IP Library Granted Patent US 8,932,381
Granted Patent B2
US 8,932,381 · App. 13/375,844 · Granted Jan 13, 2015

Sintered porous material comprising particles of different average sizes

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Quick Facts
Patent No.
US 8,932,381
App. No.
13/375,844
Granted
Jan 13, 2015
Kind
B2
Abstract

A porous membrane, comprising a blend of a first powder of metal particles of the first average size and a second powder of metal particles of a second average size, the first powder and the second powder sintered together. The first average size is five to fifty times greater than the second average size. The porous membrane comprises from 40% to 60% by weight of the first powder.

Claims (39)

1. A porous membrane, comprising a blend of a first powder of metal particles of a first average size and a second powder of metal particles of a second average size, the first powder and the second powder sintered together,

wherein the first average size is five to fifty times greater than the second average size, and

wherein the porous membrane comprises from 40% to 60% by weight of the first powder,

wherein the water bubble point of the porous membrane is from 4 to 8 psi, and

wherein the porous membrane has a Log Reduction Value (LRV) of 4 or more for 0.1 micron particles in a gas having velocity of 3 slpm/cm 2 measured on a 0.4 centimeter thick membrane,

wherein the first average size is from about 40 microns to about 60 microns, and the second average size is not greater than about 2 microns.

2. The porous membrane of claim 1 , wherein a porosity of the porous membrane is from 37% by volume to 50% by volume.

3. The porous membrane of claim 1 , wherein a porosity of the porous membrane is from 42% by volume to 48% by volume.

4. The porous membrane of claim 1 , wherein the first average size is about 50 microns, and the second average size is about 2 microns.

5. The porous membrane of claim 1 , wherein the metal particles of the first powder and the metal particles of the second powder are each independently selected from nickel or stainless steel.

6. The porous membrane of claim 1 , wherein the metal particles of the first powder and the metal particles of the second powder are each selected from nickel.

7. A gas diffuser device comprising:

a housing having an inlet and an outlet; and

a porous membrane of claim 1 .

8. The device of claim 7 , wherein a porosity of the porous membrane is from 37% by volume to 50% by volume.

9. The device of claim 7 , wherein a porosity of the porous membrane is from 42% by volume to 48% by volume.

10. The device of claim 7 , wherein the first average size is about 50 microns, and the second average size is about 2 microns.

11. The device of claim 7 , wherein the metal particles of the first powder and the metal particles of the second powder are each independently selected from nickel or stainless steel.

12. The device of claim 7 , wherein the metal particles of the first powder and the metal particles of the second powder are each selected from nickel.

13. The device of claim 7 , wherein the porous membrane is a flat sheet having a thickness of 0.1 inch or more.

14. The device of claim 7 , wherein the porous membrane is a flat sheet having a thickness from 0.2 cm to 0.5 cm, and further wherein the Log Reduction Value of the porous membrane is at least 6 in a gas for 0.1 micron particles and velocity of 3 slpm/cm 2 .

15. The device of claim 14 , wherein the porous membrane has a burst pressure of at least 300 pounds per square inch.

16. The device of claim 14 , wherein the porous membrane has a burst pressure of greater than 350 pounds per square inch.

17. A method of purifying a gas stream, comprising:

directing a gas stream through a porous membrane of claim 1 ,

thereby purifying the gas stream.

18. The method of claim 17 , wherein a porosity of the porous membrane is from 37% by volume to 50% by volume.

19. The method of claim 17 , wherein a porosity of the porous membrane is from 42% by volume to 48% by volume.

20. The method of claim 17 , wherein the first average size is about 50 microns, and the second average size is about 2 microns.

21. The method of claim 17 , wherein the metal particles of the first powder and the metal particles of the second powder are each independently selected from nickel or stainless steel.

22. The method of claim 17 , wherein the metal particles of the first powder and the metal particles of the second powder are each selected from nickel.

23. The method of claim 17 , wherein the porous membrane is a flat sheet having a thickness of 0.1 inch or more.

24. The method of claim 17 , wherein the porous membrane is a flat sheet having a thickness from 0.2 cm to 0.5 cm, and further wherein the Log Reduction Value of the porous membrane is at least 6 in a gas for 0.1 micron particles and velocity of 3 slpm/cm 2 .

25. The method of claim 24 , wherein the porous membrane has a burst pressure of at least 300 pounds per square inch.

26. The method of claim 24 , wherein the porous membrane has a burst pressure of greater than 350 pounds per square inch.

27. A gas diffuser device comprising:

a housing having an inlet and an outlet; and

a porous membrane of claim 1 disposed within the housing in fluid communication with the inlet and the outlet,

wherein the porous membrane is a flat sheet having a thickness from 0.2 cm to 0.5 cm, having Log Reduction Value of at least 6 in a gas for 0.1 micron particles and velocity of 3 slpm/cm 2 , and a burst pressure of at least 300 pounds per square inch

Assignments (7)
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
ASSIGNMENT OF PATENT SECURITY INTEREST RECORDED AT REEL/FRAME 048811/0679 Recorded Nov 5, 2019
From: GOLDMAN SACHS BANK USA
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 050965/0035 →
SECURITY INTEREST Recorded Nov 13, 2018
From: ENTEGRIS, INC.; SAES PURE GAS, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 048811/0679 →
RELEASE OF SECURITY INTEREST Recorded Nov 8, 2018
From: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
To: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ATMI PACKAGING, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.
Reel/Frame 047477/0151 →
RELEASE OF SECURITY INTEREST Recorded Nov 8, 2018
From: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
To: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ATMI PACKAGING, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.
Reel/Frame 047477/0032 →
SECURITY INTEREST Recorded May 2, 2014
From: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.; ATMI PACKAGING, INC.
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 032812/0192 →
SECURITY INTEREST Recorded May 1, 2014
From: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.; ATMI PACKAGING, INC.
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 032815/0852 →