IP Library Granted Patent US 9,520,617
Granted Patent B2
US 9,520,617 · App. 14/211,528 · Granted Dec 13, 2016

Sulfolane mixtures as ambient aprotic polar solvents

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,520,617
App. No.
14/211,528
Granted
Dec 13, 2016
Kind
B2
Abstract

An improved solvent containing sulfolane and at least one dialkyl sulfone, preferably dimethyl sulfone, wherein the improved solvent is a liquid at room temperature and can be used for reaction media and electrochemistry.

Claims (10)

1. A mixture consisting of 85 wt % to 99 wt % of sulfolane and 1 wt %-15 wt % of at least one dialkyl sulfone, wherein the at least one dialkyl sulfone has the formula R—(SO 2 )—R′, where R and R′ can be the same as or different from one another and can be any C 1 -C 6 alkyl group.

2. The mixture of claim 1 , wherein the at least one dialkyl sulfone is selected from the group consisting of dimethylsulfone, ethyl methyl sulfone, dipropyl sulfone, ethyl propyl sulfone, diethyl sulfone, dibutyl sulfone, and combinations thereof.

3. The mixture of claim 1 , wherein the at least one dialkyl sulfone comprises dimethylsulfone.

4. The mixture of claim 1 , wherein the mixture is substantially devoid of water.

5. The mixture of claim 1 , wherein the mixture has a melting point between about 7° C. and about 20° C.

6. The mixture of claim 1 , wherein the mixture is a liquid at room temperature.

7. A method of lowering the melting point of sulfolane, said method comprising preparing a mixture consisting of 85 wt % to 99 wt % of sulfolane and 1 wt %-15 wt % of at least one dialkyl sulfone, wherein the dialkyl sulfone has the formula R—(SO 2 )—R′, where R and R′ can be the same as or different from one another and can be any C 1 -C 6 alkyl group.

8. The method of claim 7 , wherein the mixture of sulfolane and at least one dialkyl sulfone is substantially devoid of water.

9. The method of claim 7 , wherein the mixture of sulfolane and at least one dialkyl sulfone has a melting point between about 7° C. and about 20° C.

10. The method of claim 7 , wherein the at least one dialkyl sulfone is selected from the group consisting of dimethylsulfone, ethyl methyl sulfone, dipropyl sulfone, ethyl propyl sulfone, diethyl sulfone, dibutyl sulfone, and combinations thereof.

Assignments (4)
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
ASSIGNMENT OF PATENT SECURITY INTEREST RECORDED AT REEL/FRAME 048811/0679 Recorded Nov 5, 2019
From: GOLDMAN SACHS BANK USA
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 050965/0035 →
SECURITY INTEREST Recorded Nov 13, 2018
From: ENTEGRIS, INC.; SAES PURE GAS, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 048811/0679 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 19, 2016
From: ADVANCED TECHNOLOGY MATERIALS, INC.
To: ENTEGRIS, INC.
Reel/Frame 041029/0903 →