IP Library Granted Patent US 9,761,417
Granted Patent B2
US 9,761,417 · App. 14/234,023 · Granted Sep 12, 2017

AION coated substrate with optional yttria overlayer

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Quick Facts
Patent No.
US 9,761,417
App. No.
14/234,023
Granted
Sep 12, 2017
Kind
B2
Abstract

A fluorine plasma resistant coating on a substrate being a component in a semiconductor manufacturing system is disclosed. In one embodiment the composition includes an AlON coating that overlies a substrate, and an optional yttria coating layer that overlies the AlON coating, with a total coating thickness of about 5-6 microns.

Claims (11)

1. A substrate comprising a plasma-resistant layer of AlON overlying the substrate, wherein the AlON layer is from about 1 micron to about 10 microns thick, and an outermost plasma-resistant layer of yttria that is from about 1 micron to about 10 microns thick immediately overlying the AlON layer, said layer of yttria does not contain aluminum, the substrate being a component in a semiconductor manufacturing system, wherein the plasma-resistant layer of AlON and the outermost plasma-resistant layer of yttria protect the substrate from plasma exposure during semiconductor manufacturing and the substrate is quartz, alumina, aluminum, steels, metals, or alloys.

2. The substrate of claim 1 , wherein the AlON layer is from about 2 microns to about 3 microns thick and the AlON layer has a composition 41 atomic % Al (+/−1 atomic %), 57 atomic % O (+/−1 atomic %), and 2.0 atomic % N (+/−1 atomic %).

3. The substrate of claim 1 , wherein said yttria layer has a composition determined by Energy-dispersive X-ray spectroscopy (EDS) that substantially corresponds to the composition of yttria and there is no detectable aluminum in the yttria layer.

4. The substrate of claim 3 , wherein the yttria layer is from about 2 microns to about 3 microns thick and the yttria layer has a composition 25 atomic % Y (+/−1 atomic %) and 75 atomic % O (+/−1 atomic %).

5. The substrate of claim 1 , wherein the AlON layer, the yttria layer or both are deposited on the quartz substrate by pulsed reactive physical vapor deposition.

6. The substrate according to claim 1 , wherein the quartz is stoichiometric silicon dioxide with polycrystalline structure.

7. The substrate of claim 1 , wherein the component in the semiconductor manufacturing system is a chamber, chamber component, wafer susceptor, chuck, showerhead, liner, ring, nozzle, baffle, fastener, or wafer transport component.

8. The substrate of claim 1 , wherein the substrate is alumina and a total thickness of the AlON layer and the yttria layer is from about 5 microns to about 6 microns.

9. The substrate of claim 1 , wherein the substrate is aluminum and a total thickness of the AlON layer and the yttria layer is from about 5 microns to about 6 microns.

10. The substrate of claim 1 , wherein the substrate is a metal alloy and a total thickness of the AlON layer and the yttria layer is from about 5 microns to about 6 microns.

11. A substrate consisting of a plasma-resistant layer of AlON overlying the substrate, wherein the AlON layer is from about 1 micron to about 10 microns thick, and an outermost plasma-resistant layer of yttria that is from about 1 micron to about 10 microns thick immediately overlying the AlON layer, said layer of yttria does not contain aluminum, the substrate being a component in a semiconductor manufacturing system, wherein the plasma-resistant layer of AlON and the outermost plasma-resistant layer of yttria protect the substrate from plasma exposure during semiconductor manufacturing and the substrate is quartz, alumina, aluminum, steels, metals, or alloys.

Assignments (8)
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
ASSIGNMENT OF PATENT SECURITY INTEREST RECORDED AT REEL/FRAME 048811/0679 Recorded Nov 5, 2019
From: GOLDMAN SACHS BANK USA
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 050965/0035 →
SECURITY INTEREST Recorded Nov 13, 2018
From: ENTEGRIS, INC.; SAES PURE GAS, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 048811/0679 →
RELEASE OF SECURITY INTEREST Recorded Nov 8, 2018
From: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
To: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ATMI PACKAGING, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.
Reel/Frame 047477/0151 →
RELEASE OF SECURITY INTEREST Recorded Nov 8, 2018
From: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
To: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ATMI PACKAGING, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.
Reel/Frame 047477/0032 →
SECURITY INTEREST Recorded May 2, 2014
From: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.; ATMI PACKAGING, INC.
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 032812/0192 →
SECURITY INTEREST Recorded May 1, 2014
From: ENTEGRIS, INC.; POCO GRAPHITE, INC.; ATMI, INC.; ADVANCED TECHNOLOGY MATERIALS, INC.; ATMI PACKAGING, INC.
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 032815/0852 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 23, 2014
From: GUNDA, NILESH
To: ENTEGRIS, INC.
Reel/Frame 032031/0929 →