IP Library Granted Patent US 7,892,367
Granted Patent B2
US 7,892,367 · App. 10/572,252 · Granted Feb 22, 2011

Tantalum sputtering target

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Quick Facts
Patent No.
US 7,892,367
App. No.
10/572,252
Granted
Feb 22, 2011
Kind
B2
Abstract

A tantalum sputtering target, wherein when the sum of the overall crystalline orientation is 1 on a tantalum target surface, the area ratio of crystals having any orientation among (100), (111), (110) does not exceed 0.5. Thus, obtained is a tantalum sputtering target having superior deposition properties where the deposition speed is high, film evenness (uniformity) is superior, and generation of arcings or particles is reduced.

Claims (16)

1. A sputtering target, comprising a tantalum sputtering target having a recrystallized grain structure formed by forging, rolling and heat treatment processing of a cast ingot such that said recrystallized grain structure has fine and uniform crystal grains, and said target having a random crystal orientation, wherein, when a sum of an overall crystalline orientation of a surface of said tantalum sputtering target is made to be 1, an area ratio of crystals having any orientation among (100), (111) and (110) does not exceed 0.5, and the area ratio of crystals having the orientation of (100) is 0.3 to 0.5.

2. The tantalum sputtering target according to claim 1 , wherein when the sum of the overall crystalline orientation of said surface of said tantalum sputtering target is 1, a sum of the area ratio of crystals having any two orientations among (100), (111) and (110) does not exceed 0.75.

3. A tantalum sputtering target according to claim 2 , wherein said surface is a sputtered erosion face of said tantalum sputtering target.

4. A tantalum sputtering target according to claim 3 , wherein an average crystal grain size of said tantalum sputtering target is 80 μm or less.

5. A tantalum sputtering target according to claim 1 , wherein said surface is a sputtered erosion face of said tantalum sputtering target.

6. A tantalum sputtering target according to claim 1 , wherein an average crystal grain size of said tantalum sputtering target is 80 μm or less.

7. A tantalum sputtering target according to claim 1 , wherein a purity of said tantalum sputtering target is 99.99% or more.

8. A tantalum sputtering target according to claim 1 , wherein the area ratio of crystals having the orientation of (100) is 0.4 to 0.5.

9. A sputtering target, comprising a tantalum sputtering target having a recrystallized grain structure formed by forging, rolling and heat treatment processing of a cast ingot such that said recrystallized grain structure has fine and uniform crystal grains, and said target having a random crystal orientation, wherein, when a sum of an overall crystalline orientation of a surface of said tantalum sputtering target is made to be 1, a sum of an area ratio of crystals having any two orientations among (100), (111) and (110) does not exceed 0.75, and an area ratio of crystals having an orientation of (100) is 0.3 to 0.5.

10. A tantalum sputtering target according to claim 9 , wherein the area ratio of crystals having the orientation of (100) is 0.4 to 0.5.

11. A sputtering target, comprising a tantalum sputtering target having a recrystallized grain structure formed by forging, rolling and heat treatment processing of a cast ingot such that said recrystallized grain structure has fine and uniform crystal grains, and said target having a random crystal orientation, wherein, when a sum of an overall crystalline orientation of a surface of said tantalum sputtering target is made to be 1, an area ratio of crystals having any orientation among (100)<001>, (111)<001> and (110)<001> of which is angular errors from an ND direction are within 10° does not exceed 0.5, and the area ratio of crystals having the orientation of (100)<001> of which angular errors from the ND direction are within 10° is 0.3 to 0.5.

12. A tantalum sputtering target according to claim 11 , wherein, when the sum of the overall crystalline orientation is 1 on said surface, the sum of the area ratio of crystals having any two orientations among (100)<001>, (111)<001> and (110)<001> of which angular errors from the ND direction are within 10° does not exceed 0.75.

13. A tantalum sputtering target according to claim 11 , wherein said surface is a sputtered erosion face of said tantalum sputtering target.

14. A tantalum sputtering target according to claim 11 , wherein an area ratio of crystals having the orientation of (111)<001> of which angular errors from the ND direction are within 10° is 0.2 to 0.3.

15. A sputtering target, comprising a tantalum sputtering target having a recrystallized grain structure formed by forging, rolling and heat treatment processing of a cast ingot such that said recrystallized grain structure has fine and uniform crystal grains, and said target having a random crystal orientation, wherein, when a sum of an overall crystalline orientation of a surface of said tantalum sputtering target is made to be 1, a sum of the area ratio of crystals having any two orientations among (100)<001>, (111)<001> and (110)<001> of which angular errors from an ND direction are within 10° does not exceed 0.75, and an area ratio of crystals having an orientation of (100)<001> of which angular errors from the ND direction are within 10° is 0.3 to 0.5.

16. A tantalum sputtering target according to claim 15 , wherein an area ratio of crystals having the orientation of (111)<001> of which angular errors from the ND direction are within 10° is 0.2 to 0.3.

Assignments (6)
CHANGE OF ADDRESS Recorded Aug 11, 2021
From: JX NIPPON MINING & METALS CORPORATION
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 057160/0114 →
CHANGE OF ADDRESS Recorded Feb 7, 2017
From: JX NIPPON MINING & METALS CORPORATION
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 041649/0733 →
CHANGE OF NAME Recorded Oct 12, 2010
From: NIPPON MINING HOLDINGS, INC.
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 025123/0358 →
MERGER Recorded Oct 8, 2010
From: NIPPON MINING & METALS CO., LTD.
To: NIPPON MINING HOLDINGS, INC.
Reel/Frame 025115/0062 →
CHANGE OF NAME Recorded Nov 29, 2006
From: NIKKO MATERIALS CO., LTD.
To: NIPPON MINING & METALS CO., LTD.
Reel/Frame 018560/0126 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2006
From: ODA, KUNIHIRO
To: NIKKO MATERIALS CO., LTD.
Reel/Frame 018519/0517 →