5 . The semi-solid biodegradable refrigerant gel according to claim 1 , wherein the gel retains the shape of a container where the gel solidified.

6 . The semi-solid biodegradable refrigerant gel according to claim 1 , wherein the gel has a Latent Heat of Fusion >275 J/g and a eutectic point of about 0° Celsius.

7 . The semi-solid biodegradable refrigerant gel according to claim 1 , wherein the sodium aluminum sulfate has a different dissolution rate than the aluminum sulfate and is used in concert with the aluminum sulfate to achieve a specific pot-life.

8 . The semi-solid biodegradable refrigerant gel of claim 1 , wherein the gel has a pH above 4.0.

9 . The semi-solid biodegradable refrigerant gel of claim 1 , wherein the gel is utilized in a refrigerant pack.

10 . A method of making a semi-solid biodegradable refrigerant gel comprising:

providing a chamber and a disperser proximate to the chamber;

depositing a predetermined amount of water into the chamber;

adding a blend of raw materials to the water via the disperser, wherein the blend of raw materials comprises:

sodium carboxymethyl cellulose;

aluminum sulfate;

sodium aluminum sulfate;

sodium benzoate;

potassium sorbate;

citric acid; and

sodium carbonate;

mixing the blend of raw materials with the water to create a viscous liquid gel;

filling containers or molds with the viscous liquid gel or encapsulating the viscous liquid gel in an encapsulation material; and

allowing the viscous liquid gel to set in the containers or molds or encapsulation material to form the semi-solid gel.

11 . The method of claim 10 , further comprising freezing the gel to create a cold pack.

12 . The method of claim 10 , wherein the encapsulation material includes a low-barrier containment material.

13 . The method of claim 12 , wherein the low-barrier containment material is rollstock material and is converted into a pouch or bag during a filling process by sealed seams.

14 . The method of claim 11 , wherein the low-barrier containment material is a paper material consisting of over 85% fiber content by weight.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 5, 2025
From: MINUS WORKS INC.
To: TEMPERATSURE, LLC
Reel/Frame 070116/0738 →
MERGER Recorded Mar 5, 2024
From: MINUS WORKS LLC
To: MINUS WORKS INC.
Reel/Frame 066652/0237 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 4, 2023
From: SHORE, BENJAMIN WYCKOFF
To: MINUS WORKS INC.
Reel/Frame 063537/0001 →
Continuity (2)
Provisional Application 63338056 · May 4, 2022
Related Publication 20230357618A1 · Nov 9, 2023
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