IP Library Granted Patent US 8,974,869
Granted Patent B2
US 8,974,869 · App. 12/693,548 · Granted Mar 10, 2015

Method for improving plating on non-conductive substrates

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Quick Facts
Patent No.
US 8,974,869
App. No.
12/693,548
Granted
Mar 10, 2015
Kind
B2
Abstract

A method of treating a laser-activated thermoplastic substrate having a metal compound dispersed therein is described. The substrate is contacted with an aqueous composition comprising: (i) a thiol functional organic compound; (ii) an ethoxylated alcohol surfactant; and (iii) xanthan gum. By use of the treatment composition, when the substrate is subsequently laser-activated and plated by electroless plating, extraneous plating of the substrate is substantially eliminated.

Claims (25)

1. A method of treating a laser-activatable non-conductive substrate, the method comprising the steps of:

a) treating the non-conductive substrate with an aqueous composition comprising:

i) a thiol functional organic compound; and

ii) preferably, a surfactant;

b) selectively laser activating portions of a surface of the non-conductive substrate;

c) contacting the substrate with an electroless plating bath such that areas of the substrate which were contacted by the laser plate, but areas that were not contacted by the laser do not plate.

2. The method according to claim 1 , wherein the thiol functional organic is selected from the group consisting of dodecanethiol, lauryl mercaptan, cetyl mercaptan, and stearyl mercaptan, alkyl thioglycollate, stearyl thioglycollate, cetyl thioglycollate, methyl mercaptan, n-butyl mercaptan, cyclohexyl mercaptan, n-dodecyl mercaptan, n-propyl mercaptan, n-octyl mercaptan and t-nonyl mercaptan and combinations of one or more of the foregoing.

3. The method according to claim 2 , wherein the thiol functional organic comprises stearyl mercaptan.

4. The method according to claim 1 , wherein the concentration of the thiol functional organic in the aqueous composition is between about 1 to about 20 g/l.

5. The method according to claim 1 , wherein the surfactant comprises an ethoxylated alcohol surfactant.

6. The method according to claim 5 , wherein the concentration of the ethoxylated alcohol surfactant in the aqueous composition is between about 0.1 to about 10 g/l.

7. The method according to claim 1 , wherein the aqueous compositions also comprises xanthan gum.

8. The method according to claim 7 , wherein the aqueous composition comprises a surfactant.

9. The method according to claim 1 , wherein the aqueous composition comprises a surfactant.

10. The method according to claim 1 , wherein the electroless plating bath comprises an electroless copper plating bath.

11. The method according to claim 1 , wherein the non-conductive substrate is selected from the group consisting of thermoplastic resins and thermosetting resins.

12. The method according to claim 11 , wherein the non-conductive substrate is a thermoplastic resin selected from the group consisting of polycarbonate/acrylonitrile butadiene styrene blend resins, cross-linked polybutyleneterephthalate, nylon, and liquid crystal polymers.

13. The method according to claim 12 , wherein the non-conductive substrate is a polycarbonate/acrylonitrile-butadiene-styrene blend resin.

14. The method according to claim 1 , wherein the non-conductive substrate is impregnated with a copper compound.

15. A method of treating a laser-activatable non-conductive substrate, the method comprising the steps of:

a) treating the non-conductive substrate with an aqueous composition comprising:

i) a thiol functional organic compound selected from the group consisting of dodecanethiol, lauryl mercaptan, cetyl mercaptan, and stearyl mercaptan, alkyl thioglycollate, stearyl thioglycollate, cetyl thioglycollate, methyl mercaptan, n-butyl mercaptan, cyciohexyl mercaptan, n-dodecyl mercaptan, n-propyl mercaptan, n-octyl mercaptan and t-nonyl mercaptan and combinations of one or more of the foregoing; and

ii) preferably, a surfactant;

b) selectively laser activating portions of a surface of the non-conductive substrate;

c) contacting the substrate with an electroless plating bath such that areas of the substrate which were contacted by the laser plate, but areas that were not contacted by the laser do not plate.

Assignments (8)
ASSIGNMENT OF SECURITY INTEREST IN PATENT COLLATERAL Recorded Nov 17, 2022
From: BARCLAYS BANK PLC
To: CITIBANK, N.A.
Reel/Frame 061956/0643 →
SECURITY INTEREST Recorded Feb 5, 2019
From: MACDERMID ACUMEN, INC.
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 048260/0828 →
RELEASE OF SECURITY INTEREST Recorded Feb 4, 2019
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: MACDERMID ACUMEN, INC.
Reel/Frame 048232/0405 →
ASSIGNMENT AND ASSUMPTION OF SECURITY INTERESTS AT REEL/FRAME NOS. 30831/0549, 30833/0660, 30831/0606, 30833/0700, AND 30833/0727 Recorded Nov 1, 2013
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS FIRST LIEN COLLATERAL AGENT
To: BARCLAYS BANK PLC, AS SUCCESSOR COLLATERAL AGENT
Reel/Frame 031536/0778 →
RELEASE OF SECURITY INTEREST IN PATENT COLLATERAL AT REEL/FRAME NO. 30831/0675 Recorded Nov 1, 2013
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS SECOND LIEN COLLATERAL AGENT
To: MACDERMID ACUMEN, INC.
Reel/Frame 031537/0094 →
SECOND LIEN PATENT SECURITY AGREEMENT Recorded Jul 19, 2013
From: MACDERMID ACUMEN, INC.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS SECOND LIEN COLLATERAL AGENT
Reel/Frame 030831/0675 →
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Jul 19, 2013
From: MACDERMID ACUMEN, INC.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS FIRST LIEN COLLATERAL AGENT
Reel/Frame 030831/0549 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 10, 2010
From: HAMILTON, ROBERT; LONG, ERNEST; KROL, ANDREW M.
To: MACDERMID, INCORPORATED
Reel/Frame 023919/0231 →