IP Library › Granted Patent US 12,749,866
Granted Patent B2
US 12,749,866 · App. 18/337,713 · Granted Sep 29, 2026

Differential frequency generation

Inventors: Christian Keyser (Milton, FL); Micah Raab (Crestview, FL)
Assignee: United States of America as represented by the Secretary of the Air Force
H01S3/1083G02F1/3534G02F1/3548G02F1/361G02F1/392G02F1/395H01S3/06729H01S3/1086H01S3/20H01S3/302H01S3/307
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Quick Facts
Patent No.
US 12,749,866
App. No.
18/337,713
Granted
Sep 29, 2026
Kind
B2
Abstract

A fluid filled fiber for a quasi-phase matched generator and a laser incorporating such a fluid filled fiber. The laser has a liquid filled fiber with charge transfer molecules dissolved in a solvent. The liquid of the liquid filled fiber comprises or consists essentially of highly polar liquids and/or charge transfer molecules having relatively high molecular dipole values.

Claims (43)

1 . A liquid filled quasi-phase matched optical parametric amplification fiber laser comprising:

a light source in optical communication with a light transmitting fiber having a cladding and a liquid filled core therein, the liquid being a polar liquid adapted for OPA wherein the liquid further comprises Zwitterionic molecules,

the fiber having a Λ/D value ranging from 2.3 to 666.7.

2 . A fiber laser according to claim 1 wherein the liquid further comprises imidazolium ionic liquids having dipole moments from 12 D to 14 D.

3 . A fiber laser according to claim 2 wherein the liquid is free of dopant.

4 . A fiber laser according to claim 1 wherein the liquid has a dielectric constant ranging from 1 to 40.

5 . A fiber laser according to claim 4 wherein the liquid comprises from 80 w/% to 95 w/% bromotrichloromethane and from 5 w % to 15 w/% perfluorohexane.

6 . A fiber laser according to claim 1 wherein wherein n core >n cladding .

7 . A fiber laser according to claim 1 wherein wherein n core <n cladding .

8 . A fiber laser according to claim 1 , wherein the liquid further comprises charge transfer molecules having a bond length alternation from −0.045 to +0.045 whereby the liquid is configured for OPA and OPG.

9 . A difference frequency generator comprising:

a light source in communication with a hollow core fiber,

the hollow fiber being filled with at least two mixed liquids not having mutually overlapping Raman lines, one said liquid with Λ from 100 μm to 1000 μm, and σ from 0.1 μm to 10 μm, and a gas with Λ from 1000 μm to 10000 μm, and σ 1 from 1.0 μm to 10 μm;

two spaced apart electrodes configured to enable second order wave mixing the liquid or gas inside the hollow fiber, and having an electrode period of 0.1-10.0% of Λ.

10 . A generator according to claim 9 satisfying the equation:

deff

,

QPM

⁢

DFG

=

k

*

⁢

χ

⁡

(

2

)

/

2.

11 . A generator according to claim 10 wherein Λ/D ranges from 3 to 500 and D is the separation distance between electrodes in microns.

12 . A method of making a liquid filled quasi-phase matched optical parametric amplification fiber laser comprising the steps of:

selecting a nonlinear liquid charge transfer molecule having a uB ranging from 2 to E-48 esu to 2 E-40 esu;

selecting a transmissive solvent;

combining the nonlinerar liquid charge transfer molecule and the NIR transmissive solvent to yield a liquid having a dielectric constant of 1.5 to 7.5 to thereby provide a QPM OPA/G gain/SRS gain ratio greater than 1; and

disposing the liquid in a light transmitting fiber in optical communication with a light source.

13 . A method according to claim 12 wherein the solvent is NIR transmissive.

14 . A method according to claim 13 wherein the solvent is transmissive to light having a wavelength of 0.8 to 10 microns.

15 . A method according to claim 14 wherein the solvent is transmissive to light having a wavelength of 1 to 2 microns.

16 . A method according to claim 15 wherein the solvent is selected from the group consisting of bromotrichloromethane, perfluorohexane, trichloroacetonitrile and combinations thereof.

17 . A method according to claim 15 wherein the solvent consists of at least 40% BTM.

18 . A method according to claim 14 wherein the liquid is free of zwitterionic dopant.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 2, 2023
From: KEYSER, CHRISTIAN; ANYAR, INC.
To: THE GOVERNMENT OF THE UNITED STATES AS REPRESENTED BY THE SECRETARY OF THE AIR FORCE
Reel/Frame 064467/0799 →
Continuity (2)
Provisional Application 63438750 · Jan 12, 2023
Related Publication 20240243541A1 · Jul 18, 2024
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